WO2010143915A3 - 나노크기를 갖는 티탄산바륨 입자 및 그의 제조 방법 - Google Patents
나노크기를 갖는 티탄산바륨 입자 및 그의 제조 방법 Download PDFInfo
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- WO2010143915A3 WO2010143915A3 PCT/KR2010/003778 KR2010003778W WO2010143915A3 WO 2010143915 A3 WO2010143915 A3 WO 2010143915A3 KR 2010003778 W KR2010003778 W KR 2010003778W WO 2010143915 A3 WO2010143915 A3 WO 2010143915A3
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- milling
- rutile
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- barium titanate
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/46—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates
- C04B35/462—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates
- C04B35/465—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates based on alkaline earth metal titanates
- C04B35/468—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates based on alkaline earth metal titanates based on barium titanates
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
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- C04B35/465—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates based on alkaline earth metal titanates
- C04B35/468—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates based on alkaline earth metal titanates based on barium titanates
- C04B35/4682—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates based on alkaline earth metal titanates based on barium titanates based on BaTiO3 perovskite phase
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- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
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- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/62605—Treating the starting powders individually or as mixtures
- C04B35/6261—Milling
- C04B35/62615—High energy or reactive ball milling
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- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/62605—Treating the starting powders individually or as mixtures
- C04B35/62645—Thermal treatment of powders or mixtures thereof other than sintering
- C04B35/62675—Thermal treatment of powders or mixtures thereof other than sintering characterised by the treatment temperature
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- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
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- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
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- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3231—Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
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- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
- C04B2235/54—Particle size related information
- C04B2235/5418—Particle size related information expressed by the size of the particles or aggregates thereof
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- C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
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- C04B2235/5418—Particle size related information expressed by the size of the particles or aggregates thereof
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- Chemical & Material Sciences (AREA)
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- Environmental & Geological Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Physics & Mathematics (AREA)
- Nanotechnology (AREA)
- Thermal Sciences (AREA)
- Composite Materials (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Crystallography & Structural Chemistry (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Compositions Of Oxide Ceramics (AREA)
Abstract
본 발명은 나노크기를 갖는 티탄산바륨 입자 및 그의 제조 방법에 관한 것으로, 혼합비즈를 사용하여 균일분쇄와 분산효과를 동시에 얻을 수 있도록 하고, BaCO3 출발원료를 나노 분쇄한 후 나노크기의 TiO2와 혼합하는 방법을 사용하되, 1차 0.65mm, 1mm 혼합비즈와 1600rpm의 저속으로 고에너지밀에 의하여 분산을 행하고, 직렬로 연결된 0.1mm, 0.3mm 나노분쇄분산용 고에너지밀에 장입하여 분쇄 및 분산이 동시에 수행될 수 있도록 하는 발명에 관한 것이다. 아울러, 본 발명은 TiO2 출발원료를 사용하는 경우 루틸(58.2%) + 아나타제(41.8%)로 혼합된 것을 사용하여, 원활한 확산경로를 얻을 수 있도록 하고, 루틸 상의 높은 결정화도를 동시에 이용할 수 있도록 하여, 다른 출발원료를 즉 루틸이나 아나타제 단일상을 사용하는 것에 비하여 높은 반응성과 정방정비(c/a)를 얻을 수 있도록 하는 발명에 관한 것이다.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010800254046A CN102686535A (zh) | 2009-06-11 | 2010-06-11 | 具有纳米大小的BaTiO3粒子及其制备方法 |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR10-2009-0051863 | 2009-06-11 | ||
| KR1020090051863A KR101104627B1 (ko) | 2009-06-11 | 2009-06-11 | 나노크기를 갖는 티탄산바륨 입자 및 그의 제조 방법 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| WO2010143915A2 WO2010143915A2 (ko) | 2010-12-16 |
| WO2010143915A3 true WO2010143915A3 (ko) | 2011-04-14 |
Family
ID=43309387
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PCT/KR2010/003778 Ceased WO2010143915A2 (ko) | 2009-06-11 | 2010-06-11 | 나노크기를 갖는 티탄산바륨 입자 및 그의 제조 방법 |
Country Status (3)
| Country | Link |
|---|---|
| KR (1) | KR101104627B1 (ko) |
| CN (1) | CN102686535A (ko) |
| WO (1) | WO2010143915A2 (ko) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102557122A (zh) * | 2011-12-28 | 2012-07-11 | 广东风华高新科技股份有限公司 | 一种超细钛酸钡材料的制备方法 |
| WO2014084428A1 (ko) * | 2012-11-30 | 2014-06-05 | 삼성정밀화학(주) | 티탄산바륨 분말의 제조방법 및 그 방법에 의하여 제조된 티탄산바륨 분말 |
| KR101719840B1 (ko) * | 2012-11-30 | 2017-03-27 | 삼성전기주식회사 | 고결정성 유전체 물질의 제조방법 |
| CN108217720B (zh) * | 2016-12-15 | 2020-05-05 | 南方科技大学 | 片式多层陶瓷电容器用钛酸钡纳米晶的制备方法 |
| CN106745223A (zh) * | 2017-03-16 | 2017-05-31 | 东北大学 | 改性二氧化钛粉体的制备方法及改性二氧化钛粉体 |
| RU2646062C1 (ru) * | 2017-04-27 | 2018-03-01 | Открытое акционерное общество "Витебский завод радиодеталей "Монолит" (ОАО "ВЗРД "Монолит") | Способ изготовления титаната бария (BaTiO3) для многослойных керамических конденсаторов с температурой спекания диэлектрика не более 1130oС |
| CN110655378B (zh) * | 2018-06-29 | 2022-02-15 | 昆山微电子技术研究院 | 一种柔性电路板用复合材料的制备方法 |
| CN112266012B (zh) * | 2020-10-28 | 2021-10-22 | 潮州三环(集团)股份有限公司 | 一种钛酸钡粉体及其制备方法 |
| CN112808260B (zh) * | 2020-12-28 | 2023-10-20 | 江门市科恒实业股份有限公司 | 一种球磨法制备铈锆固溶体的方法 |
| CN117185343A (zh) * | 2022-09-06 | 2023-12-08 | 中国科学院上海硅酸盐研究所 | 一种固相法制备超细四方相钛酸钡粉体的方法 |
| CN120097380B (zh) * | 2025-05-08 | 2025-08-08 | 杭州兴容科技有限公司 | 一种超细钛酸钡粉体的固相法制备方法 |
| CN120097723B (zh) * | 2025-05-12 | 2025-07-29 | 杭州兴容科技有限公司 | 一种可用于mlcc的钙钛矿结构材料及其制备方法 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100475478B1 (ko) * | 2002-08-30 | 2005-03-10 | 한창산업주식회사 | 미세 분말상 티탄산바륨의 제조방법 |
| KR100771796B1 (ko) * | 2005-04-30 | 2007-10-30 | 삼성전기주식회사 | 유전체용 세라믹분말의 제조방법 |
| KR100921352B1 (ko) * | 2009-03-12 | 2009-10-15 | 한화석유화학 주식회사 | 미립 티탄산바륨계 분말의 제조방법 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4140695B2 (ja) * | 2002-07-31 | 2008-08-27 | 株式会社大阪チタニウムテクノロジーズ | 四塩化チタン水溶液及びこれを用いたチタン系複合酸化物の粉末製造方法 |
| KR100633723B1 (ko) * | 2005-08-04 | 2006-10-13 | 한화석유화학 주식회사 | 티탄산바륨의 제조방법 |
| JP2007161527A (ja) * | 2005-12-14 | 2007-06-28 | Matsushita Electric Ind Co Ltd | チタン酸バリウム粉末の製造方法および積層セラミックコンデンサ |
| CN101333000B (zh) * | 2007-06-27 | 2010-11-03 | 仙桃市中星电子材料有限公司 | 液相法合成高纯电子级钛酸钡的工艺 |
-
2009
- 2009-06-11 KR KR1020090051863A patent/KR101104627B1/ko not_active Expired - Fee Related
-
2010
- 2010-06-11 WO PCT/KR2010/003778 patent/WO2010143915A2/ko not_active Ceased
- 2010-06-11 CN CN2010800254046A patent/CN102686535A/zh active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100475478B1 (ko) * | 2002-08-30 | 2005-03-10 | 한창산업주식회사 | 미세 분말상 티탄산바륨의 제조방법 |
| KR100771796B1 (ko) * | 2005-04-30 | 2007-10-30 | 삼성전기주식회사 | 유전체용 세라믹분말의 제조방법 |
| KR100921352B1 (ko) * | 2009-03-12 | 2009-10-15 | 한화석유화학 주식회사 | 미립 티탄산바륨계 분말의 제조방법 |
Also Published As
| Publication number | Publication date |
|---|---|
| KR101104627B1 (ko) | 2012-01-12 |
| CN102686535A (zh) | 2012-09-19 |
| WO2010143915A2 (ko) | 2010-12-16 |
| KR20100133135A (ko) | 2010-12-21 |
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