WO2003046245A3 - Procede de fabrication de paillettes a l'echelle de l'angstrom fonctionnelles et de bel aspect - Google Patents

Procede de fabrication de paillettes a l'echelle de l'angstrom fonctionnelles et de bel aspect Download PDF

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Publication number
WO2003046245A3
WO2003046245A3 PCT/US2002/038292 US0238292W WO03046245A3 WO 2003046245 A3 WO2003046245 A3 WO 2003046245A3 US 0238292 W US0238292 W US 0238292W WO 03046245 A3 WO03046245 A3 WO 03046245A3
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WO
WIPO (PCT)
Prior art keywords
vacuum
flakes
chamber
vapor
release
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Application number
PCT/US2002/038292
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English (en)
Other versions
WO2003046245A2 (fr
Inventor
Karl Josephy
James P Rettker
Howard H Enlow
Original Assignee
Avery Dennison Corp
Karl Josephy
James P Rettker
Howard H Enlow
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Avery Dennison Corp, Karl Josephy, James P Rettker, Howard H Enlow filed Critical Avery Dennison Corp
Priority to KR10-2004-7008262A priority Critical patent/KR20040068564A/ko
Priority to JP2003547673A priority patent/JP2005510629A/ja
Priority to CA002467912A priority patent/CA2467912A1/fr
Priority to EP02799891A priority patent/EP1453987A2/fr
Priority to AU2002364515A priority patent/AU2002364515A1/en
Publication of WO2003046245A2 publication Critical patent/WO2003046245A2/fr
Publication of WO2003046245A3 publication Critical patent/WO2003046245A3/fr

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    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/65—Additives macromolecular
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/02—Making metallic powder or suspensions thereof using physical processes
    • B22F9/12—Making metallic powder or suspensions thereof using physical processes starting from gaseous material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/0015—Pigments exhibiting interference colours, e.g. transparent platelets of appropriate thinness or flaky substrates, e.g. mica, bearing appropriate thin transparent coatings
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/0015—Pigments exhibiting interference colours, e.g. transparent platelets of appropriate thinness or flaky substrates, e.g. mica, bearing appropriate thin transparent coatings
    • C09C1/0018—Pigments exhibiting interference colours, e.g. transparent platelets of appropriate thinness or flaky substrates, e.g. mica, bearing appropriate thin transparent coatings uncoated and unlayered plate-like particles
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/62—Metallic pigments or fillers
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/0005—Separation of the coating from the substrate
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/24—Vacuum evaporation
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/56—Apparatus specially adapted for continuous coating; Arrangements for maintaining the vacuum, e.g. vacuum locks
    • C23C14/562—Apparatus specially adapted for continuous coating; Arrangements for maintaining the vacuum, e.g. vacuum locks for coating elongated substrates
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/56—Apparatus specially adapted for continuous coating; Arrangements for maintaining the vacuum, e.g. vacuum locks
    • C23C14/568—Transferring the substrates through a series of coating stations
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2998/00—Supplementary information concerning processes or compositions relating to powder metallurgy
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/20—Particle morphology extending in two dimensions, e.g. plate-like
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/01—Use of inorganic substances as compounding ingredients characterized by their specific function
    • C08K3/013—Fillers, pigments or reinforcing additives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/34—Silicon-containing compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K7/00—Use of ingredients characterised by shape
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2210/00—Special effects or uses of interference pigments
    • C09C2210/30—A layer or the substrate forming a grating
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2210/00—Special effects or uses of interference pigments
    • C09C2210/40—Embossed layers
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2220/00—Methods of preparing the interference pigments
    • C09C2220/20—PVD, CVD methods or coating in a gas-phase using a fluidized bed

Abstract

L'invention porte sur un procédé économique et à fort débit de fabrication de paillettes fonctionnelles ou décoratives consistant à appliquer des empilements de couches alternées de métal et d'anti-adhérent sur un tambour tournant refroidi ou sur tout support adapté placé dans une chambre d'évaporation sous vide. Les couches de métal sont déposées par évaporation sous vide et les couches intercalaires, faites de préférence d'un thermoplastique soluble dans un solvant ou de polymères faiblement réticulés, le sont par évaporation sous vide de sources placées dans la chambre. L'empilement est alors retiré du tambour puis traité par un solvant organique adapté qui dissout l'anti-adhérent dans un processus d'extraction qui laisse les paillettes métalliques quasiment exemptes d'anti-adhérent. Le solvant et l'anti-adhérent sont alors extraits par centrifugation ce qui laisse un gâteau de paillettes concentrées qu'on peut désagréger à l'air puis décharger sur un moyen de transport et calibrer et homogénéiser pour ses utilisations finales dans des encres, des peintures ou des revêtements. Dans une exécution les paillettes peuvent provenir de couches uniques de métal ou d'alliage métalliques, ou de matériaux minéraux; dans une autre exécution elles peuvent être revêtues des deux côtés de couches protectrices de polymères appliquées à partir de sources appropriées placées dans la chambre d'évaporation. L'anti-adhérent peut être fait d'un polymère réticulable et durcissable sous l'effet de rayonnements, à faible densité de réticulation, déposé par évaporation. L'exposition à des rayons de forte énergie réticule suffisamment l'anti-adhérent pour produire des couches solubles sensiblement non collantes. Dans une exécution l'empilement est accumulé sur un convoyeur sans fin traversant la chambre d'évaporation et une cloison étanche la séparant de la chambre d'extraction, les deux chambres étant en dépression lors de la décharge des paillettes sur le convoyeur. Pour prélever périodiquement le dépôt, on réduit la vitesse du convoyeur, on ralentit les sources de dépôt de la chambre, et on place un dispositif de recueil des vapeurs de dépôt, dans la chambre d'extraction, sous le convoyeur après interposition de cloisons étanches qui maintiennent la chambre d'extraction en dépression pendant le prélèvement sur le convoyeur du matériau déposé par évaporation sous vide.
PCT/US2002/038292 2001-11-29 2002-11-27 Procede de fabrication de paillettes a l'echelle de l'angstrom fonctionnelles et de bel aspect WO2003046245A2 (fr)

Priority Applications (5)

Application Number Priority Date Filing Date Title
KR10-2004-7008262A KR20040068564A (ko) 2001-11-29 2002-11-27 옹스트롬 크기의 높은 애스펙트 비를 가진 기능성 미소플레이트의 제조 방법
JP2003547673A JP2005510629A (ja) 2001-11-29 2002-11-27 オングストロームスケール及び高アスペクト機能性小板の製造方法
CA002467912A CA2467912A1 (fr) 2001-11-29 2002-11-27 Procede de fabrication de paillettes a l'echelle de l'angstrom fonctionnelles et de bel aspect
EP02799891A EP1453987A2 (fr) 2001-11-29 2002-11-27 Procede de fabrication de paillettes a l'echelle de l'angstrom fonctionnelles et de bel aspect
AU2002364515A AU2002364515A1 (en) 2001-11-29 2002-11-27 Process for making angstrom scale and high aspect functional platelets

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US33426001P 2001-11-29 2001-11-29
US60/334,260 2001-11-29

Publications (2)

Publication Number Publication Date
WO2003046245A2 WO2003046245A2 (fr) 2003-06-05
WO2003046245A3 true WO2003046245A3 (fr) 2004-02-12

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PCT/US2002/038292 WO2003046245A2 (fr) 2001-11-29 2002-11-27 Procede de fabrication de paillettes a l'echelle de l'angstrom fonctionnelles et de bel aspect

Country Status (8)

Country Link
EP (1) EP1453987A2 (fr)
JP (1) JP2005510629A (fr)
KR (1) KR20040068564A (fr)
CN (1) CN100354451C (fr)
AU (1) AU2002364515A1 (fr)
CA (1) CA2467912A1 (fr)
MX (1) MXPA04005106A (fr)
WO (1) WO2003046245A2 (fr)

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BRPI0607670A2 (pt) * 2005-04-26 2009-09-22 Avery Dennison Corp processo para produção de flocos metálicos finos de partìculas finas realçadas que têm brilho e intensidade de cor, processo de formação de um primeiro revestimento que contém flocos realçados, flocos metálicos refletores, laminado de múltiplas camadas e revestimento resinoso
DE602006020761D1 (de) * 2005-11-17 2011-04-28 Basf Se Verfahren zur herstellung von schuppenförmigen partikeln
WO2007093401A2 (fr) 2006-02-14 2007-08-23 Eckart Gmbh Pigments à effet métallique foncés produits au moyen d'un procédé de dépôt physique en phase vapeur
KR20100024295A (ko) 2008-08-25 2010-03-05 주식회사 잉크테크 금속박편의 제조방법
JP5705129B2 (ja) * 2008-12-19 2015-04-22 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ 薄アルミニウムフレーク
PL2504400T3 (pl) 2009-11-27 2018-02-28 Basf Se Kompozycje powłokowe do elementów zabezpieczających i hologramów
JP2012140692A (ja) * 2011-01-06 2012-07-26 Oike Ind Co Ltd 金属超微粉体
JP2013040357A (ja) * 2011-08-11 2013-02-28 Optorun Co Ltd 成膜装置
CN102989998B (zh) * 2012-12-25 2014-10-29 常州大学 一种利用物质熔化和升华及汽化吸热的激冷醇基涂料
WO2015122632A1 (fr) * 2014-02-12 2015-08-20 이형곤 Système de fabrication d'un agrégat à film mince, agrégat à film mince, film mince, agent protecteur anti-uv et produits cosmétiques
WO2017015006A1 (fr) * 2015-07-17 2017-01-26 3M Innovative Properties Company Compositions comprenant des microsphères en céramique
KR101856623B1 (ko) * 2016-08-12 2018-05-10 주식회사 테토스 반사성 입자의 스퍼터링 방법
JP2020079368A (ja) * 2018-11-14 2020-05-28 トヨタ自動車株式会社 光輝性顔料およびその製造方法
CN109576454A (zh) * 2018-12-19 2019-04-05 深圳先进技术研究院 金属纳米片的制备方法、金属纳米片、用途和负极活性材料
DE102019005456A1 (de) * 2019-08-02 2021-02-04 Giesecke+Devrient Currency Technology Gmbh Verfahren zum Herstellen von Effektpigmenten

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EP0081599A1 (fr) * 1981-12-10 1983-06-22 Revlon, Inc. Procédé de fabrication de pigments métalliques pelliculants
EP0227423A2 (fr) * 1985-12-23 1987-07-01 Flex Products, Inc. Lamelles optiques en film mince, revêtement optique par réplique, revêtements et encres contenant ces lamelles et procédé
WO1994016022A1 (fr) * 1993-01-14 1994-07-21 Carl Schlenk Aktiengesellschaft Procede de fabrication de pigments dores ou argentes ou de pigments d'autres couleurs
WO2000024946A1 (fr) * 1998-10-23 2000-05-04 Avery Dennison Corporation Procede de fabrication de paillettes metalliques
US6270840B1 (en) * 1998-09-28 2001-08-07 Weinert Vakuum Verfahrenstechnik Gmbh Apparatus and method for producing plane-parallel flakes

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JP2005510629A (ja) 2005-04-21
EP1453987A2 (fr) 2004-09-08
AU2002364515A1 (en) 2003-06-10
CN100354451C (zh) 2007-12-12
WO2003046245A2 (fr) 2003-06-05
CN1596322A (zh) 2005-03-16
MXPA04005106A (es) 2004-08-19
CA2467912A1 (fr) 2003-06-05
KR20040068564A (ko) 2004-07-31

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