WO2009155454A3 - Procédé de séparation d'air hybride à enrichissement préliminaire non cryogénique et purification cryogénique faisant appel à un générateur de gaz ou de liquide à un seul composant - Google Patents

Procédé de séparation d'air hybride à enrichissement préliminaire non cryogénique et purification cryogénique faisant appel à un générateur de gaz ou de liquide à un seul composant Download PDF

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Publication number
WO2009155454A3
WO2009155454A3 PCT/US2009/047850 US2009047850W WO2009155454A3 WO 2009155454 A3 WO2009155454 A3 WO 2009155454A3 US 2009047850 W US2009047850 W US 2009047850W WO 2009155454 A3 WO2009155454 A3 WO 2009155454A3
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WIPO (PCT)
Prior art keywords
nitrogen
oxygen
cryogenic
noncryogenic
single component
Prior art date
Application number
PCT/US2009/047850
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English (en)
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WO2009155454A2 (fr
Inventor
William Brigham
Nick Ortenberg
Michael Schroeder
Original Assignee
William Brigham
Nick Ortenberg
Michael Schroeder
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Publication date
Application filed by William Brigham, Nick Ortenberg, Michael Schroeder filed Critical William Brigham
Priority to US12/999,965 priority Critical patent/US20110100055A1/en
Priority to CA2728244A priority patent/CA2728244A1/fr
Publication of WO2009155454A2 publication Critical patent/WO2009155454A2/fr
Publication of WO2009155454A3 publication Critical patent/WO2009155454A3/fr

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/22—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by diffusion
    • B01D53/229—Integrated processes (Diffusion and at least one other process, e.g. adsorption, absorption)
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/02—Preparation of oxygen
    • C01B13/0229—Purification or separation processes
    • C01B13/0248—Physical processing only
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/02—Preparation of oxygen
    • C01B13/0229—Purification or separation processes
    • C01B13/0248—Physical processing only
    • C01B13/0251—Physical processing only by making use of membranes
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/02—Preparation of oxygen
    • C01B13/0229—Purification or separation processes
    • C01B13/0248—Physical processing only
    • C01B13/0259—Physical processing only by adsorption on solids
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/02—Preparation of oxygen
    • C01B13/0229—Purification or separation processes
    • C01B13/0248—Physical processing only
    • C01B13/0259—Physical processing only by adsorption on solids
    • C01B13/0277—Temperature swing adsorption
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    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04006—Providing pressurised feed air or process streams within or from the air fractionation unit
    • F25J3/04078—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression
    • F25J3/04084—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression of nitrogen
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    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
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    • F25J3/04078—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression
    • F25J3/0409—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression of oxygen
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    • F25J3/04248—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04284—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams
    • F25J3/0429—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams of feed air, e.g. used as waste or product air or expanded into an auxiliary column
    • F25J3/04296—Claude expansion, i.e. expanded into the main or high pressure column
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    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/044—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a single pressure main column system only
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
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    • F25J3/04636—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a hybrid air separation unit, e.g. combined process by cryogenic separation and non-cryogenic separation techniques
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    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2256/00—Main component in the product gas stream after treatment
    • B01D2256/10—Nitrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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    • B01D2256/00—Main component in the product gas stream after treatment
    • B01D2256/12—Oxygen
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    • B01D—SEPARATION
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    • B01D2259/416—Further details for adsorption processes and devices involving cryogenic temperature treatment
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    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047—Pressure swing adsorption
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
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    • F25J2290/12—Particular process parameters like pressure, temperature, ratios
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    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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    • Y02P20/151—Reduction of greenhouse gas [GHG] emissions, e.g. CO2

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  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • General Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Separation By Low-Temperature Treatments (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)

Abstract

L'invention porte sur un système portable qui permet de produire de grandes quantités d'un gaz azote ou oxygène de grande pureté à haute pression. Selon l'invention, un système PSA, VSA, TSA ou à membrane perméable nettoie l'air en éliminant l'eau et le dioxyde de carbone, comme cela se fait normalement lors d'un cycle de distillation cryogénique, mais en élimine aussi une quantité significative d'oxygène ou d'azote, en fonction du gaz produit désiré. L'élimination de l'oxygène ou de l'azote préalablement au processus cryogénique permet d'utiliser une colonne de distillation significativement plus courte que d'ordinaire, entraînant une réduction de la taille de l'équipement qui rend ce dernier facile à transporter et à installer. On utilise en outre une pompe à liquide à haute pression pour augmenter la pression de l'azote ou de l'oxygène immédiatement avant leur admission dans l'échangeur de chaleur cryogénique où le liquide est vaporisé et le gaz entrant est refroidi.
PCT/US2009/047850 2008-06-19 2009-06-18 Procédé de séparation d'air hybride à enrichissement préliminaire non cryogénique et purification cryogénique faisant appel à un générateur de gaz ou de liquide à un seul composant WO2009155454A2 (fr)

Priority Applications (2)

Application Number Priority Date Filing Date Title
US12/999,965 US20110100055A1 (en) 2008-06-19 2009-06-18 Hybrid Air Separation Method with Noncryogenic Preliminary Enrichment and Cryogenic Purification Based on a Single Component Gas or Liquid Generator
CA2728244A CA2728244A1 (fr) 2008-06-19 2009-06-18 Procede de separation d'air hybride a enrichissement preliminaire non cryogenique et purification cryogenique faisant appel a un generateur de gaz ou de liquide a un seul composant

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US7411808P 2008-06-19 2008-06-19
US61/074,118 2008-06-19

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WO2009155454A3 true WO2009155454A3 (fr) 2010-04-01

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WO2012099510A1 (fr) * 2011-01-19 2012-07-26 Ahmad Reza Shirazi Extraction d'eau dans du gaz effluent provenant de procédés de combustion et industriels
US20130000352A1 (en) * 2011-06-30 2013-01-03 General Electric Company Air separation unit and systems incorporating the same
WO2014193751A1 (fr) * 2013-05-29 2014-12-04 Air Products And Chemicals, Inc. Purification, récupération et recyclage de gaz d'évent
US10145514B2 (en) * 2013-11-18 2018-12-04 Man Energy Solutions Se Cold-box system and method for power management aboard ships
WO2015128560A2 (fr) * 2014-02-25 2015-09-03 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Appareil de séparation d'air comprenant une colonne de séparation dont la partie inférieure est enfouie
FR3017940B1 (fr) * 2014-02-25 2019-06-28 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Appareil de separation d’air comprenant au moins un element souterrain
CN105911197B (zh) * 2016-05-25 2018-06-29 延边大学 全自动样品热解吸与液相微富集装置
CN108575343B (zh) * 2018-07-02 2023-06-27 合肥工业大学智能制造技术研究院 一种低能耗充氮储粮系统
IT202000032657A1 (it) * 2020-12-29 2022-06-29 Saipem Spa Sistema di accumulo e produzione di energia per la stabilizzazione della rete elettrica
CN115092891B (zh) * 2022-05-16 2023-08-15 西安交通大学 一种适用于高原环境制氧机及方法

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