WO2004012839A1 - Procede de separation d'un melange a composants multiples et procede correspondant - Google Patents

Procede de separation d'un melange a composants multiples et procede correspondant Download PDF

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WO2004012839A1
WO2004012839A1 PCT/RU2003/000329 RU0300329W WO2004012839A1 WO 2004012839 A1 WO2004012839 A1 WO 2004012839A1 RU 0300329 W RU0300329 W RU 0300329W WO 2004012839 A1 WO2004012839 A1 WO 2004012839A1
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mixture
ρeaκtsiοnnοy
κοmποnenτοm
zone
οbοgaschennοgο
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PCT/RU2003/000329
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English (en)
Russian (ru)
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Jury Vasilievich Drobyshevsky
Sergei Nikolaevich Stolbov
Sergei Jurievich Golovchenko
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Jury Vasilievich Drobyshevsky
Sergei Nikolaevich Stolbov
Sergei Jurievich Golovchenko
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Priority to AU2003254980A priority Critical patent/AU2003254980A1/en
Publication of WO2004012839A1 publication Critical patent/WO2004012839A1/fr

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1893—Membrane reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/28—Moving reactors, e.g. rotary drums

Definitions

  • ⁇ s ⁇ ve ⁇ s ⁇ vii with u ⁇ azannym s ⁇ s ⁇ b ⁇ m is ⁇ dnuyu zhid ⁇ s ⁇ vv ⁇ dya ⁇ sve ⁇ u down ⁇ i ⁇ sevuyu ⁇ blas ⁇ ⁇ ea ⁇ tsi ⁇ nn ⁇ y z ⁇ ny, ⁇ uyu ⁇ iv ⁇ dya ⁇ v ⁇ v ⁇ aschenie, ⁇ dve ⁇ gayu ⁇ zhid ⁇ s ⁇ v ⁇ z ⁇ as ⁇ ayuschemu tsen ⁇ bezhn ⁇ mu us ⁇ eniyu and ⁇ e ⁇ emeschayu ⁇ is ⁇ dnuyu zhid ⁇ s ⁇ on ⁇ e ⁇ i ⁇ e ⁇ iyu ⁇ ea ⁇ tsi ⁇ nn ⁇ y z ⁇ ny where deys ⁇ vue ⁇ ma ⁇ simaln ⁇ e tsen ⁇ bezhn ⁇ e us ⁇ enie and where it nag ⁇ evayu ⁇
  • ⁇ ⁇ ezul ⁇ a ⁇ e nag ⁇ evaniya is ⁇ dn ⁇ y zhid ⁇ s ⁇ i ⁇ na chas ⁇ ichn ⁇ ⁇ e ⁇ b ⁇ azue ⁇ sya in ⁇ a ⁇ b ⁇ azn ⁇ e s ⁇ s ⁇ yanie and vsleds ⁇ vie ⁇ adialn ⁇ g ⁇ pressure increase ⁇ busl ⁇ vlenn ⁇ g ⁇ v ⁇ ascheniem ⁇ ea ⁇ tsi ⁇ nn ⁇ y z ⁇ ny, ⁇ a ⁇ vaya ⁇ a ⁇ tsiya ⁇ e ⁇ emeschae ⁇ sya in tsen ⁇ s ⁇ emi ⁇ eln ⁇ m na ⁇ avlenii ⁇ ⁇ i ⁇ sev ⁇ y ⁇ blas ⁇ i ⁇ ea ⁇ tsi ⁇ nn ⁇ y z ⁇ ny, ⁇ sled ⁇ va ⁇ eln ⁇ ⁇ e ⁇ d ⁇ levaya ⁇ i e ⁇ m chas ⁇ ichn
  • a device containing a drum installed with the possibility of rotation of the shaft is used.
  • the internal partly accessible walls of the indicated cam- era are made from a commercially available material, which has sizes of 6-10 times more than the length of the mixture, which is free of charge.
  • the indicated empty walls are secured by one of their own external switches on the inside of the drum or the bottom of the drum.
  • the height of the drum is less than the height.
  • the outer wall of the camcorder which is equipped with a drum, is equipped with a heating device.
  • the external drum chamber is equipped with a distributor for the quick-release fluid
  • the central internal drum is equipped with an appliance for the product
  • P ⁇ i ⁇ iv ⁇ chn ⁇ m motion is ⁇ dn ⁇ y mixture in ⁇ a ⁇ b ⁇ azn ⁇ m s ⁇ s ⁇ yanii, is ⁇ dn ⁇ y mixture in zhid ⁇ m s ⁇ s ⁇ yanii and zhid ⁇ y ⁇ legmy che ⁇ ez nasad ⁇ i v ⁇ aschayuschi ⁇ sya ⁇ ltse ⁇ b ⁇ azny ⁇ elemen ⁇ v ⁇ is ⁇ di ⁇ ne ⁇ e ⁇ yvny ⁇ bmen ⁇ m ⁇ nen ⁇ ami ⁇ a ⁇ v ⁇ y and zhid ⁇ s ⁇ n ⁇ y ⁇ az is ⁇ dn ⁇ y mixture.
  • the liquid is rich in high-leveling components, and steam is low-leveling.
  • Received products are withdrawn from the re-processing zone from the place of their formation.
  • the original mixture is heated at high pressure, excluding the formation of steam;
  • the tangible introduction of the process of the separated mixture ensures the separation of the separated mixture in the reactive zone of the rotational motion of the mixture.
  • the aforementioned device is equipped with a fixed mounted housing with a cylindrical working device.
  • the area is equipped with tangential units, which have an integral part in the form of a Laval complex.
  • the tangential parts are intended for use as a ready-to-use mixture, Laval's component ensures that the mixture is not exposed to waste.
  • the appliance is equipped with a liquid product from the factory and the gas outlet from the factory.
  • ⁇ -v ⁇ y ⁇ to increase ⁇ e ⁇ itsien ⁇ a ⁇ azdeleniya zhid ⁇ s ⁇ n ⁇ y mixture ne ⁇ b ⁇ dim ⁇ uvelichiva ⁇ s ⁇ s ⁇ ⁇ dachi in ⁇ ea ⁇ tsi ⁇ nnuyu ⁇ ame ⁇ u is ⁇ dn ⁇ y mixture ch ⁇ ⁇ iv ⁇ di ⁇ ⁇ za ⁇ a ⁇ am ene ⁇ gii on s ⁇ zdanie s ⁇ s ⁇ n ⁇ g ⁇ na ⁇ a and s ⁇ ve ⁇ s ⁇ venn ⁇ , snizhae ⁇ e ⁇ e ⁇ ivn ⁇ s ⁇ vseg ⁇ ⁇ tsessa.
  • E ⁇ a task ⁇ eshena s ⁇ zdaniem s ⁇ s ⁇ ba ⁇ azdeleniya mn ⁇ g ⁇ m ⁇ nen ⁇ ny ⁇ mixtures v ⁇ lyuchayuscheg ⁇ ⁇ mi ⁇ vanie ⁇ a ⁇ azdelyaem ⁇ y mixture ⁇ angentsialnuyu ⁇ dachu ⁇ azdelyaem ⁇ y mixture in ⁇ ea ⁇ tsi ⁇ nnuyu z ⁇ nu, d ⁇ sseli ⁇ vanie and ⁇ e ⁇ emeschenie mixture in ⁇ adialn ⁇ m na ⁇ avlenii with ⁇ b ⁇ az ⁇ vaniem gaz ⁇ b ⁇ azn ⁇ g ⁇ ⁇ du ⁇ a, ⁇ b ⁇ gaschenn ⁇ g ⁇ niz ⁇ i ⁇ yaschim ⁇ m ⁇ nen ⁇ m and zhid ⁇ g ⁇ ⁇ du ⁇ a, ⁇ b ⁇ gaschenn ⁇ g ⁇ vys ⁇ i ⁇ yaschim
  • Zhela ⁇ eln ⁇ in ⁇ aches ⁇ ve ⁇ is ⁇ g ⁇ me ⁇ all ⁇ e ⁇ amiches ⁇ g ⁇ ma ⁇ e ⁇ iala is ⁇ lz ⁇ va ⁇ me ⁇ all ⁇ e ⁇ amiches ⁇ y ma ⁇ e ⁇ ial having ⁇ is ⁇ s ⁇ ⁇ 30% and 60 d ⁇ ⁇ nitsaem ⁇ s ⁇ ⁇ d ⁇ 1000 15000 l / m 2 -a ⁇ m.-s.
  • P ⁇ s ⁇ avlennaya task ⁇ eshena ⁇ a ⁇ zhe s ⁇ zdaniem us ⁇ ys ⁇ va for ⁇ azdeleniya mn ⁇ g ⁇ m ⁇ nen ⁇ ny ⁇ mixtures s ⁇ de ⁇ zhascheg ⁇ tsilind ⁇ iches ⁇ y ⁇ us, ⁇ is ⁇ s ⁇ blenie for ⁇ dachi ⁇ azdelyaem ⁇ y mixture ⁇ is ⁇ s ⁇ blenie for vyv ⁇ da zhid ⁇ g ⁇ ⁇ du ⁇ a, ⁇ b ⁇ gaschenn ⁇ g ⁇ vys ⁇ i ⁇ yaschim ⁇ m ⁇ nen ⁇ m and ⁇ is ⁇ s ⁇ blenie for vyv ⁇ da gaz ⁇ b ⁇ azn ⁇ g ⁇ ⁇ du ⁇ a, ⁇ b ⁇ gaschenn ⁇ g ⁇ niz ⁇ i ⁇ yaschim ⁇ m ⁇ nen ⁇ m where s ⁇ glasn ⁇ iz ⁇ b ⁇ e ⁇ eniyu in ⁇
  • ch ⁇ by b ⁇ vaya s ⁇ en ⁇ a ⁇ a was vy ⁇ lnena of ⁇ is ⁇ g ⁇ me ⁇ all ⁇ e ⁇ amiches ⁇ g ⁇ ma ⁇ e ⁇ iala, ⁇ y ⁇ g ⁇ ⁇ eds ⁇ avlyayu ⁇ s ⁇ b ⁇ y ⁇ is ⁇ s ⁇ blenie for introducing the mixture into ⁇ azdelyaem ⁇ y tsen ⁇ alnuyu ⁇ ea ⁇ tsi ⁇ nnuyu ⁇ ame ⁇ u, vy ⁇ lnenn ⁇ e with v ⁇ zm ⁇ zhn ⁇ s ⁇ yu d ⁇ sseli ⁇ vaniya mixture.
  • cylindrical partial disassembled converter is made from an industrial metal material.
  • Fig. 1 schematically illustrates devices for separating a plurality of a mixture, a consensus of the invention, view of the unit;
  • Fig. 2 schematically illustrates devices for separating a plurality of a mixture, a consensus of the invention, type of mixture;
  • Fig. 2 It is a matter of inhalation of the presence of liquid in the process and the presence of a large amount of liquid in it.
  • the inventive method is related to the separation of multi-component systems, in liquid com- ponents, in various types of gases, ⁇ ⁇ sn ⁇ ve ⁇ azdeleniya mn ⁇ g ⁇ m ⁇ nen ⁇ ny ⁇ sis ⁇ em lezhi ⁇ ⁇ susches ⁇ vlenie mn ⁇ g ⁇ a ⁇ n ⁇ y chas ⁇ ichn ⁇ y ⁇ ndensatsii mn ⁇ g ⁇ m ⁇ nen ⁇ n ⁇ y mixture na ⁇ dyascheysya in ⁇ a ⁇ gaz ⁇ v ⁇ m s ⁇ s ⁇ yanii and is ⁇ a ⁇ eniya mn ⁇ g ⁇ m ⁇ nen ⁇ n ⁇ y mixture na ⁇ dyascheysya in zhid ⁇ m s ⁇ s ⁇ yanii in ⁇ ezhime in ⁇ ensivn ⁇ g ⁇ ⁇ n ⁇ a ⁇ a u ⁇ azanny ⁇ ⁇ az, d ⁇ s ⁇ igaem ⁇ g ⁇ ⁇ i i ⁇ ⁇
  • E ⁇ e ⁇ ivn ⁇ s ⁇ is ⁇ a ⁇ eniya and ⁇ ndensatsii michvanny ⁇ ⁇ az ⁇ busl ⁇ vlena s ⁇ s ⁇ yu ⁇ tsess ⁇ v mass ⁇ bmena and ⁇ e ⁇ l ⁇ bmena vesches ⁇ v, na ⁇ dyaschi ⁇ sya in ⁇ a ⁇ gaz ⁇ v ⁇ m and zhid ⁇ m s ⁇ s ⁇ yanii and zavisi ⁇ ⁇ ⁇ l ⁇ schadi ⁇ ve ⁇ n ⁇ s ⁇ ey on ⁇ y ⁇ ⁇ susches ⁇ vlyae ⁇ sya ⁇ n ⁇ a ⁇ u ⁇ azanny ⁇ ⁇ az. 10
  • a reactive zone which is used for separation of a large mixture, is divided into a transient important There is a rotation of the central re-active zone, and, therefore, the re-active zone remains stationary.
  • the original mixture in the gas and gas industry is in the process, it is predominantly flat, and the tangential it is transmitted to the environment.
  • ⁇ where ⁇ ⁇ 2 are the masses of the separable substances, ⁇ is the angular velocity of the motion of the separable substances, g 2 , g-. - initial and final radii, ⁇ - temperature, ⁇ - universal gas constant.
  • a long gas-vapor mixture in a reactive reactive zone achieves greater acceleration rates, which allows a greater degree of separation.
  • the operation is implemented due to changes in the internal energy of the gas, which is caused by the reduction of the temperature and partial compensation of the vapor phase of the mixture. With this, it turns out to be more advantageous to convert to a good phase of the high mixture ratio, that is, to remove the internal energy from the mixture from the product.
  • the first factor is the separation of the vapor-gas mixture when it is introduced, the revolving reactive zone through the above-treated metal material.
  • the first factor is the separation of the vapor-gas mixture when it is introduced, the revolving reactive zone through the above-treated metal material.
  • me ⁇ all ⁇ e ⁇ amiches ⁇ g ⁇ ma ⁇ e ⁇ iala ⁇ a ⁇ gaz ⁇ vaya mixture us ⁇ yae ⁇ sya, ⁇ ichem s ⁇ n ⁇ shenie s ⁇ s ⁇ ey on v ⁇ de and vy ⁇ de ⁇ edelyae ⁇ sya ⁇ mul ⁇ y: ⁇ 2 - ⁇ - ⁇ - ⁇ 2) + ⁇ g 2 wherein ⁇ ⁇ 2 - en ⁇ al ⁇ ii ⁇ a ⁇ gaz ⁇ v ⁇ y mixture on v ⁇ de in ⁇ is ⁇ y me ⁇ all ⁇ e ⁇ amiches ⁇ y ma ⁇ e ⁇ ial and vy ⁇ de from it.
  • P ⁇ vedennymi issled ⁇ vaniyami byl ⁇ us ⁇ an ⁇ vlen ⁇ , ch ⁇ if ⁇ u ⁇ i ⁇ a ⁇ gaz ⁇ v ⁇ g ⁇ ⁇ a, dvigayuscheg ⁇ sya ⁇ ⁇ e ⁇ i ⁇ e ⁇ ii ⁇ tsen ⁇ u ⁇ bschey ⁇ ea ⁇ tsi ⁇ nn ⁇ y z ⁇ ny, ⁇ mes ⁇ i ⁇ chas ⁇ ichn ⁇ ⁇ nitsaemuyu ⁇ e ⁇ eg ⁇ d ⁇ u, ⁇ bladayuschuyu gid ⁇ dinamiches ⁇ im s ⁇ ivleniem and vy ⁇ lnennuyu of ⁇ a ⁇ a ⁇ e ⁇ iz ⁇ vann ⁇ g ⁇ above ⁇ is ⁇ g ⁇ me ⁇ all ⁇ e ⁇ amiches ⁇ g ⁇ ma ⁇ e ⁇ iala and ⁇ susches ⁇ vlya ⁇ ⁇ i e ⁇ m d ⁇ sseli ⁇ vanie mixture, ⁇ with ⁇
  • E ⁇ e ⁇ ivn ⁇ s ⁇ is ⁇ a ⁇ eniya and ⁇ ndensatsii ⁇ busl ⁇ vlena s ⁇ s ⁇ yu ⁇ tsess ⁇ v mass ⁇ bmena and ⁇ e ⁇ l ⁇ bmena vesches ⁇ v, na ⁇ dyaschi ⁇ sya in ⁇ a ⁇ gaz ⁇ v ⁇ m and zhid ⁇ m s ⁇ s ⁇ yanii and zavisi ⁇ ⁇ ⁇ l ⁇ schadi and ⁇ ivizny ⁇ ve ⁇ n ⁇ s ⁇ ey on ⁇ y ⁇ ⁇ susches ⁇ vlyae ⁇ sya ⁇ n ⁇ a ⁇ u ⁇ azanny ⁇ ⁇ az.
  • P ⁇ vedennye issled ⁇ vaniya ⁇ azali ⁇ lezn ⁇ s ⁇ vy ⁇ lneniya chas ⁇ ichn ⁇ ⁇ nitsaemy ⁇ ⁇ e ⁇ eg ⁇ d ⁇ of ⁇ is ⁇ g ⁇ ma ⁇ e ⁇ iala, imeyuscheg ⁇ ⁇ azme ⁇ ⁇ ⁇ g ⁇ ⁇ yad ⁇ a same, and the length ch ⁇ sv ⁇ b ⁇ dn ⁇ g ⁇ ⁇ bega m ⁇ le ⁇ ul vesches ⁇ v ⁇ azdelyaem ⁇ y mn ⁇ g ⁇ m ⁇ nen ⁇ n ⁇ y mixture.
  • I - ⁇ k ⁇ " ⁇ / ( ⁇ ) 1/2 c P / s ⁇
  • ⁇ k ⁇ -! ⁇ e ⁇ itsien ⁇ ⁇ nudsen ⁇ vs ⁇ y di ⁇ uzii, ⁇ lichayuschiysya ⁇ ⁇ bychn ⁇ g ⁇ ⁇ em, ch ⁇ ⁇ l sv ⁇ b ⁇ dn ⁇ g ⁇ ⁇ bega ig ⁇ ae ⁇ diame ⁇ ⁇ ve ⁇ s ⁇ iya, ⁇ - ⁇ e ⁇ itsien ⁇ , uchi ⁇ yvayuschy diame ⁇ and ⁇ mu ⁇ ve ⁇ s ⁇ y
  • ⁇ is the molecular mass of the gas
  • ⁇ / ⁇ is the pressure gradient between the walls of the separator.
  • ⁇ a ⁇ im ⁇ b ⁇ az ⁇ m ⁇ i is ⁇ echenii ⁇ a ⁇ gaz ⁇ v ⁇ y mixture s ⁇ s ⁇ yaschey, na ⁇ ime ⁇ from dvu ⁇ vesches ⁇ v with m ⁇ le ⁇ ulya ⁇ nymi masses ⁇ , ⁇ , che ⁇ ez chas ⁇ ichn ⁇ ⁇ nitsaemuyu ⁇ e ⁇ eg ⁇ d ⁇ u, vy ⁇ lnennuyu of ⁇ is ⁇ g ⁇ me ⁇ all ⁇ e ⁇ amiches ⁇ g ⁇ ma ⁇ e ⁇ iala, bude ⁇ ⁇ is ⁇ di ⁇ its ⁇ azdelenie, ⁇ ichem e ⁇ e ⁇ ivny
  • the 1/0 separation factor will be rated ( ⁇ ⁇ / ⁇ ). It should be noted that the effective separation of the differential separation of the inlet pressure is proportional to the pressure of the gas mixture. ⁇ We declare that due to the distribution of each partial part of the process, there is a consequent reduction of pressure due to the fact that the The general coefficient of distribution of separation is equal to the production of separation of components of all partly distributed, centrally located. The results of the above studies show that this effect makes up 30% of the total separation factor.
  • ⁇ y ⁇ lnenie ⁇ is ⁇ y ⁇ ⁇ e ⁇ eg ⁇ d ⁇ , ⁇ bladayuschi ⁇ gid ⁇ dinamiches ⁇ im s ⁇ ivleniem, ⁇ a ⁇ ⁇ edlagae ⁇ sya in nas ⁇ yaschem iz ⁇ b ⁇ e ⁇ enii from ⁇ is ⁇ g ⁇ me ⁇ all ⁇ e ⁇ amiches ⁇ g ⁇ ma ⁇ e ⁇ iala ⁇ bes ⁇ echivae ⁇ ⁇ vyshenie mass ⁇ - and ⁇ e ⁇ l ⁇ bmena and uvelichivae ⁇ d ⁇ ⁇ anee not d ⁇ s ⁇ igaem ⁇ g ⁇ u ⁇ vnya e ⁇ e ⁇ ivn ⁇ s ⁇ ⁇ azdeleniya is ⁇ dn ⁇ y mixture.
  • ⁇ s ⁇ ve ⁇ s ⁇ vii with iz ⁇ b ⁇ e ⁇ eniem ⁇ eimusches ⁇ venn ⁇ is ⁇ lzuyu ⁇ me ⁇ all ⁇ e ⁇ amiches ⁇ y ma ⁇ e ⁇ ial having ⁇ is ⁇ s ⁇ , s ⁇ s ⁇ avlyayuschuyu ⁇ d ⁇ 30% 60% ⁇ nitsaem ⁇ s ⁇ , s ⁇ s ⁇ avlyayuschuyu ⁇ 1000 l / m 2 -a ⁇ m.-c d ⁇ 15000 l / m 2 -a ⁇ m.-c and us ⁇ ednenny ⁇ azme ⁇ ⁇ no more than 10 microns.
  • ⁇ a ⁇ ⁇ azali issled ⁇ vaniya ⁇ i is ⁇ lz ⁇ vanii me ⁇ all ⁇ e ⁇ amiches ⁇ g ⁇ ma ⁇ e ⁇ iala with ⁇ is ⁇ s ⁇ yu least 30% nablyudayu ⁇ vys ⁇ e s ⁇ ivlenie ⁇ e ⁇ emescheniyu ⁇ azdelyaem ⁇ y mixture and clogging ⁇ ⁇ m ⁇ nen ⁇ ami ⁇ azdelyaem ⁇ y mixture and ⁇ i is ⁇ lz ⁇ vanii me ⁇ all ⁇ e ⁇ amiches ⁇ g ⁇ ma ⁇ e ⁇ iala with ⁇ is ⁇ s ⁇ yu b ⁇ lee 60% snizhae ⁇ sya ⁇ chn ⁇ s ⁇ chas ⁇ ichn ⁇ ⁇ nitsaemy ⁇ ⁇ e ⁇ eg ⁇ d ⁇ and ⁇ as ⁇ e ⁇ ve ⁇ ya ⁇ n ⁇ s ⁇ i ⁇ ⁇ az ⁇ usheniya in ⁇ tsesse ⁇ e ⁇ emescheniya
  • ⁇ ⁇ ezul ⁇ a ⁇ e ⁇ susches ⁇ vleniya zayavlyaem ⁇ g ⁇ s ⁇ s ⁇ ba in ⁇ ea ⁇ tsi ⁇ nn ⁇ y z ⁇ ne ⁇ is ⁇ di ⁇ ⁇ b ⁇ az ⁇ vanie ⁇ du ⁇ a, ⁇ b ⁇ gaschenn ⁇ g ⁇ niz ⁇ i ⁇ yaschim ⁇ m ⁇ nen ⁇ m, imeyuscheg ⁇ gaz ⁇ b ⁇ azn ⁇ e s ⁇ s ⁇ yanie and ⁇ du ⁇ a, ⁇ b ⁇ gaschenn ⁇ g ⁇ vys ⁇ i ⁇ yaschim ⁇ m ⁇ nen ⁇ m, imeyuscheg ⁇ zhid ⁇ e s ⁇ s ⁇ yanie.
  • ⁇ b ⁇ az ⁇ vannye ⁇ du ⁇ y vyv ⁇ dya ⁇ of mes ⁇ i ⁇ ⁇ b ⁇ az ⁇ vaniya in ⁇ ea ⁇ tsi ⁇ nn ⁇ y z ⁇ ne, ⁇ i e ⁇ m gaz ⁇ b ⁇ azny niz ⁇ i ⁇ yaschy ⁇ m ⁇ nen ⁇ vyv ⁇ dya ⁇ of ⁇ i ⁇ sev ⁇ y chas ⁇ i tsen ⁇ aln ⁇ y ⁇ ea ⁇ tsi ⁇ nn ⁇ y z ⁇ ny and zhid ⁇ y vys ⁇ i ⁇ yaschy ⁇ m ⁇ nen ⁇ in v ⁇ dya ⁇ i ⁇ ⁇ e ⁇ i ⁇ e ⁇ iyn ⁇ y ⁇ ea ⁇ tsi ⁇ nn ⁇ y z ⁇ ny.
  • inventive methods for separating multi-component liquid mixtures may, of course, be available, but not necessarily be available on a separate basis.
  • the second channel has an 8 channel connected to the central 6.
  • the indicated cylinder 2 is installed in the cylinder 1 and is in conjunction with a quick one, which transfers the camera 7.
  • a side wall of 9 cylindrical housing 1 is located 10 for the delivery of a separable mixture, which has a distinctive slit-like 11 (FIG. 2) Sopel 11 (Fig. 2) ensures the delivery of the process of the separated mixture to the pre-reactive chamber 13, which is connected between the internal external part 9 18
  • a side wall 3 of process 2 has an apparatus 15 for introducing a separable mixture into a centrally separated chamber 6, which is separated by a separation unit.
  • the side wall of the 3 cylindrical unit 2 may be made from non-proprietary or partial material.
  • the mixer has
  • the proposed device for separating a multi-component mixture works as follows. ⁇ n ⁇ g ⁇ m ⁇ nen ⁇ nuyu mixture ⁇ dlelsaschuyu ⁇ azdeleniyu in ⁇ a ⁇ gaz ⁇ v ⁇ m s ⁇ s ⁇ yanii ⁇ mi ⁇ uyu ⁇ in ⁇ and ⁇ dayu ⁇ in ⁇ e ⁇ i ⁇ e ⁇ iynuyu ⁇ ea ⁇ tsi ⁇ nnuyu ⁇ ame ⁇ u 13 ⁇ as ⁇ l ⁇ zhennuyu in zaz ⁇ e between vnu ⁇ enney ⁇ ve ⁇ n ⁇ s ⁇ yu b ⁇ v ⁇ y s ⁇ en ⁇ i 9 ⁇ usa 1 us ⁇ ys ⁇ va and outer ⁇ ve ⁇ n ⁇ s ⁇ yu b ⁇ v ⁇ y s ⁇ en ⁇ i 3 eg ⁇ ⁇ a 2.
  • ⁇ s ⁇ le 11 ⁇ a ⁇ gaz ⁇ vaya mixture us ⁇ yae ⁇ sya and vy ⁇ de ⁇ mi ⁇ ue ⁇ sya in ⁇ l ⁇ s ⁇ a ⁇ allelny ⁇ , ⁇ y ⁇ angentsialn ⁇ na ⁇ avlyayu ⁇ on tsilind ⁇ iches ⁇ uyu b ⁇ vuyu s ⁇ en ⁇ u 3 ⁇ ivedenn ⁇ g ⁇ v ⁇ v ⁇ aschenie ⁇ a.
  • Reactive chamber 6 where the vapor-gas mixture keeps its rotational motion.
  • P ⁇ i e ⁇ m vys ⁇ i ⁇ yaschie ⁇ m ⁇ nen ⁇ y mixture chas ⁇ ichn ⁇ ⁇ ndensi ⁇ uyu ⁇ sya in lsid ⁇ s ⁇ and ⁇ n ⁇ y ⁇ len ⁇ y ⁇ d deys ⁇ viem tsen ⁇ bezhn ⁇ y force ⁇ as ⁇ edelyayu ⁇ sya ⁇ vnu ⁇ enney ⁇ ve ⁇ n ⁇ s ⁇ i tsilind ⁇ iches ⁇ y s ⁇ en ⁇ i 3 ⁇ a 2.
  • Pa ⁇ gaz ⁇ vaya mixture ⁇ bednennaya vys ⁇ i ⁇ yaschimi ⁇ m ⁇ nen ⁇ ami ⁇ sle di ⁇ undi ⁇ vaniya che ⁇ ez ⁇ y ⁇ e ⁇ v ⁇ y ⁇ e ⁇ eg ⁇ d ⁇ i 14, the outer ⁇ adae ⁇ ⁇ ve ⁇ n ⁇ s ⁇ v ⁇ y ⁇ e ⁇ eg ⁇ d ⁇ i 14 di ⁇ undi ⁇ ue ⁇ che ⁇ ez its ⁇ y, ch ⁇ ⁇ bes ⁇ echivae ⁇ d ⁇ lni ⁇ eln ⁇ e its d ⁇ sseli ⁇ vanie and s ⁇ ve ⁇ s ⁇ venn ⁇ , ⁇ bes ⁇ echivae ⁇ further reduction ⁇ em ⁇ e ⁇ a ⁇ u ⁇ y ⁇ a ⁇ gaz ⁇ v ⁇ y and pressure of the mixture.
  • ⁇ e ⁇ e ⁇ yvn ⁇ vv ⁇ di maya ⁇ i e ⁇ m in tsen ⁇ alnuyu ⁇ ea ⁇ tsi ⁇ nnuyu ⁇ ame ⁇ u 6 ⁇ azdelyaemaya ⁇ a ⁇ gaz ⁇ vaya mixture moving ⁇ na ⁇ avleniyu ⁇ ⁇ i ⁇ sev ⁇ y chas ⁇ i tsen ⁇ aln ⁇ y ⁇ ea ⁇ tsi ⁇ nn ⁇ y ⁇ ame ⁇ y 6 ⁇ sled ⁇ va ⁇ eln ⁇ vzaim ⁇ deys ⁇ vue ⁇ with zhid ⁇ s ⁇ yu, s ⁇ ndensi ⁇ vavsheysya on vnu ⁇ enney ⁇ ve ⁇ n ⁇ s ⁇ i tsilind ⁇ iches ⁇ y b ⁇ v ⁇ y s ⁇ en ⁇ i 3 ⁇ a 2 and vnu ⁇ enney ⁇ ve ⁇ n ⁇ s ⁇ i ⁇ azhd ⁇ y ⁇ e
  • the efficiency of the interaction of a vapor-gas mixture and a condensed liquid, and the mean separation of the mixture, is higher than the liquid film temperature by a factor of e ⁇ n ⁇ s ⁇ i ⁇ e ⁇ eg ⁇ d ⁇ 14 and vnu ⁇ enney ⁇ ve ⁇ n ⁇ s ⁇ i b ⁇ v ⁇ y s ⁇ en ⁇ i 2 and 3 ⁇ a b ⁇ lshe specific ⁇ ve ⁇ n ⁇ s ⁇ chas ⁇ ichn ⁇ ⁇ nitsaemy ⁇ tsilind ⁇ iches ⁇ i ⁇ ⁇ e ⁇ eg ⁇ d ⁇ 14.
  • P ⁇ i e ⁇ m nsid ⁇ y ⁇ du ⁇ chas ⁇ ichn ⁇ is ⁇ a ⁇ yae ⁇ sya on account ⁇ e ⁇ la ⁇ a ⁇ gaz ⁇ v ⁇ y is ⁇ dn ⁇ y mixture into said ⁇ s ⁇ u ⁇ ayuschey ⁇ e ⁇ i ⁇ e ⁇ iynuyu ⁇ ea ⁇ tsi ⁇ nnuyu ⁇ ame ⁇ u 13, which blag ⁇ da ⁇ ya zhid ⁇ y ⁇ du ⁇ d ⁇ lni ⁇ eln ⁇ ⁇ sv ⁇ b ⁇ lsdae ⁇ sya ⁇ ⁇ s ⁇ a ⁇ v niz ⁇ i ⁇ yascheg ⁇ ⁇ m ⁇ nen ⁇ a and ⁇ a ⁇ gaz ⁇ vaya is ⁇ dnaya mixture ⁇ b ⁇ gaschae ⁇ sya niz ⁇ i ⁇ yaschim 24
  • the height of the body of the device is 150 mm.
  • the diameter of the device is 300 mm.
  • the external diameter is 250 mm.
  • the number of operating hours in the operating mode is 50 Hz.
  • the linear velocity of rotation of the lateral wall of the drive is 40 m / s.
  • the speed of the flow of water from steam to the pressure sensitive reactive camera is 170 m / s.
  • Non-rusting metal is made of stainless steel, it has a share of 60%, the average size is 9 ⁇ m, 25
  • the ultimate water quality is as follows.
  • Consumables are available for use with a complimentary appliance and consumables.
  • the next year’s death, after 8, is equipped with a simple end.
  • the cross-section of the end is chosen so that the speed of the discharge of the waste of steam is more than the set speed of rotation of the rotational speed. If it falls into aperiodic reactive chamber for separating multicomponent mixtures, water turns on it.
  • the steam, purified from mixtures and removed from the device to separate the multi-component mixtures, is then condensed in the condensate.
  • Wastewater supply is 16 kg / h.
  • Pressure of water supplied by steam is 1.3 atm.
  • the pressure of a saturated vapor in a reaction chamber is 0.8 atm.
  • the pressure of the vapor at the outlet of the reaction chamber is 0.5 atm.
  • PRODUCTIVITY IS USED FOR SEPARATION OF MULTIPLE MIXTURES FOR A PURPOSE PRODUCT OF 15 KG / HOUR.
  • the calculation factor calculated on the content of calcium and lead in the source water and in the resulting target product was 2 ⁇ 0 4 , for lead it was ⁇ 0 3 .
  • the proposed devices are used for the separation of multi-functional mixtures with the following products.
  • the height of the body is 150 mm.
  • the diameter of the device is 300 mm.
  • the external diameter is 250 mm. Height - 110 mm.
  • a centrally operating chamber in the case of a metal and ceramic components that are cylindrical inverted, they have a diameter of 21 mm, they are 22 mm, they are 22 mm, The number of operating hours in the operating mode is 50 Hz.
  • the linear velocity of rotation of the lateral wall of the drive is 40 m / s. 27
  • the flow rate of the waste water-alcohol mixture from sperm to the pressure-sensitive zone is 120 m / s.
  • Each metal recirculating device is made of nickel, has an output of - 40%, the average size is 6 mkm, a little 2- minute - a little 2 mn.
  • the alcohol is purified from water and removed from the device for the separation of multicomponent mixtures, then it is condensed in the condensate.
  • the yield of a generous mixture is 28 kg / hour.
  • the pressure of the supplied mixture is 1.0 atm.
  • the pressure of the vapor mixture in the reaction chamber is 0.5 atm. 28
  • the pressure of the consumer product at the outlet of the device is 0.25 atm.
  • the number of operating hours in the operating mode is 60 Hz.
  • the concentration of alcohol in the original mixture is 15%.
  • the concentration of alcohol in the target product is 96%.
  • the diameter of the device is 300 mm.
  • the height of the body is 150 mm.
  • the external diameter is 250 mm. Height - 110 mm.
  • the diameter of the brightest side wall of the vessel is 23 mm.
  • Each metal recirculating appliance is made from titanium, has a surplus of -30%, the average size is about 6 mkm, apart from the industrial unit, it is 1000 meters apart.
  • the pressure of the saturated saturated vapor in the vaporized reactive chamber is 0.35 atm.
  • the vapor pressure in the central part of the central reaction chamber is 0.12 atm.
  • the waste of saturated steam is 10 kg / hour.
  • the number of operating times in the operating mode is 100 Hz.
  • the linear velocity of rotation of the lateral wall of the drive is 79 m / s.
  • the rate of exhaustion of saturated steam from sapl to aperiodic reactive camera is 250 m / s.
  • the operating mode is water-conditioned with an operating speed of 50% ( ⁇ issue - one particle per million).
  • the content of the action in the source water is 140%.
  • the calculation factor is 2.8.
  • v ⁇ zni ⁇ ae ⁇ ne ⁇ b ⁇ dim ⁇ s ⁇ in ⁇ azdelenii mn ⁇ g ⁇ m ⁇ nen ⁇ ny ⁇ sis ⁇ em, na ⁇ ime ⁇ , zhid ⁇ s ⁇ -gas zhid ⁇ s ⁇ - zhid ⁇ s ⁇ gas- ⁇ a ⁇ in ⁇ m including ⁇ i capture mel ⁇ dis ⁇ e ⁇ sny ⁇ ae ⁇ z ⁇ ley, ⁇ b ⁇ azuyuschi ⁇ sya in ⁇ ezul ⁇ a ⁇ e vzaim ⁇ deys ⁇ viya ⁇ imiches ⁇ i ⁇ vesches ⁇ v with moisture.

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)

Abstract

Le procédé de séparation d'un mélange à composants multiples comprend une première détente du mélange gaz / vapeur lors de l'alimentation tangentielle du mélange ainsi formé dans la zone de réaction périphérique, une deuxième détente du mélange lors de l'injection d'un flux rotatif de mélange depuis la zone périphérique dans la zone de réaction centrale rotative, accompagnée de la formation à la frontière des zones de réaction d'une couche du produit liquide enrichi par un composant à point d'ébullition élevé, sur les surfaces d'au moins une séparation partiellement perméable (14) disposée dans la zone de réaction rotative. Le dispositif de l'invention comprend un boîtier (1) dans lequel se trouve une chambre de réaction périphérique (13), un rotor (2) avec une chambre de réaction centrale (6), un accessoire (10) pour alimenter le mélange à séparer qui se présente comme une buse en fente (11) permettant la détente du mélange et un accessoire (18) de sortie du produit liquide enrichi du composant à point d'ébullition élevé. Le rotor est muni d'un accessoire (15) destiné à l'introduction du mélange à séparer dans la chambre de réaction centrale (6) permettant la détente du liquide, au moins une séparation cylindrique montée coaxialement (14) faite de manière à permettre la détente du mélange et un accessoire (18) destiné à l'évacuation du produit liquide enrichi du composant à point d'ébullition élevé depuis la chambre de réaction centrale (6) vers la chambre de réaction périphérique (13).
PCT/RU2003/000329 2002-08-02 2003-07-24 Procede de separation d'un melange a composants multiples et procede correspondant WO2004012839A1 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
AU2003254980A AU2003254980A1 (en) 2002-08-02 2003-07-24 Method for dividing multicomponent mixture and device for carrying out said method

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
RU2002120533 2002-08-02
RU2002120533A RU2206388C1 (ru) 2002-08-02 2002-08-02 Способ разделения многокомпонентной смеси и устройство для его осуществления

Publications (1)

Publication Number Publication Date
WO2004012839A1 true WO2004012839A1 (fr) 2004-02-12

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AU (1) AU2003254980A1 (fr)
RU (1) RU2206388C1 (fr)
WO (1) WO2004012839A1 (fr)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EA029322B1 (ru) * 2014-05-25 2018-03-30 Николае Лаповщук Способ разделения гомогенной жидкой смеси и устройство для его осуществления
RU2567612C1 (ru) * 2014-07-25 2015-11-10 Юрий Васильевич Дробышевский Способ разделения многокомпонентной смеси и устройство для его осуществления

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4382900A (en) * 1980-09-01 1983-05-10 Imperial Chemical Industries Plc Centrifugal gas-liquid contact apparatus
SU1274708A1 (ru) * 1985-02-21 1986-12-07 Предприятие П/Я Р-6956 Аппарат дл разделени газожидкостных смесей
US4666564A (en) * 1984-04-21 1987-05-19 Fried. Krupp Gesellschaft Mit Beschrankter Haftung Method of and apparatus for distilling a monoazeotropic liquid mixture
RU2055628C1 (ru) * 1991-08-14 1996-03-10 Александр Нинельевич Лукьянов Способ центробежной ректификации и устройство для его осуществления

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4382900A (en) * 1980-09-01 1983-05-10 Imperial Chemical Industries Plc Centrifugal gas-liquid contact apparatus
US4666564A (en) * 1984-04-21 1987-05-19 Fried. Krupp Gesellschaft Mit Beschrankter Haftung Method of and apparatus for distilling a monoazeotropic liquid mixture
SU1274708A1 (ru) * 1985-02-21 1986-12-07 Предприятие П/Я Р-6956 Аппарат дл разделени газожидкостных смесей
RU2055628C1 (ru) * 1991-08-14 1996-03-10 Александр Нинельевич Лукьянов Способ центробежной ректификации и устройство для его осуществления

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RU2206388C1 (ru) 2003-06-20
AU2003254980A1 (en) 2004-02-23

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