WO2006135983A1 - Process for producing a mineral whey product - Google Patents

Process for producing a mineral whey product Download PDF

Info

Publication number
WO2006135983A1
WO2006135983A1 PCT/AU2006/000886 AU2006000886W WO2006135983A1 WO 2006135983 A1 WO2006135983 A1 WO 2006135983A1 AU 2006000886 W AU2006000886 W AU 2006000886W WO 2006135983 A1 WO2006135983 A1 WO 2006135983A1
Authority
WO
WIPO (PCT)
Prior art keywords
stream
high potassium
calcium
precipitation
whey
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/AU2006/000886
Other languages
English (en)
French (fr)
Inventor
Michael John Phillips
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Murray Goulburn Co Opeartive Co Ltd
Original Assignee
Murray Goulburn Co Opeartive Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from AU2005903308A external-priority patent/AU2005903308A0/en
Application filed by Murray Goulburn Co Opeartive Co Ltd filed Critical Murray Goulburn Co Opeartive Co Ltd
Priority to JP2008517281A priority Critical patent/JP2008543318A/ja
Priority to EP06741275A priority patent/EP1898714A4/en
Priority to NZ564364A priority patent/NZ564364A/en
Priority to AU2006252322A priority patent/AU2006252322B2/en
Priority to US11/917,952 priority patent/US20100062124A1/en
Priority to CA002612182A priority patent/CA2612182A1/en
Publication of WO2006135983A1 publication Critical patent/WO2006135983A1/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23JPROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
    • A23J3/00Working-up of proteins for foodstuffs
    • A23J3/04Animal proteins
    • A23J3/08Dairy proteins
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING OR TREATMENT THEREOF
    • A23C1/00Concentration, evaporation or drying
    • A23C1/12Concentration by evaporation
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING OR TREATMENT THEREOF
    • A23C1/00Concentration, evaporation or drying
    • A23C1/14Concentration, evaporation or drying combined with other treatment
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING OR TREATMENT THEREOF
    • A23C21/00Whey; Whey preparations
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/16Inorganic salts, minerals or trace elements
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

Definitions

  • the invention relates to the commercial processing of dairy-derived materials.
  • it relates to an improved process for the production of a relatively high potassium product derived from commercial whey.
  • a process for the production of a commercial mineral whey product derived from a feed stream of milk or whey including the steps of: primary de-mineralisation of the feed stream, preferably carried out by either membrane separation or ion exchange to produce a high potassium stream and a demineralised stream; secondary demineralisation of the high potassium stream, either by precipitation and subsequent separation of a predominantly calcium-phosphate complex, or by the removal of calcium by ion exchange; concentrating the high potassium stream to obtain a concentrate having a total solids content of around 20 to 60% by weight; and further processing of said concentrated said high potassium stream into a desired form for storage and distribution.
  • Said further processing preferably includes removal of moisture to produce a concentrate, paste or powder. It has been determined by the inventors that the above-mentioned calcium- phosphate complex is primarily responsible for the fouling problems associated with the prior art processes. An important advantage of the present invention, therefore, is that the secondary demineralisation stage removes those minerals which contribute to these fouling problems. Further, it has been found that this process step does not adversely affect the flavour profile or the functional performance of the mineral whey product produced thereby, and in fact significantly improves the solubility of the resulting mineral whey product, particularly where the calcium content of the final product is less than 0.5% by mass on a dry solids basis. This is particularly useful where the whey product is to be used as an ingredient in a food product where translucency is a desirable characteristic of the food.
  • said precipitation of the calcium-phosphate complex is achieved by heating said high potassium stream to a precipitation temperature of between 50°C and 99°C and holding said high potassium stream in that temperature range for a minimum holding time.
  • the precipitation temperature is approximately 80°C.
  • said minimum holding time of said high potassium stream at the precipitation temperature is between 2 and 60 minutes, and most preferably is approximately 20 minutes.
  • said precipitation of the calcium-phosphate complex can be further enhanced by increasing the pH of said high potassium stream to the range of pH 6.5 to 9.0, and more preferably within the range 7.0 to 7.5.
  • a non-dairy additive e.g. potassium hydroxide
  • an ion exchange process can be used instead of, or in conjunction with, the membrane demineralisation process.
  • the permeate was transferred to a reverse osmosis plant (EPIL plant; DOW Filmtec FT30 membranes) where it was concentrated to approximately 2.8% total solids.
  • EPIL plant DOW Filmtec FT30 membranes
  • the concentrated permeate was then heated to 80°C by a combination of indirect heating and direct steam injection and held for 20 minutes. This caused the precipitation of a calcium-phosphate complex from the permeate.
  • the calcium phosphate was then removed by a centrifugal separator (Westfalia Separator, model MSD-60), leaving 9,810 kg of the feed stream containing 2.7% total solids, 0.45% protein (TN x 6.38) and 1.45% minerals.
  • the calcium-phosphate could be removed from the feed stream using membrane filtration.
  • the feed stream was then concentrated to 60% total solids in a triple-effect falling film evaporator (Tetra Pak EC 500). Following concentration of this permeate, said evaporator was opened and found to be clean and free from fouling.
  • the concentrate was then spray dried to produce 251 kg of mineral whey powder.
  • the mineral whey powder contained 4.6% moisture, 15.9% protein (TN x 6.38) and 51.2% ash of which only 0.3% was calcium.
  • the powder was cooled and packed for use as an ingredient in food products.
  • This whey product is particularly suited for use as an ingredient in low-sodium food products.
  • the concentrated product ex-evaporator need not be dried to a powder for storage or transport. It is equally possible to package the concentrate as is, or to further concentrate it into a paste without departing from the invention.

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Mycology (AREA)
  • Zoology (AREA)
  • Biochemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Dairy Products (AREA)
PCT/AU2006/000886 2005-06-23 2006-06-23 Process for producing a mineral whey product Ceased WO2006135983A1 (en)

Priority Applications (6)

Application Number Priority Date Filing Date Title
JP2008517281A JP2008543318A (ja) 2005-06-23 2006-06-23 ミネラル乳清製品を製造するための方法
EP06741275A EP1898714A4 (en) 2005-06-23 2006-06-23 METHOD FOR MANUFACTURING MINERAL WHEY PRODUCT
NZ564364A NZ564364A (en) 2005-06-23 2006-06-23 Process for producing a mineral whey product
AU2006252322A AU2006252322B2 (en) 2005-06-23 2006-06-23 Process for producing a mineral whey product
US11/917,952 US20100062124A1 (en) 2005-06-23 2006-06-23 Process for Producing a Mineral Whey Product
CA002612182A CA2612182A1 (en) 2005-06-23 2006-06-23 Process for producing a mineral whey product

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
AU2005903308A AU2005903308A0 (en) 2005-06-23 Process for Producing a Mineral Whey Powder
AU2005903308 2005-06-23

Publications (1)

Publication Number Publication Date
WO2006135983A1 true WO2006135983A1 (en) 2006-12-28

Family

ID=37570040

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/AU2006/000886 Ceased WO2006135983A1 (en) 2005-06-23 2006-06-23 Process for producing a mineral whey product

Country Status (7)

Country Link
US (1) US20100062124A1 (enExample)
EP (1) EP1898714A4 (enExample)
JP (2) JP2008543318A (enExample)
AR (1) AR053934A1 (enExample)
CA (1) CA2612182A1 (enExample)
NZ (1) NZ564364A (enExample)
WO (1) WO2006135983A1 (enExample)

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL1034315C2 (nl) * 2007-08-31 2009-03-03 Tetra Laval Holdings & Finance Werkwijze voor het behandelen van zuivelproducten zoals melk, wei en/of permeaat daaruit verkregen.
DE102011002654A1 (de) * 2011-01-13 2012-07-19 Chemische Fabrik Budenheim Kg Schmelzsalzersatzmittel
EP2030512A4 (en) * 2006-06-21 2014-01-29 Adeka Corp AGENT IMPROVING AROMA
EP2745704A1 (fr) * 2012-12-21 2014-06-25 Euroserum Sel d'origine laitière riche en potassium et procédé d'obtention
WO2015119368A1 (ko) * 2013-12-06 2015-08-13 (주)한국게르마늄팜스 고농도 유기 게르마늄을 함유하는 우유 및 이의 제조방법
US9775366B2 (en) 2012-04-10 2017-10-03 Kraft Foods R & D, Inc. Process for producing cream cheese
EP3837983A1 (de) 2019-12-17 2021-06-23 DMK Deutsches Milchkontor GmbH Demineralisiertes süssmolkepulver mit erhöhtem proteingehalt
US12161132B2 (en) 2016-06-21 2024-12-10 Arla Foods Amba Process for production of improved nutritional products containing milk protein and milk saccharides, and products obtained by the process

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP6026768B2 (ja) * 2012-05-07 2016-11-16 株式会社Adeka 風味素材の製造方法及び風味改良油脂の製造方法
EP2796051B1 (de) * 2013-04-24 2018-12-26 DMK Deutsches Milchkontor GmbH Quarkgrundmasse mit verbesserten Geschmackseigenschaften
EP2839749B1 (de) * 2013-08-18 2019-01-02 DMK Deutsches Milchkontor GmbH Quarkgrundmasse mit verbesserten Geschmackseigenschaften III
GB2562711B (en) 2017-04-11 2019-07-03 Kraft Foods R & D Inc A method for the manufacture of a flavour-enhancing composition
EP3488702A1 (de) * 2017-11-23 2019-05-29 DMK Deutsches Milchkontor GmbH Verfahren zur verminderung des anfalls von mischphasen bei der konzentrierung von milchströmen

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4400315A (en) * 1983-01-21 1983-08-23 Thomas Frank A Method of removing phosphate materials from deproteinized cheese whey
US4963387A (en) * 1987-05-20 1990-10-16 Chugai Seiyaku Kabushiki Kaisha Salt substitute and foodstuffs containing same
US5185166A (en) * 1988-12-07 1993-02-09 San-Ei Chemical Industries, Ltd. Process for the production of milk mineral concentrate and drink containing minerals
US5223107A (en) * 1991-05-31 1993-06-29 Ionics, Inc. Electrodialysis method for demineralization of liquid, whey-based material
US5639501A (en) * 1995-01-31 1997-06-17 Vembu; Rajan Separation of minerals from whey permeate
US6077358A (en) * 1998-12-18 2000-06-20 Hydrite Chemical Co. Compositions and method of treatment of whey
US6399140B1 (en) * 1998-02-12 2002-06-04 Valio Ltd. Whey salt powder, process for its production and its use

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2088606A (en) * 1936-04-24 1937-08-03 David D Peebles Manufacture of stable powdered products containing milk sugar
US2465907A (en) * 1945-06-06 1949-03-29 Western Condensing Co Method of making lacteal food products
JPS49116257A (enExample) * 1973-03-12 1974-11-06
AU552141B2 (en) * 1980-11-25 1986-05-22 Unilever Plc Coluble protein product from whey
JPS60248152A (ja) * 1984-05-24 1985-12-07 Meiji Milk Prod Co Ltd 強化用カルシウム塩、その製法及び利用
JPH057474A (ja) * 1991-07-01 1993-01-19 Meiji Milk Prod Co Ltd 調味料及びその製造方法
US5707678A (en) * 1995-04-12 1998-01-13 Galagen Inc. Method for microfiltration of milk or colostral whey
AUPO821397A0 (en) * 1997-07-24 1997-08-14 Commonwealth Scientific And Industrial Research Organisation Process for the purification of nutrients from food process streams
FR2793652B1 (fr) * 1999-05-17 2001-08-10 Vidaubanaise Ingenierie Procede de traitement d'un lactoserum en vue de sa demineralisation
NZ527159A (en) * 2003-07-24 2005-10-28 Fonterra Co Operative Group Dairy product and process

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4400315A (en) * 1983-01-21 1983-08-23 Thomas Frank A Method of removing phosphate materials from deproteinized cheese whey
US4963387A (en) * 1987-05-20 1990-10-16 Chugai Seiyaku Kabushiki Kaisha Salt substitute and foodstuffs containing same
US5185166A (en) * 1988-12-07 1993-02-09 San-Ei Chemical Industries, Ltd. Process for the production of milk mineral concentrate and drink containing minerals
US5223107A (en) * 1991-05-31 1993-06-29 Ionics, Inc. Electrodialysis method for demineralization of liquid, whey-based material
US5639501A (en) * 1995-01-31 1997-06-17 Vembu; Rajan Separation of minerals from whey permeate
US6399140B1 (en) * 1998-02-12 2002-06-04 Valio Ltd. Whey salt powder, process for its production and its use
US6077358A (en) * 1998-12-18 2000-06-20 Hydrite Chemical Co. Compositions and method of treatment of whey

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
See also references of EP1898714A4 *

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2030512A4 (en) * 2006-06-21 2014-01-29 Adeka Corp AGENT IMPROVING AROMA
NL1034315C2 (nl) * 2007-08-31 2009-03-03 Tetra Laval Holdings & Finance Werkwijze voor het behandelen van zuivelproducten zoals melk, wei en/of permeaat daaruit verkregen.
DE102011002654A1 (de) * 2011-01-13 2012-07-19 Chemische Fabrik Budenheim Kg Schmelzsalzersatzmittel
US9775366B2 (en) 2012-04-10 2017-10-03 Kraft Foods R & D, Inc. Process for producing cream cheese
EP2745704A1 (fr) * 2012-12-21 2014-06-25 Euroserum Sel d'origine laitière riche en potassium et procédé d'obtention
FR2999875A1 (fr) * 2012-12-21 2014-06-27 Euroserum Sel d'origine laitiere riche en potassium et procede d'obtention
CN103960636A (zh) * 2012-12-21 2014-08-06 欧洲乳清公司 乳来源的高钾盐和其生产方法
CN103960636B (zh) * 2012-12-21 2018-02-27 欧洲乳清公司 乳来源的高钾盐和其生产方法
WO2015119368A1 (ko) * 2013-12-06 2015-08-13 (주)한국게르마늄팜스 고농도 유기 게르마늄을 함유하는 우유 및 이의 제조방법
US12161132B2 (en) 2016-06-21 2024-12-10 Arla Foods Amba Process for production of improved nutritional products containing milk protein and milk saccharides, and products obtained by the process
EP3837983A1 (de) 2019-12-17 2021-06-23 DMK Deutsches Milchkontor GmbH Demineralisiertes süssmolkepulver mit erhöhtem proteingehalt

Also Published As

Publication number Publication date
NZ564364A (en) 2011-04-29
EP1898714A1 (en) 2008-03-19
EP1898714A4 (en) 2008-09-17
JP2008543318A (ja) 2008-12-04
CA2612182A1 (en) 2006-12-28
JP2012080896A (ja) 2012-04-26
AR053934A1 (es) 2007-05-23
US20100062124A1 (en) 2010-03-11

Similar Documents

Publication Publication Date Title
JP2012080896A (ja) ミネラル乳清製品を製造するための方法
EP2986153B1 (en) Process and system for preparing dry milk formulae
AU774203B2 (en) Whey protein concentrate and method of producing the same
WO2013137714A1 (en) Process for the humanization of animal skim milk and products obtained thereby
US20240196915A1 (en) Product and method of producing dairy products comprising dairy-derived emulsifying salts
EP3046420A2 (en) Improved process for the humanization of animal skim milk
JP3236828B2 (ja) 乳カルシウム組成物
AU2006252322B2 (en) Process for producing a mineral whey product
CN106465754A (zh) 一种山羊奶脱盐乳清粉的生产方法
Dec et al. Characteristics of acid whey powder partially demineralised by nanofiltration
Chandrapala Whey wastes and powders
AU2011213773A1 (en) Process for the Preparation of a Mineral Whey Product
US20160330989A1 (en) Dairy products with reduced electrolytes and systems and methods of making same
US9854818B2 (en) Yogurt whey and method
EP4165998A1 (en) A method of producing a dry composition comprising a high amount of lactose obtained from a lactose permeate and in addition casein, composition obtained therefrom and product comprising the composition
IE20030563A1 (en) Process for preparing a milk powder
GB2404560A (en) Process for preparing a milk powder
RU2766886C1 (ru) Способ получения сухой молочной сыворотки
JPH02261343A (ja) シアル酸類を含有する脱塩濃縮乳および脱塩粉乳の調製方法
WO2022210231A1 (ja) 食品組成物の製造方法
IE20030564U1 (en) Process for preparing a milk powder
NL8600922A (nl) Werkwijze voor winning van mineralenrijke produkten uit melk.
IES20030564A2 (en) Process for preparing a milk powder
US20150208680A1 (en) Milk powders with a high whey protein index ii
IES83230Y1 (en) Process for preparing a milk powder

Legal Events

Date Code Title Description
WWE Wipo information: entry into national phase

Ref document number: 2006252322

Country of ref document: AU

ENP Entry into the national phase

Ref document number: 2006252322

Country of ref document: AU

Date of ref document: 20060623

Kind code of ref document: A

WWP Wipo information: published in national office

Ref document number: 2006252322

Country of ref document: AU

121 Ep: the epo has been informed by wipo that ep was designated in this application
WWE Wipo information: entry into national phase

Ref document number: 2006741275

Country of ref document: EP

WWE Wipo information: entry into national phase

Ref document number: 2612182

Country of ref document: CA

WWE Wipo information: entry into national phase

Ref document number: 564364

Country of ref document: NZ

WWE Wipo information: entry into national phase

Ref document number: 2008517281

Country of ref document: JP

NENP Non-entry into the national phase

Ref country code: DE

WWW Wipo information: withdrawn in national office

Country of ref document: DE

WWP Wipo information: published in national office

Ref document number: 2006741275

Country of ref document: EP

WWE Wipo information: entry into national phase

Ref document number: 11917952

Country of ref document: US