WO2010143915A3 - 나노크기를 갖는 티탄산바륨 입자 및 그의 제조 방법 - Google Patents

나노크기를 갖는 티탄산바륨 입자 및 그의 제조 방법 Download PDF

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WO2010143915A3
WO2010143915A3 PCT/KR2010/003778 KR2010003778W WO2010143915A3 WO 2010143915 A3 WO2010143915 A3 WO 2010143915A3 KR 2010003778 W KR2010003778 W KR 2010003778W WO 2010143915 A3 WO2010143915 A3 WO 2010143915A3
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milling
rutile
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production method
barium titanate
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WO2010143915A2 (ko
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장길완
윤만순
임광수
최병기
이진형
손용호
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CQV Co Ltd
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Publication of WO2010143915A3 publication Critical patent/WO2010143915A3/ko
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Abstract

본 발명은 나노크기를 갖는 티탄산바륨 입자 및 그의 제조 방법에 관한 것으로, 혼합비즈를 사용하여 균일분쇄와 분산효과를 동시에 얻을 수 있도록 하고, BaCO3 출발원료를 나노 분쇄한 후 나노크기의 TiO2와 혼합하는 방법을 사용하되, 1차 0.65mm, 1mm 혼합비즈와 1600rpm의 저속으로 고에너지밀에 의하여 분산을 행하고, 직렬로 연결된 0.1mm, 0.3mm 나노분쇄분산용 고에너지밀에 장입하여 분쇄 및 분산이 동시에 수행될 수 있도록 하는 발명에 관한 것이다. 아울러, 본 발명은 TiO2 출발원료를 사용하는 경우 루틸(58.2%) + 아나타제(41.8%)로 혼합된 것을 사용하여, 원활한 확산경로를 얻을 수 있도록 하고, 루틸 상의 높은 결정화도를 동시에 이용할 수 있도록 하여, 다른 출발원료를 즉 루틸이나 아나타제 단일상을 사용하는 것에 비하여 높은 반응성과 정방정비(c/a)를 얻을 수 있도록 하는 발명에 관한 것이다.
PCT/KR2010/003778 2009-06-11 2010-06-11 나노크기를 갖는 티탄산바륨 입자 및 그의 제조 방법 Ceased WO2010143915A2 (ko)

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CN2010800254046A CN102686535A (zh) 2009-06-11 2010-06-11 具有纳米大小的BaTiO3粒子及其制备方法

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KR10-2009-0051863 2009-06-11
KR1020090051863A KR101104627B1 (ko) 2009-06-11 2009-06-11 나노크기를 갖는 티탄산바륨 입자 및 그의 제조 방법

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WO2010143915A3 true WO2010143915A3 (ko) 2011-04-14

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Families Citing this family (12)

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Publication number Priority date Publication date Assignee Title
CN102557122A (zh) * 2011-12-28 2012-07-11 广东风华高新科技股份有限公司 一种超细钛酸钡材料的制备方法
WO2014084428A1 (ko) * 2012-11-30 2014-06-05 삼성정밀화학(주) 티탄산바륨 분말의 제조방법 및 그 방법에 의하여 제조된 티탄산바륨 분말
KR101719840B1 (ko) * 2012-11-30 2017-03-27 삼성전기주식회사 고결정성 유전체 물질의 제조방법
CN108217720B (zh) * 2016-12-15 2020-05-05 南方科技大学 片式多层陶瓷电容器用钛酸钡纳米晶的制备方法
CN106745223A (zh) * 2017-03-16 2017-05-31 东北大学 改性二氧化钛粉体的制备方法及改性二氧化钛粉体
RU2646062C1 (ru) * 2017-04-27 2018-03-01 Открытое акционерное общество "Витебский завод радиодеталей "Монолит" (ОАО "ВЗРД "Монолит") Способ изготовления титаната бария (BaTiO3) для многослойных керамических конденсаторов с температурой спекания диэлектрика не более 1130oС
CN110655378B (zh) * 2018-06-29 2022-02-15 昆山微电子技术研究院 一种柔性电路板用复合材料的制备方法
CN112266012B (zh) * 2020-10-28 2021-10-22 潮州三环(集团)股份有限公司 一种钛酸钡粉体及其制备方法
CN112808260B (zh) * 2020-12-28 2023-10-20 江门市科恒实业股份有限公司 一种球磨法制备铈锆固溶体的方法
CN117185343A (zh) * 2022-09-06 2023-12-08 中国科学院上海硅酸盐研究所 一种固相法制备超细四方相钛酸钡粉体的方法
CN120097380B (zh) * 2025-05-08 2025-08-08 杭州兴容科技有限公司 一种超细钛酸钡粉体的固相法制备方法
CN120097723B (zh) * 2025-05-12 2025-07-29 杭州兴容科技有限公司 一种可用于mlcc的钙钛矿结构材料及其制备方法

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CN102686535A (zh) 2012-09-19
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