WO2011071706A1 - Procédé et appareil permettant de réguler la pression dans de multiples zones d'un outil de traitement - Google Patents

Procédé et appareil permettant de réguler la pression dans de multiples zones d'un outil de traitement Download PDF

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Publication number
WO2011071706A1
WO2011071706A1 PCT/US2010/058156 US2010058156W WO2011071706A1 WO 2011071706 A1 WO2011071706 A1 WO 2011071706A1 US 2010058156 W US2010058156 W US 2010058156W WO 2011071706 A1 WO2011071706 A1 WO 2011071706A1
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WO
WIPO (PCT)
Prior art keywords
pressure
flow
channel
orifice
controller
Prior art date
Application number
PCT/US2010/058156
Other languages
English (en)
Inventor
Junhua Ding
Original Assignee
Mks Instruments, Inc.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mks Instruments, Inc. filed Critical Mks Instruments, Inc.
Priority to KR1020147032950A priority Critical patent/KR101633266B1/ko
Priority to JP2012542109A priority patent/JP5764570B2/ja
Priority to GB1209918.0A priority patent/GB2487703B/en
Priority to DE201011004710 priority patent/DE112010004710T5/de
Publication of WO2011071706A1 publication Critical patent/WO2011071706A1/fr

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Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/455Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for introducing gases into reaction chamber or for modifying gas flows in reaction chamber
    • C23C16/45557Pulsed pressure or control pressure
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/228Gas flow assisted PVD deposition
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/455Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for introducing gases into reaction chamber or for modifying gas flows in reaction chamber
    • C23C16/45561Gas plumbing upstream of the reaction chamber
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/52Controlling or regulating the coating process
    • GPHYSICS
    • G05CONTROLLING; REGULATING
    • G05DSYSTEMS FOR CONTROLLING OR REGULATING NON-ELECTRIC VARIABLES
    • G05D16/00Control of fluid pressure
    • G05D16/02Modifications to reduce the effects of instability, e.g. due to vibrations, friction, abnormal temperature, overloading or imbalance
    • GPHYSICS
    • G05CONTROLLING; REGULATING
    • G05DSYSTEMS FOR CONTROLLING OR REGULATING NON-ELECTRIC VARIABLES
    • G05D16/00Control of fluid pressure
    • G05D16/20Control of fluid pressure characterised by the use of electric means
    • G05D16/2006Control of fluid pressure characterised by the use of electric means with direct action of electric energy on controlling means
    • G05D16/2013Control of fluid pressure characterised by the use of electric means with direct action of electric energy on controlling means using throttling means as controlling means
    • G05D16/2026Control of fluid pressure characterised by the use of electric means with direct action of electric energy on controlling means using throttling means as controlling means with a plurality of throttling means
    • G05D16/206Control of fluid pressure characterised by the use of electric means with direct action of electric energy on controlling means using throttling means as controlling means with a plurality of throttling means the plurality of throttling means being arranged for the control of a plurality of diverging pressures from a single pressure

Definitions

  • the disclosure is directed to multiple zone pressure controllers, and more particularly to an improved method of and apparatus for controlling pressure in multiple zones of a process tool such as a vacuum deposition chamber.
  • the wafer is positioned on a wafer support and held in place by a vacuum.
  • the wafer may not form a complete seal around the contact areas between the wafer and the wafer support.
  • a needle valve (called a "leakby" valve) is employed for partially diverting some of the flow of each channel from the inlet flow into a corresponding zone so that the inlet flow pressure of the gas or vapor into each zone can be adjusted so as to maintain the desired pressure of the inlet flow to each zone despite leakage at the contact areas between the wafer support and the wafer.
  • leakby needle valves can be used to tweak each channel so as to ensure that the inlet flow to each zone are match from channel to channel for a given same pressure setpoint. This way the flow rates into the various zones of a chamber can be equalized by tweaking the various needle valves. Needle valves, however, are expensive and physically take up space usually in a confined manufacturing area.
  • the system comprises: at least two channels configured and arranged so as to provide the flow of the gas or vapor to corresponding zones of the process tool, each channel including a pressure controller configured and arranged to control the pressure of gas or vapor in each channel, a leakby orifice or nozzle configured to provide a leak rate of gas or vapor from the channel; and a controller configured and arrange to determine the true flow information to each zone of the process tool so that the true leak rate in the chamber can be determined.
  • FIG. 1 is a partial schematic, partial block diagram of one embodiment of a multiple zone controller for controlling the pressure of inlet flow of a gas or vapor into multiple zones of a vacuum deposition chamber;
  • Fig. 2 is a partial schematic, partial block diagram of one channel of the multiple zone controller of Fig. 1 ;
  • FIG. 3 is a partial schematic, partial block diagram of a second embodiment of a multiple zone controller for controlling the pressure of inlet flow of a gas or vapor into multiple zones of a vacuum deposition chamber..
  • embodiments of the present disclosure are directed to a system for and method of providing an improved solution for multiple zone pressure control.
  • the system and method provide improved pressure control performance in response to upstream pressure disturbances.
  • the system is configured and arranged and the method is performed so as to provide true flow information to multiple zones of a process tool such as a vacuum deposition chamber, while reducing the material and manufacturing and performance costs of that of the dual zone pressure controller described above.
  • each needle valve is replaced by an orifice or a nozzle to provide a leakby line for pressure control in each channel.
  • Such orifice/nozzle configuration reduces costs, material and space, which is desirable to purchasers and users of multiple zone pressure controllers.
  • Employing orifice/nozzles alone however, would require extremely tight tolerances when machining the orifice/nozzles in order to match the existing needle valve set up of the current devices. This would add significant costs to the system, defeating the purpose of reducing costs by replacing each needle valve with a simpler device.
  • the multiple zone pressure controller is arranged and configured to provide the substitution of the orifice/nozzles for the needle valves with permissible manufacturing tolerances when constructing and employing the orifice/nozzles as replacements for the corresponding needle valves.
  • the system is constructed and arranged so as to sense any upstream pressure disturbances. This is preferably accomplished by employing a pressure transducer or sensor to monitor the upstream pressure.
  • the pressure transducer provides information that can be used by the multiple zone pressure controller so as to provide pressure insensitive (PI) flow control. If there is an upstream pressure disturbance and a false flow signal in the sensor of the mass flow controller, the system will know it by virtue of the output of the upstream pressure transducer and cancel the false flow signal.
  • the multiple zone pressure controller can also use the upstream pressure information to do a proactive control before the upstream pressure disturbance affects the downstream pressure control.
  • the system and method described provide better control performance, at reduced cost for manufacturers and customers alike.
  • one embodiment of the multiple zone pressure controller system 10 includes an inlet 12 receiving a gas or vapor from a gas source 14. The rate of flow into the system is indicated as Qt.
  • Pu 16 is connected to sense the pressure of the gas or vapor flowing into the system, and provide a signal to the controller 26 representative of the upstream pressure measurement.
  • the system receives the flow from the inlet and divides the flow among a plurality of (two or more) channels 18a, 18b ... 18n.
  • Each channel includes a mass flow controller (designated 20a, 20b ...20n).
  • Each mass flow controller 20 includes a mass flow sensor 22 and a control valve 24.
  • the sensor 22 of each mass flow controller 20 is constructed and arranged to sense the flow rate of gas or vapor through the corresponding channel 18, and provide a signal representative of the sensed flow to the controller 26.
  • Controller 26 is arranged and configured to receive and send data from and to a user through a user interface (UI).
  • Each channel 18 is also provided with a pressure transducer (designated 28a, 28b ... 28n) for sensing the pressure in the corresponding channel.
  • a signal is provided to the controller 26 representative of the pressure measured by each transducer
  • needle valves are expensive and take up significant space. Accordingly, it is desirable to replace each needle valve with an orifice/nozzle which is substantially cheaper, and takes up less space than the corresponding needle valve. But elimination of the needle valve eliminates the ability to tweak the individual channels in order to fine tune the system. This results in a high requirement that the orifices and the valves are identical in performance, within tight tolerances so that the flow through each channel is matched. Such tight tolerances drives up the costs, and results in the loss of savings that are gained from eliminating the needle valves.
  • each channel can be provided with an orifice/nozzle 32a, 32b ... 32n for providing leakby from the corresponding channel, without concern of tight tolerances that otherwise would be required.
  • the leakby lines including leakby orifice/nozzle 32 are all connected to a vacuum pump 34 for drawing gas or vapor from the channel for pressure control.
  • Each downstream transducer 28 provides a measurement of the pressure within a corresponding channel, and generates a signal as a function of the measured pressure to the controller 26.
  • the controller 26 compares the measured pressure with that of a set point, and provides a signal to the control valve 24 associated with the channel to make any adjustments to the flow so the measured pressure and the set point remain the same.
  • each channel includes a mass flow controller 20 for controlling the rate of flow through each corresponding channel.
  • the raw flow sensor signal of sensor 20 of each mass flow controller 20 is typically used for process tool diagnosis. However, any upstream pressure disturbance will generate a false flow signal in the flow sensor, which causes a false alarm during the process tool diagnosis at least in some applications. Further, the raw flow sensor signal is not a good indicator of the leaking around the wafer in the chamber.
  • controller 26 of the system 10 is configured and arranged to use data from each sensor 22, the upstream pressure transducer 16 and each downstream pressure transducer 28 to measure and control the true flow through each channel into the process tool 36, according to the following relationship:
  • Q mpc,i i s trie A° w rate measured by the flow sensor 22 of the mass flow controller 20. It can be further compensated by the upstream pressure transducer 16 in channel i such that it is a pressure insensitive flow rate;
  • each nozzle/orifice 32 is constructed so that choke flow conditions exist through each nozzle/orifice-this can be either measured or calculated based on the properties of the nozzle/orifice); while the last term:
  • T slp is the standard temperature which is 273.15K, and is the standard pressure which is 1.01325e5 Pa.
  • C is the discharge coefficient for the orifice (typical values are from 0.7 to 1.0)
  • a / is the cross section size of the orifice; is the downstream pressure measured with the transducer 28 in channel i, and
  • ,M is a gas function, which is a function of the specific heat ratio of the gas ⁇ , the molecular weight M of the gas, and the temperature T of the gas.
  • Qchamber indicates the true leaking around the wafer in the processing chamber in zone i. It is more accurate and meaningful than the previously used variable Q mp cr , h for process tool diagnosis. Acceptance of using Qchamber for diagnosing the leaking rate around the wafer will result in eliminating the need for tight tolerance requirements on the leak-by orifice/nozzle, thus reducing the costs of each orifice/nozzle.
  • the system and method provide (a) good control performance for multiple zone pressure control applications, (b) pressure insensitive flow output information form the multiple zone pressure controller, and (c) true flow information to process tools, such as chambers, for process tool diagnosis, while eliminating the need for needle valves.
  • the result is a good solution for multiple zone pressure control applications, improving the control performance in response to upstream pressure disturbances, as well as providing true flow information to the process chambers for process tool diagnosis.
  • each nozzle/orifice 32 be constructed so that choke flow conditions exist through each nozzle/orifice-this can be either measured or calculated based on the properties of the nozzle/orifice.
  • the multiple zone pressure controller system 40 which can be constructed arranged so that each nozzle/orifice 42a, 42b ...42n can operate under both chock and non-choke flow conditions.
  • a pressure transducer 44 can be connected and arranged so as to measure the downstream pressure of the leakby line so that the leakby flow rate can be calculated even if the flow through the leakby orifice/nozzle is not choked.
  • the leakby flow through each orifice/nozzle can be calculated by either one of two methods: (1) a mathematical formula or (2) a lookup table having the various values of ieakby , as function of the upstream pressure of the nozzle which is measured by the pressure transducer 28 and the downstream pressure of the nozzle which is measured by the downstream pressure transducer 44.
  • control algorithms/software/signals for controlling electrolysis can be implemented in hardware, software, firmware, or any combinations of such, and over one or more networks.

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Metallurgy (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Fluid Mechanics (AREA)
  • General Physics & Mathematics (AREA)
  • Automation & Control Theory (AREA)
  • Chemical Vapour Deposition (AREA)
  • Flow Control (AREA)
  • Physical Vapour Deposition (AREA)

Abstract

La présente invention a trait à un procédé et à un système de régulateur de pression à zones multiples permettant de réguler la pression d'un gaz ou l'écoulement de la vapeur vers au moins deux zones d'un outil de traitement tel qu'une chambre de dépôt par évaporation sous vide. Le système comprend : au moins deux canaux configurés et conçus de manière à fournir l'écoulement du gaz ou de la vapeur vers des zones correspondantes de l'outil de traitement, chaque canal incluant un régulateur de pression configuré et conçu de manière à réguler la pression du gaz ou de la vapeur dans chaque canal, un orifice ou une buse de fuite configuré de manière à fournir des pertes de gaz ou de vapeur à partir du canal ; et un régulateur configuré et conçu de manière à déterminer les informations du véritable écoulement de chaque zone de l'outil de traitement de sorte que les véritables fuites de gaz dans la chambre peuvent être déterminées.
PCT/US2010/058156 2009-12-07 2010-11-29 Procédé et appareil permettant de réguler la pression dans de multiples zones d'un outil de traitement WO2011071706A1 (fr)

Priority Applications (4)

Application Number Priority Date Filing Date Title
KR1020147032950A KR101633266B1 (ko) 2009-12-07 2010-11-29 다중 구역 압력 제어기 및 제어 방법
JP2012542109A JP5764570B2 (ja) 2009-12-07 2010-11-29 プロセス工具の多帯域の圧力を制御する方法及び制御するための装置
GB1209918.0A GB2487703B (en) 2009-12-07 2010-11-29 Methods of and apparatus for controlling pressure in multiple zones of a process tool
DE201011004710 DE112010004710T5 (de) 2009-12-07 2010-11-29 Verfahren und Vorrichtung zum Steuern bzw. Regeln des Druckes in mehreren Zonen eines Prozesswekzeuges

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US12/632,514 US9127361B2 (en) 2009-12-07 2009-12-07 Methods of and apparatus for controlling pressure in multiple zones of a process tool
US12/632,514 2009-12-07

Publications (1)

Publication Number Publication Date
WO2011071706A1 true WO2011071706A1 (fr) 2011-06-16

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Country Link
US (1) US9127361B2 (fr)
JP (1) JP5764570B2 (fr)
KR (2) KR101633266B1 (fr)
DE (1) DE112010004710T5 (fr)
GB (1) GB2487703B (fr)
TW (1) TWI537418B (fr)
WO (1) WO2011071706A1 (fr)

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DE112010004710T5 (de) 2012-10-31
US20110135821A1 (en) 2011-06-09
JP2013513028A (ja) 2013-04-18
TWI537418B (zh) 2016-06-11
GB201209918D0 (en) 2012-07-18
TW201144477A (en) 2011-12-16
KR20120101490A (ko) 2012-09-13
KR20140148499A (ko) 2014-12-31
JP5764570B2 (ja) 2015-08-19
GB2487703A (en) 2012-08-01
US9127361B2 (en) 2015-09-08
KR101633266B1 (ko) 2016-06-27
GB2487703B (en) 2015-09-02

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