MY160494A - Method for separation of methane and nitrogen - Google Patents

Method for separation of methane and nitrogen

Info

Publication number
MY160494A
MY160494A MYPI2015703932A MYPI2015703932A MY160494A MY 160494 A MY160494 A MY 160494A MY PI2015703932 A MYPI2015703932 A MY PI2015703932A MY PI2015703932 A MYPI2015703932 A MY PI2015703932A MY 160494 A MY160494 A MY 160494A
Authority
MY
Malaysia
Prior art keywords
methane
nitrogen
adsorption
gas
separation
Prior art date
Application number
MYPI2015703932A
Inventor
Akihiro Nakamura
Takayoshi Adachi
Takafumi Tomioka
Atsuko SHIGEOKA
Takuya Hasegawa
Original Assignee
Taiyo Nippon Sanso Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Taiyo Nippon Sanso Corp filed Critical Taiyo Nippon Sanso Corp
Publication of MY160494A publication Critical patent/MY160494A/en

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047Pressure swing adsorption
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/20Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising free carbon; comprising carbon obtained by carbonising processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28078Pore diameter
    • B01J20/28085Pore diameter being more than 50 nm, i.e. macropores
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10LFUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L3/00Gaseous fuels; Natural gas; Synthetic natural gas obtained by processes not covered by subclass C10G, C10K; Liquefied petroleum gas
    • C10L3/06Natural gas; Synthetic natural gas obtained by processes not covered by C10G, C10K3/02 or C10K3/04
    • C10L3/10Working-up natural gas or synthetic natural gas
    • C10L3/101Removal of contaminants
    • C10L3/105Removal of contaminants of nitrogen
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2253/00Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10Inorganic adsorbents
    • B01D2253/102Carbon
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2253/00Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/30Physical properties of adsorbents
    • B01D2253/302Dimensions
    • B01D2253/308Pore size
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2256/00Main component in the product gas stream after treatment
    • B01D2256/24Hydrocarbons
    • B01D2256/245Methane
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2257/00Components to be removed
    • B01D2257/10Single element gases other than halogens
    • B01D2257/102Nitrogen
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2259/00Type of treatment
    • B01D2259/40Further details for adsorption processes and devices
    • B01D2259/403Further details for adsorption processes and devices using three beds
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10LFUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L2290/00Fuel preparation or upgrading, processes or apparatus therefore, comprising specific process steps or apparatus units
    • C10L2290/12Regeneration of a solvent, catalyst, adsorbent or any other component used to treat or prepare a fuel
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10LFUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L2290/00Fuel preparation or upgrading, processes or apparatus therefore, comprising specific process steps or apparatus units
    • C10L2290/54Specific separation steps for separating fractions, components or impurities during preparation or upgrading of a fuel
    • C10L2290/542Adsorption of impurities during preparation or upgrading of a fuel

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Nanotechnology (AREA)
  • Inorganic Chemistry (AREA)
  • Separation Of Gases By Adsorption (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Treating Waste Gases (AREA)

Abstract

PROVIDED IS A METHOD OF ACQUIRING HIGH-PURITY NITROGEN GAS FROM A MIXED GAS OF METHANE AND NITROGEN USING AN INEXPENSIVE PSA APPARATUS AND RECOVERING METHANE FOR POWER GENERATION AT A HIGH RECOVERY RATE. PROVIDED IS A METHOD FOR SEPARATION OF METHANE AND NITROGEN FROM FEED GAS WHICH IS A MIXED GAS MAINLY FORMED OF METHANE AND NITROGEN BY A PRESSURE FLUCTUATION TYPE ADSORPTION METHOD USING TWO OR MORE ADSORPTION TOWERS A AND B, IN WHICH GAS SEPARATION ADSORBENTS 21 AND 22 HAVING AN EQUILIBRIUM ADSORPTION AMOUNT WITH RESPECT TO METHANE WHICH IS GREATER THAN THAT WITH RESPECT TO NITROGEN ARE FILLED IN THE ADSORPTION TOWERS A AND B, THE TIME OF THE PRESSURE EQUALIZATION STEP PERFORMED BY THE ADSORPTION TOWER A AFTER FINISHING THE ABSORPTION STEP AND THE ADSORPTION TOWER B AFTER FINISHING THE REGENERATION STEP IS 25 SECONDS TO 35 SECONDS, METHANE IS OBTAINED AT A CONCENTRATION OF 70% OR MORE AND A RECOVERY RATE OF 95% OR MORE, AND NITROGEN IS RECOVERED AT A CONCENTRATION OF 95% OR MORE.
MYPI2015703932A 2013-05-10 2014-05-09 Method for separation of methane and nitrogen MY160494A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2013100598 2013-05-10

Publications (1)

Publication Number Publication Date
MY160494A true MY160494A (en) 2017-03-15

Family

ID=51867332

Family Applications (1)

Application Number Title Priority Date Filing Date
MYPI2015703932A MY160494A (en) 2013-05-10 2014-05-09 Method for separation of methane and nitrogen

Country Status (4)

Country Link
JP (1) JP5901849B2 (en)
CN (1) CN105188885A (en)
MY (1) MY160494A (en)
WO (1) WO2014181860A1 (en)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP6468647B2 (en) * 2015-03-30 2019-02-13 住友精化株式会社 Pressure fluctuation adsorption apparatus and gas separation method
CN112742172B (en) * 2019-10-31 2023-03-24 中国石油化工股份有限公司 Energy gas purification method
CN112742170B (en) * 2019-10-31 2023-04-07 中国石油化工股份有限公司 Method for purifying high-nitrogen-content energy gas
CN114437846B (en) * 2020-11-04 2023-01-10 中国石油化工股份有限公司 Optimization method for natural gas pressure swing adsorption denitrification based on computer
WO2024036169A1 (en) * 2022-08-09 2024-02-15 Archaea Energy, Inc. Nitrogen removal system for methane purification from landfill gas, and method thereof

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0634894B2 (en) * 1985-01-31 1994-05-11 日本酸素株式会社 Method of equalizing the constant air volume of the adsorber
JPH06154595A (en) * 1992-11-19 1994-06-03 Kanebo Ltd Molecular sieve carbon for pressure swing type adsorption apparatus
US5536300A (en) * 1994-10-21 1996-07-16 Nitrotec Corporation Natural gas enrichment process
US5792239A (en) * 1994-10-21 1998-08-11 Nitrotec Corporation Separation of gases by pressure swing adsorption
JP2000312824A (en) * 1999-03-04 2000-11-14 Takeda Chem Ind Ltd Molecular sieving carbon for separating methane from mixed gas of methane and nitrogen
AU2007315542B2 (en) * 2006-10-31 2012-05-10 Osaka Gas Co., Ltd. Flammable gas concentration system
CN101935032B (en) * 2010-09-03 2012-11-07 同济大学 Preparation method and use of carbon molecular sieve
JP2012144628A (en) * 2011-01-12 2012-08-02 Air Water Inc Method and device for removing nitrogen in gas essentially composed of methane
CN202237712U (en) * 2011-10-11 2012-05-30 北京科技大学 Device for concentrating coal mine ventilation air methane through multi-tower vacuum pressure swing adsorption method

Also Published As

Publication number Publication date
CN105188885A (en) 2015-12-23
WO2014181860A1 (en) 2014-11-13
JPWO2014181860A1 (en) 2017-02-23
JP5901849B2 (en) 2016-04-13

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