WO2011158216A1 - Method for protecting rice from being infected by fungi - Google Patents

Method for protecting rice from being infected by fungi Download PDF

Info

Publication number
WO2011158216A1
WO2011158216A1 PCT/IB2011/052653 IB2011052653W WO2011158216A1 WO 2011158216 A1 WO2011158216 A1 WO 2011158216A1 IB 2011052653 W IB2011052653 W IB 2011052653W WO 2011158216 A1 WO2011158216 A1 WO 2011158216A1
Authority
WO
WIPO (PCT)
Prior art keywords
rice
epoxiconazole
tricyclazole
weight
active compound
Prior art date
Application number
PCT/IB2011/052653
Other languages
English (en)
French (fr)
Inventor
Reinhard Stierl
Original Assignee
Basf Se
Basf (China) Company Limited
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se, Basf (China) Company Limited filed Critical Basf Se
Priority to IN282CHN2013 priority Critical patent/IN2013CN00282A/en
Priority to KR1020137001307A priority patent/KR20130025943A/ko
Priority to CN201180029351.XA priority patent/CN102946731B/zh
Priority to US13/703,822 priority patent/US20130090360A1/en
Priority to BR112012032355A priority patent/BR112012032355A2/pt
Publication of WO2011158216A1 publication Critical patent/WO2011158216A1/en

Links

Classifications

    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/64—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
    • A01N43/647—Triazoles; Hydrogenated triazoles
    • A01N43/653—1,2,4-Triazoles; Hydrogenated 1,2,4-triazoles
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N61/00—Biocides, pest repellants or attractants, or plant growth regulators containing substances of unknown or undetermined composition, e.g. substances characterised only by the mode of action

Definitions

  • Epoxiconazole and tricyclazole can be present in different isomeric forms. Their preparation and their action against harmful fungi are generally known to a person skilled in the art. Both compounds are commercially available (cf. , for example, www.alan- wood.net/pesticides/index_cn_frame.html).
  • the control of Pyricularia grisea and/or Rhizoctonia so- lani is particularly preferred.
  • control of Bipolaris oryzae, Microdochium oryzae and/or Ustilaginoidea virens is preferred.
  • the control of dirty panicle complex - a combination of various diseases in combination Curvularia lunata, Cercospora orzyae, Helmin- thosporium oryzae and/or Fusarium spp. is preferred.
  • the control of Pyricularia grisea and/or Rhizoctonia solani is very particularly preferred.
  • the rice plants or seed treated with the combinations of epoxiconazole and tricyclazole may by wildlife types, plants or seed obtained by breeding, mutagenesis or genetic engineering including but not limiting to agricultural biotech products on the market or in development, as well as rice plants which have been rendered tolerant to applications of specific classes of herbicides.
  • Genetically modified plants are plants, which genetic material has been so modified by the use of recombinant DNA techniques that under natural circumstances cannot readily be obtained by cross breeding, mutations or natural recombination (e.g. Golden Rice).
  • one or more genes have been integrated into the genetic material of a genetically modified plant in order to improve certain properties of the plant.
  • ge- netic modifications also include but are not limited to targeted post-translational modification of protein(s), oligo- or polypeptides e. g. by glycosylation or polymer additions such as prenylated, acetylated or farnesylated moieties or PEG moieties.
  • the further active compound is applied together with epoxiconazole and tricyclazole in synergistically effective amounts.
  • Combinations of epoxiconazole and tricyclazole with a herbicide are used in particular in rice varieties in which the sensitivity of the plants to the herbicide, i.e. glyphosate, is reduced.
  • Solvents/auxiliaries suitable for this purpose are essentially:
  • emulsifiers such as nonionogenic and anionic emulsifiers (for example polyoxy- ethylene fatty alcohol ethers, alkylsulfonates and arylsulfonates) and dispersants such as lignosulfite waste liquors and methylcellulose.
  • nonionogenic and anionic emulsifiers for example polyoxy- ethylene fatty alcohol ethers, alkylsulfonates and arylsulfonates
  • dispersants such as lignosulfite waste liquors and methylcellulose.
  • Suitable for use as surfactants are alkali metal, alkaline earth metal and ammonium salts of lignosulfonic acid, naphthalenesulfonic acid, phenolsulfonic acid, dibutyl- naphthalenesulfonic acid, alkylarylsulfonates, alkyl sulfates, alkylsulfonates, fatty alcohol sulfates, fatty acids and sulfated fatty alcohol glycol ethers, furthermore condensates of sulfonated naphthalene and naphthalene derivatives with formaldehyde, condensates of naphthalene or of naphthalenesulfonic acid with phenol and formaldehyde, polyoxyethylene octylphenyl ether, ethoxylated isooctylphenol, octyl- phenol, nonylphenol, alkylphenyl polyglycol ethers,
  • Substances which are suitable for the preparation of directly sprayable solutions, emulsions, pastes or oil dispersions are mineral oil fractions of medium to high boiling point, such as kerosene or diesel oil, furthermore coal tar oils and oils of vegetable or animal origin, aliphatic, cyclic and aromatic hydrocarbons, for example toluene, xylene, paraffin, tetrahydronaphthalene, alkylated naphthalenes or their derivatives, methanol, ethanol, propanol, butanol, cyclohexanol, cyclohexanone, isophorone, highly polar solvents, for example dimethyl sulfoxide, N-methylpyrrolidone and water.
  • Suitable antifreeze agents are, for example, glycerol, ethylene glycol and propylene glycol.
  • Suitable antifoams are, for example, silicon stearates or magnesium stearates.
  • Binders serve to improve the adhesion of the active compound or the active com- pounds on the seed.
  • Suitable binders are, for example, polyethylene oxide/polypropylene oxide copolymers, polyvinyl alcohol, polyvinylpyrrolidone, poly- (meth)acraylate, polybutene, polyisobutylene, polystyrene, polyethyleneamine, poly- ethyleneamide, polyethyleneimine (Lupasol ® , Polymin ® ), polyethers, polyurethanes, polyvinyl acetate and the copolymers of the above polymers.
  • Powders, materials for spreading and dustable products can be prepared by mixing or concomitantly grinding the active substances with a solid carrier.
  • Granules for example coated granules, impregnated granules and homogeneous granules, can be prepared by binding the active compounds to solid carriers.
  • solid carriers are mineral earths such as silica gels, silicates, talc, kaolin, attaclay, limestone, lime, chalk, bole, loess, clay, dolomite, diatomaceous earth, calcium sulfate, magnesium sulfate, magnesium oxide, ground synthetic materials, fertilizers, such as, for example, ammonium sulfate, ammonium phosphate, ammonium nitrate, ureas, and products of vegetable origin, such as cereal meal, tree bark meal, wood meal and nutshell meal, cellulose powders and other solid carriers.
  • mineral earths such as silica gels, silicates, talc, kaolin, attaclay, limestone, lime, chalk, bole, loess, clay, dolomite, diatomaceous earth
  • the formulations comprise from 0.01 to 95% by weight, preferably from 0.1 to 90% by weight, of the active compound(s).
  • the active compounds are employed in a purity of from 90% to 100%, preferably 95% to 100% (according to NMR spectrum).
  • the formulations can be diluted 2 to 10 times, resulting in ready-to- use preparations comprising from 0.01 to 60% by weight of the active compounds, preferably from 0.1 to 40% by weight of the active compounds.
  • Emulsions EW, EO, ES
  • the active compound(s) 25 parts by weight of the active compound(s) are dissolved in 35 parts by weight of xylene with addition of calcium dodecylbenzenesulfonate and castor oil ethoxylate (in each case 5 parts by weight).
  • This mixture is added to 30 parts by weight of water by means of an emulsifying machine (e.g. Ultraturrax) and made into a homogeneous emulsion. Dilution with water gives an emulsion.
  • the formulation has an active compound content of 25% by weight.
  • the active compound(s) are comminuted with addition of 10 parts by weight of dispersants and wetting agents and 70 parts by weight of water or an organic solvent to give a fine active compound suspension. Dilution with water gives a stable suspension of the active compound.
  • the active compound content in the formulation is 20% by weight.
  • the active compound(s) are ground finely with addition of 50 parts by weight of dispersants and wetting agents and made into water-dispersible or water- soluble granules by means of technical appliances (for example extrusion, spray tower, fluidized bed). Dilution with water gives a stable dispersion or solution of the active compound.
  • the formulation has an active compound content of 50% by weight.
  • 20 parts by weight of the active compound(s) are, with addition of 10 parts by weight of dispersants, 1 part by weight of gelling agent and 70 parts by weight of water or an organic solvent, comminuted in a bead mill to give a fine active compound suspension. Dilution with water affords a stabile suspension of the active compound.
  • the formulation has an active compound content of 20 parts by weight.
  • Oils of various types, wetting agents, adjuvants, herbicides, fungicides, other pesticides, or bactericides may be added to the active compounds even, if appropriate, not until immediately prior to use (tank mix). These agents are typically admixed with the compositions according to the invention in a weight ratio of from 1 :100 to 100:1 , preferably from 1 :10 to 10:1 .
  • Example 2 Activity against Pyricularia oryzae (rice blast)
  • the diseases were converted into efficacies.
  • An efficacy of 0 means that the infection level of the treated plants corresponds to that of the untreated control plants; an efficacy of 100 means that the treated plants were not infected.
  • the expected efficacies of active compound mixtures were determined using Colby's formula [R.S. Colby, "Calculating synergistic and antagonistic responses of herbicide combinations", Weeds 15, 20-22 (1967)] and compared with the observed efficacies. The dosages used and the obtained results are shown below:

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Pretreatment Of Seeds And Plants (AREA)
PCT/IB2011/052653 2010-06-18 2011-06-17 Method for protecting rice from being infected by fungi WO2011158216A1 (en)

Priority Applications (5)

Application Number Priority Date Filing Date Title
IN282CHN2013 IN2013CN00282A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) 2010-06-18 2011-06-17
KR1020137001307A KR20130025943A (ko) 2010-06-18 2011-06-17 진균에 의한 감염으로부터 벼를 보호하는 방법
CN201180029351.XA CN102946731B (zh) 2010-06-18 2011-06-17 保护稻以防真菌侵染的方法
US13/703,822 US20130090360A1 (en) 2010-06-18 2011-06-17 Method for protecting rice from being infected by fungi
BR112012032355A BR112012032355A2 (pt) 2010-06-18 2011-06-17 método para a produção do arroz contra infestação por fungos nocivos fitopatogênicos e uso de uma composição

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US35606410P 2010-06-18 2010-06-18
US61/356,064 2010-06-18
EP10166514 2010-06-18
EP10166514.9 2010-06-18

Publications (1)

Publication Number Publication Date
WO2011158216A1 true WO2011158216A1 (en) 2011-12-22

Family

ID=42735729

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/IB2011/052653 WO2011158216A1 (en) 2010-06-18 2011-06-17 Method for protecting rice from being infected by fungi

Country Status (8)

Country Link
US (1) US20130090360A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
KR (1) KR20130025943A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
CN (1) CN102946731B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
BR (1) BR112012032355A2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
CO (1) CO6650366A2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
CR (1) CR20120664A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
IN (1) IN2013CN00282A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
WO (1) WO2011158216A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102037980A (zh) * 2010-12-31 2011-05-04 利尔化学股份有限公司 杀菌农药组合物
WO2014033240A1 (en) * 2012-08-31 2014-03-06 Basf Se Use of an agrochemical composition with fungicidal, herbicidal and plant health improving action in rice

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1997040683A1 (en) * 1996-04-30 1997-11-06 Novartis Ag Pesticidal compositions
CN101258853A (zh) * 2008-04-10 2008-09-10 江苏宝灵化工股份有限公司 氯啶菌酯、唑类杀菌剂的组合物及用途
US20090124678A1 (en) * 2005-07-18 2009-05-14 Martin Semar Combined Use of Metconazole and Epoxiconazole for Reducing or Preventing the Contamination of Cereals With Mycotoxins
CN102037980A (zh) * 2010-12-31 2011-05-04 利尔化学股份有限公司 杀菌农药组合物

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ATE136728T1 (de) * 1991-12-19 1996-05-15 Ciba Geigy Ag Mikrobizide

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1997040683A1 (en) * 1996-04-30 1997-11-06 Novartis Ag Pesticidal compositions
US20090124678A1 (en) * 2005-07-18 2009-05-14 Martin Semar Combined Use of Metconazole and Epoxiconazole for Reducing or Preventing the Contamination of Cereals With Mycotoxins
CN101258853A (zh) * 2008-04-10 2008-09-10 江苏宝灵化工股份有限公司 氯啶菌酯、唑类杀菌剂的组合物及用途
CN102037980A (zh) * 2010-12-31 2011-05-04 利尔化学股份有限公司 杀菌农药组合物

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102037980A (zh) * 2010-12-31 2011-05-04 利尔化学股份有限公司 杀菌农药组合物
CN102037980B (zh) * 2010-12-31 2013-05-29 利尔化学股份有限公司 杀菌农药组合物
WO2014033240A1 (en) * 2012-08-31 2014-03-06 Basf Se Use of an agrochemical composition with fungicidal, herbicidal and plant health improving action in rice

Also Published As

Publication number Publication date
CO6650366A2 (es) 2013-04-15
BR112012032355A2 (pt) 2015-09-15
CR20120664A (es) 2013-03-04
KR20130025943A (ko) 2013-03-12
CN102946731B (zh) 2014-10-15
US20130090360A1 (en) 2013-04-11
CN102946731A (zh) 2013-02-27
IN2013CN00282A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) 2015-07-03

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