WO2008009155A1 - Appareil pour vieillissement de boisson alcoolisée - Google Patents

Appareil pour vieillissement de boisson alcoolisée Download PDF

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Publication number
WO2008009155A1
WO2008009155A1 PCT/CN2006/001391 CN2006001391W WO2008009155A1 WO 2008009155 A1 WO2008009155 A1 WO 2008009155A1 CN 2006001391 W CN2006001391 W CN 2006001391W WO 2008009155 A1 WO2008009155 A1 WO 2008009155A1
Authority
WO
WIPO (PCT)
Prior art keywords
wine
diatomaceous earth
port
electrolytic cell
earth filter
Prior art date
Application number
PCT/CN2006/001391
Other languages
English (en)
Chinese (zh)
Inventor
Qingshui Zhou
Original Assignee
Qingshui Zhou
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Qingshui Zhou filed Critical Qingshui Zhou
Priority to PCT/CN2006/001391 priority Critical patent/WO2008009155A1/fr
Publication of WO2008009155A1 publication Critical patent/WO2008009155A1/fr

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14—Ultrafiltration; Microfiltration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14—Ultrafiltration; Microfiltration
    • B01D61/145—Ultrafiltration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14—Ultrafiltration; Microfiltration
    • B01D61/147—Microfiltration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2311/00—Details relating to membrane separation process operations and control
    • B01D2311/04—Specific process operations in the feed stream; Feed pretreatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14—Ultrafiltration; Microfiltration
    • B01D61/16—Feed pretreatment

Definitions

  • the present invention relates to a brewing apparatus, and more particularly to an aging apparatus for wine.
  • the new wine that has just been brewed has the taste, smell and astringency. It is not suitable for drinking. However, after a period of natural storage, the wine is fragrant, the alcohol is mellow, and the aftertaste is long. This is the so-called "aging wine”. "The origin of this statement. The reason is that the ethanol molecules in the new wine are mostly in a free state, the alcohol and ester content are less, and the acid and aldehyde content are higher. During the long-term storage process, the wine undergoes complex oxidation, reduction and esterification reactions. The components such as acid and aldehyde which cause bad taste, odor and astringency are lowered, and the ester of the component which produces aroma is increased.
  • the use of natural storage to age the wine requires a significant increase in the cost of the wine, not only to occupy a huge space, but also to accumulate a large amount of funds.
  • the "milk material” sold on the market is a ceramic material made by combining multi-functional materials. It contains trace elements beneficial to the human body, which can promote the oxidation and esterification of the wine, and oxidize the methanol in the wine to aromatic alcohol.
  • the odor of acetaldehyde and hydrogen sulfide is rapidly volatilized, and at the same time, the alcohol molecules and water molecules are polymerized to make the wine mellow.
  • This method usually requires immersing the wine material in a certain proportion for ten to fifteen days in order to achieve the effect of one year of storage. Therefore, the process of soaking still takes up a huge space, but shortens the time of storage. Still have to back up a certain amount of money, and. This method may leave other impurity particles in the wine.
  • Chinese Patent No. 92108367 discloses a "manufacturing method and equipment for wine", which is to directly add oxygen generated by electrolyzed water to a new wine so that the concentration of oxygen in the wine ranges from 2 X 10 to 6 Up to 1 X 10 - 4 moles, the device is a voltage-adjustable DC power supply, an electrolytic cell having at least two chambers communicating with each other at the bottom, and an outer casing and an intake pipe made of a material such as stainless steel, ceramic or glass. Reinforce the device.
  • the method utilizes the characteristic that the new oxygen has strong oxidizing ability, and accelerates the oxidation and esterification reaction of the wine.
  • the wine treated by the method tastes the aging effect equivalent to natural storage for six months on the same day, and there is no "rebirth". phenomenon.
  • the oxygen is electrolyzed and then the generated oxygen is introduced into the wine to be treated through the pipe, the oxygen is not easily dissolved in the wine uniformly, and thus the efficiency is low; and, when the method is used, the hydrogenation is performed.
  • it is troublesome to operate by transferring the body pipe to the hydrogen outlet of the electrolytic cell, which is not conducive to automated production.
  • the invention provides a wine aging treatment device, the main purpose of which is to overcome the shortcomings of the prior art that the natural stagnation method for aging the wine requires a long time, occupying a large field, and accumulating a large amount of funds, and can overcome other defects.
  • the aging method is not efficient, the effect is not obvious, it is easy to produce other impurities, and it is not easy to realize automatic production.
  • the wine aging treatment device comprises: a pre-filtration system, a feeding port and a discharge port for pre-filtering the wine, the feeding port is a wine inlet to be treated, and the feeding port is provided with a pressure pump
  • the first electrolytic cell is a sealed space, and has a cathode and an anode connected to a direct current power source, and a feeding port connected to a discharge port of the pre-filtration system
  • the secondary electrolytic cell is a sealed space, and the inside thereof; a cathode and an anode connected to a direct current power source, wherein the feed port is connected to the discharge port of the primary electrolytic cell
  • the cooling device has a feed port connected to the discharge port of the secondary electrolytic cell, and the wine after electrolytic treatment
  • the cooling treatment is performed; the membrane filtration device performs post-filtration treatment on the electrolytically treated wine, and the feed port is connected to the discharge port of the cooling device, and the discharge port is the finished wine outlet.
  • the water in the wine is electrolyzed to generate oxygen and hydrogen and directly dissolved in the wine, which greatly accelerates the redox reaction and the esterification reaction in the wine, so that the wine quickly becomes mature. , mellow.
  • multiple pairs of electrodes can be placed in the electrolytic cell to speed up the electrolysis.
  • the pre-filtration system of the wine includes a casing, a hollow cylinder disposed in the casing, and a plurality of diatomaceous earth filter discs, wherein the hollow cylinder body has through holes distributed therein, and the diatomaceous earth filter discs pass through respective
  • the central hole is set on the hollow cylinder, and each diatomaceous earth filter disk is provided with a plurality of channels radially distributed and communicating with the central hole thereof, and the hollow cylinder is disposed in each adjacent two diatomaceous earth filter plates.
  • the sleeve is provided with a rubber gasket, and one end of the hollow cylinder communicates with the discharge port of the pre-filtration system.
  • the liquor After entering the outer casing from the inlet of the pre-filtration system, the liquor penetrates from the outer periphery of the diatomaceous earth filter disk, enters the hollow cylinder through the radially distributed passage, and then flows out from the discharge port.
  • the pre-filtration system removes some yeast and some bacteria.
  • the membrane filtration device uses an inorganic membrane having a pore diameter of 0.2 to 1 ⁇ ra.
  • the membrane filtration device removes suspended particles from the wine and harmful components such as bacteria and microorganisms, while retaining the beneficial components of the wine and greatly enhancing the clarity of the wine.
  • the present invention has the following advantages over the prior art:
  • the secondary electrolysis is used to directly treat the wine, and the electrolysis time is extremely short. The effect is very remarkable. It takes only ten seconds to achieve the effect of natural storage for many years. Compared with the traditional storage process or the aging process, it saves time. 2.
  • Site and capital Second, suitable for automatic control of production, no artificial participation in the production process;
  • Figure 1 is a schematic perspective view of the present invention
  • Figure 3 is a schematic cross-sectional view of the pre-filtration system of the present invention showing the internal structure of the pre-filtration system.
  • the wine aging treatment device mainly comprises a pre-filtration system 3, a grade electrolytic cell 5, a secondary electrolytic cell 6, a cooling device 7, and a membrane filtering device 8, all of which are installed on A rack 1 is provided, and the rack 1 is provided with an automatic control system 11 for controlling the coordination of the various parts.
  • the pre-filtration system 3 includes two identical diatomaceous earth filtration devices connected in series with each other.
  • the diatomaceous earth filtration device includes a casing 30, a hollow cylinder 33 disposed in the casing 30, and a plurality of diatomaceous earth filter plates 34.
  • the sidewalls of the hollow cylinders 33 are provided with through holes 330, and the diatomaceous earth filter disks 34 are disposed on the hollow cylinders 33 through respective central holes, and each of the diatomaceous earth filter disks 34 is radially distributed and arranged.
  • the discharge port 32 is connected. After entering the feed port 31 of the diatomaceous earth filter device, the wine liquid permeates from the outer periphery of each diatomaceous earth filter disk 34, enters the hollow cylinder 33 through the radially distributed passage 340, and then flows out from the discharge port 32, and the pre-filtration system It can remove large particles of suspended solids and remove some yeast and some bacteria to prepare for the next electrolysis.
  • the feed port of the pre-filtration system 3 is connected to the feed port 1 of the entire plant through a pipe, and the feed port 1 is provided with a pressurizing pump 2 to power the flow of the liquor throughout the plant.
  • the primary electrolytic cell 5 is a sealed space, and has a cathode and an anode connected to a direct current power source, and a feed port connected to the discharge port of the pre-filtration system 3; the secondary electrolytic cell 6 is also a sealed space.
  • the cathode and the anode connected to the direct current power source are also provided inside, and the feed port is connected to the discharge port of the first electrolytic cell 5; the cooling device 7 can adopt the cooling device commonly used in the industry, the feed port and the secondary electrolytic cell.
  • the electrolytically treated wine is subjected to a cooling treatment; the membrane filtration device 8 performs post-filtration treatment on the electrolytically treated wine, the feed port is connected to the discharge port of the cooling device 7, and the discharge port is connected to the finished wine outlet 9.
  • the water in the wine is electrolyzed to generate oxygen and hydrogen and directly dissolved in the wine, thereby greatly accelerating the redox reaction and the esterification reaction in the wine, so that the wine is rapidly changed. Get cooked and fragrant.
  • the membrane filtration device 8 uses an inorganic membrane having a pore diameter of 0.2 to 1 ⁇ m, and the membrane filtration device using the pore size inorganic membrane can remove suspended particles in the wine and harmful components such as bacteria and microorganisms, while retaining the beneficial components in the wine. , and the clarity of the wine is greatly improved.
  • the wine to be treated is pre-filtered through a diatomaceous earth filtering device (step S1), and after removing a large suspended solid, the first electrolytic treatment (step S2) and secondary electrolysis are performed.
  • Treatment step S3, rapid oxidation-reduction reaction and esterification reaction, rapidly becoming mature, mellow alcohol, and then cooling the electrolyzed wine (step S4), and finally filtering by membrane method to remove the suspension in the wine
  • the particles, harmful components such as bacteria and microorganisms step S5
  • the treatment device provided by the embodiment can also be used for the treatment of vinegar, mineral water, perfume, etc., and has good effects.
  • the wine aging treatment device of the invention comprises a pre-filtration system, a primary electrolytic cell, a secondary electrolytic cell, a cooling device and a membrane filtering device, and the aging rate of the wine is effectively accelerated by directly treating the wine.
  • the invention has reasonable design, convenient processing by each device, and good industrial applicability.

Landscapes

  • Engineering & Computer Science (AREA)
  • Water Supply & Treatment (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Water Treatment By Electricity Or Magnetism (AREA)
  • Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)

Abstract

La présente invention concerne un appareil pour le vieillissement de boisson alcoolisée. Cet appareil comprend plusieurs éléments. Un pré-filtre sert à filtrer le produit. L'entrée d'alimentation, qui est équipée d'une pompe de suralimentation, est l'entrée du produit brut. Le premier bain électrolytique, qui est enfermé, est équipé d'une cathode et d'une anode reliées à l'alimentation en courant continu. Son entrée est connectée à la sortie du pré-filtre. Le deuxième bain électrolytique, qui est enfermé, est équipé d'une cathode et d'une anode reliées à l'alimentation en courant continu. Son entrée est connectée à la sortie du premier bain électrolytique. Un dispositif de refroidissement sert à refroidir le produit en sortie d'électrolyse. Son entrée est connectée à la sortie du deuxième bain électrolytique. Un dispositif de filtrage à membrane sert à filtrer le produit après électrolyse. Son entrée est connectée à la sortie du dispositif de filtrage, sa sortie étant la sortie du produit fini.
PCT/CN2006/001391 2006-06-20 2006-06-20 Appareil pour vieillissement de boisson alcoolisée WO2008009155A1 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PCT/CN2006/001391 WO2008009155A1 (fr) 2006-06-20 2006-06-20 Appareil pour vieillissement de boisson alcoolisée

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/CN2006/001391 WO2008009155A1 (fr) 2006-06-20 2006-06-20 Appareil pour vieillissement de boisson alcoolisée

Publications (1)

Publication Number Publication Date
WO2008009155A1 true WO2008009155A1 (fr) 2008-01-24

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Application Number Title Priority Date Filing Date
PCT/CN2006/001391 WO2008009155A1 (fr) 2006-06-20 2006-06-20 Appareil pour vieillissement de boisson alcoolisée

Country Status (1)

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WO (1) WO2008009155A1 (fr)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108034561A (zh) * 2017-12-06 2018-05-15 江苏普莱泰可机械科技有限公司 白酒老熟装置及应用其的老熟方法
CN110205230A (zh) * 2019-05-31 2019-09-06 贵州省赤水市金钗石斛产业开发有限公司 一种模拟春夏秋冬季节加速酒分子结构变化的方法
CN112625851A (zh) * 2021-02-04 2021-04-09 沈阳农业大学 一种磁化催陈设备及催陈方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1076963A (zh) * 1992-04-04 1993-10-06 龚政 酒的高效人工催陈法和设备
CN2212010Y (zh) * 1994-10-25 1995-11-08 孟武 激电式酒质改善机
CN2309339Y (zh) * 1997-05-06 1999-03-03 郭济生 一种电子处理酒的装置
CN1615759A (zh) * 2004-12-07 2005-05-18 吉林大学 一种高压脉冲电场处理装置

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1076963A (zh) * 1992-04-04 1993-10-06 龚政 酒的高效人工催陈法和设备
CN2212010Y (zh) * 1994-10-25 1995-11-08 孟武 激电式酒质改善机
CN2309339Y (zh) * 1997-05-06 1999-03-03 郭济生 一种电子处理酒的装置
CN1615759A (zh) * 2004-12-07 2005-05-18 吉林大学 一种高压脉冲电场处理装置

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108034561A (zh) * 2017-12-06 2018-05-15 江苏普莱泰可机械科技有限公司 白酒老熟装置及应用其的老熟方法
CN110205230A (zh) * 2019-05-31 2019-09-06 贵州省赤水市金钗石斛产业开发有限公司 一种模拟春夏秋冬季节加速酒分子结构变化的方法
CN112625851A (zh) * 2021-02-04 2021-04-09 沈阳农业大学 一种磁化催陈设备及催陈方法

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