WO2012116462A1 - 用甘蔗生产黄腐酸的方法 - Google Patents

用甘蔗生产黄腐酸的方法 Download PDF

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Publication number
WO2012116462A1
WO2012116462A1 PCT/CN2011/000266 CN2011000266W WO2012116462A1 WO 2012116462 A1 WO2012116462 A1 WO 2012116462A1 CN 2011000266 W CN2011000266 W CN 2011000266W WO 2012116462 A1 WO2012116462 A1 WO 2012116462A1
Authority
WO
WIPO (PCT)
Prior art keywords
fulvic acid
sugar cane
producing
concentrating
solid
Prior art date
Application number
PCT/CN2011/000266
Other languages
English (en)
French (fr)
Inventor
朱天南
王汝新
朱毅彬
Original Assignee
Zhu Tiannan
Wang Ruxin
Zhu Yibin
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zhu Tiannan, Wang Ruxin, Zhu Yibin filed Critical Zhu Tiannan
Priority to PCT/CN2011/000266 priority Critical patent/WO2012116462A1/zh
Publication of WO2012116462A1 publication Critical patent/WO2012116462A1/zh

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F5/00—Fertilisers from distillery wastes, molasses, vinasses, sugar plant or similar wastes or residues, e.g. from waste originating from industrial processing of raw material of agricultural origin or derived products thereof
    • C05F5/004—Liquid waste from mechanical processing of material, e.g. wash-water, milling fluid, filtrate
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F11/00—Other organic fertilisers
    • C05F11/02—Other organic fertilisers from peat, brown coal, and similar vegetable deposits
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F5/00—Fertilisers from distillery wastes, molasses, vinasses, sugar plant or similar wastes or residues, e.g. from waste originating from industrial processing of raw material of agricultural origin or derived products thereof
    • C05F5/002—Solid waste from mechanical processing of material, e.g. seed coats, olive pits, almond shells, fruit residue, rice hulls
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12F—RECOVERY OF BY-PRODUCTS OF FERMENTED SOLUTIONS; DENATURED ALCOHOL; PREPARATION THEREOF
    • C12F3/00—Recovery of by-products
    • C12F3/02—Recovery of by-products of carbon dioxide
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P17/00—Preparation of heterocyclic carbon compounds with only O, N, S, Se or Te as ring hetero atoms
    • C12P17/18—Preparation of heterocyclic carbon compounds with only O, N, S, Se or Te as ring hetero atoms containing at least two hetero rings condensed among themselves or condensed with a common carbocyclic ring system, e.g. rifamycin
    • C12P17/181—Heterocyclic compounds containing oxygen atoms as the only ring heteroatoms in the condensed system, e.g. Salinomycin, Septamycin
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/02—Preparation of oxygen-containing organic compounds containing a hydroxy group
    • C12P7/04—Preparation of oxygen-containing organic compounds containing a hydroxy group acyclic
    • C12P7/06—Ethanol, i.e. non-beverage
    • C12P7/08—Ethanol, i.e. non-beverage produced as by-product or from waste or cellulosic material substrate
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/40—Preparation of oxygen-containing organic compounds containing a carboxyl group including Peroxycarboxylic acids
    • C12P7/44—Polycarboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12F—RECOVERY OF BY-PRODUCTS OF FERMENTED SOLUTIONS; DENATURED ALCOHOL; PREPARATION THEREOF
    • C12F3/00—Recovery of by-products
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
    • Y02A40/10—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
    • Y02A40/20—Fertilizers of biological origin, e.g. guano or fertilizers made from animal corpses
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/141—Feedstock
    • Y02P20/145—Feedstock the feedstock being materials of biological origin

Definitions

  • the present invention produces fulvic acid for all sugar cane production fulvic acid and sugar cane sugar by-product molasses. Background technique
  • Fulvic acid is a class of humic acid.
  • the content of fulvic acid is small. Therefore, the extraction of fulvic acid is an important research topic at home and abroad in recent years.
  • fulvic acid In the process of ttmi ⁇ ⁇ fulvic acid production, there is no discharge of waste water, waste gas and solid waste. It belongs to low-carbon economy and circular economy. In the process of producing fulvic acid, it can also produce four by-products of renewable fuel, organic fertilizer, gaseous or liquid or solid carbon dioxide and ethanol. The production of fulvic acid from molasses also eliminates the discharge of waste water, waste gas and solid waste, and can also produce two by-products of gaseous or liquid or solid carbon dioxide.
  • the invention adopts fresh sugar cane as a raw material, and obtains solid fulvic acid by pressing, fermenting, concentrating, distilling and drying.

Landscapes

  • Organic Chemistry (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Zoology (AREA)
  • Wood Science & Technology (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • General Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Biotechnology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Mechanical Engineering (AREA)
  • Botany (AREA)
  • Environmental & Geological Engineering (AREA)
  • Fertilizers (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)

Description

用甘蔗生产黄腐酸的方法
技术领域
本发明针对所有的甘蔗生产黄腐酸及甘蔗制糖副产品糖蜜生产黄腐酸。 背景技术
黄腐酸是腐植酸中的一个类别。在自然界一般的腐植酸资源中黄腐酸含量较少 所以黄腐酸的提取是近几年国内外重要的研究课题。
发明内容
相 ttmi^ ^黄腐酸生产过程中， 无废水、 废气、 固体废弃物的打排放。 属低碳经济， 循环经济范畴。 在生产黄腐酸的过程中， 还可产出可再生燃 料、 有机肥料、 气态或液态或固态二氧化碳、 乙醇四个副产品。 用糖蜜生 产黄腐酸也无废水、 废气、 固体废弃物排放， 还可产出气态或液态或固态 二氧化碳两个副产品。
附图说明
附图说明为工艺流程示意图
具体实施方式
本发明是以鲜甘蔗为原料， 经压搾、 发酵、 浓缩、 蒸馏、 干燥工序制取固 体黄腐酸。

Claims

WO 2012/116462 权 利 要 求 PCT/CN2011/000266 、 用甘蔗生产黄腐酸的方法包含压搾机、 发酵罐、 蒸馏设备、 浓缩设备、 浓缩 干燥设备。
、 根据权利要求 1所述的用甘蔗生产黄腐酸的方法， 其特征在于用鲜甘蔗经压 搾机榨取出甘蔗汁浓縮后经发酵罐发酵蒸馏后再进行干燥制取固体黄腐酸。 、 用甘蔗制糖生产的副产品糖蜜生产黄腐酸的方法包含稀释设备、 发酵罐、 蒸 馏设备、 浓缩干燥设备。
、 根据权利要求 2所述的用糖蜜生产黄腐酸的方法， 其特征在于用糖蜜经稀释 后经发酵罐蒸馏后再进行干燥制取固体黄腐酸。
PCT/CN2011/000266 2011-03-03 2011-03-03 用甘蔗生产黄腐酸的方法 WO2012116462A1 (zh)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PCT/CN2011/000266 WO2012116462A1 (zh) 2011-03-03 2011-03-03 用甘蔗生产黄腐酸的方法

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/CN2011/000266 WO2012116462A1 (zh) 2011-03-03 2011-03-03 用甘蔗生产黄腐酸的方法

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WO2012116462A1 true WO2012116462A1 (zh) 2012-09-07

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103543240A (zh) * 2013-11-11 2014-01-29 四川省农业科学院生物技术核技术研究所 发酵液中黄腐酸含量的测定方法
CN110846345A (zh) * 2019-12-06 2020-02-28 白博 一种棉花秸秆黄腐酸和纤维素乙醇生产工艺

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1087121A (zh) * 1992-11-16 1994-05-25 边文骅 利用发酵工艺生产黄腐酸的方法
CN1467180A (zh) * 2002-07-12 2004-01-14 陈五岭 微生物发酵甜高粱秸秆生产生化黄腐酸复合生物菌肥方法
CN1470638A (zh) * 2003-06-24 2004-01-28 广州市华达生化技术装备有限公司 甘蔗汁发酵节能生产酒精的方法
CN1710084A (zh) * 2005-06-14 2005-12-21 福建师范大学 糖质作物清汁发酵生产乙醇的清洁生产工艺
CN101760378A (zh) * 2010-01-25 2010-06-30 邹毅 甘蔗汁和糖蜜生产复合型兰姆酒的方法

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1087121A (zh) * 1992-11-16 1994-05-25 边文骅 利用发酵工艺生产黄腐酸的方法
CN1467180A (zh) * 2002-07-12 2004-01-14 陈五岭 微生物发酵甜高粱秸秆生产生化黄腐酸复合生物菌肥方法
CN1470638A (zh) * 2003-06-24 2004-01-28 广州市华达生化技术装备有限公司 甘蔗汁发酵节能生产酒精的方法
CN1710084A (zh) * 2005-06-14 2005-12-21 福建师范大学 糖质作物清汁发酵生产乙醇的清洁生产工艺
CN101760378A (zh) * 2010-01-25 2010-06-30 邹毅 甘蔗汁和糖蜜生产复合型兰姆酒的方法

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103543240A (zh) * 2013-11-11 2014-01-29 四川省农业科学院生物技术核技术研究所 发酵液中黄腐酸含量的测定方法
CN110846345A (zh) * 2019-12-06 2020-02-28 白博 一种棉花秸秆黄腐酸和纤维素乙醇生产工艺
CN110846345B (zh) * 2019-12-06 2020-11-06 白博 一种棉花秸秆黄腐酸和纤维素乙醇生产工艺

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