WO2003045164A1 - Procede de fabrication de pectine - Google Patents

Procede de fabrication de pectine Download PDF

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Publication number
WO2003045164A1
WO2003045164A1 PCT/RU2001/000511 RU0100511W WO03045164A1 WO 2003045164 A1 WO2003045164 A1 WO 2003045164A1 RU 0100511 W RU0100511 W RU 0100511W WO 03045164 A1 WO03045164 A1 WO 03045164A1
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WO
WIPO (PCT)
Prior art keywords
pectin
liquid phase
separation
liquid
extraction
Prior art date
Application number
PCT/RU2001/000511
Other languages
English (en)
Russian (ru)
Inventor
Vladimir Nikolaevich Golubev
Original Assignee
Vladimir Nikolaevich Golubev
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Vladimir Nikolaevich Golubev filed Critical Vladimir Nikolaevich Golubev
Priority to AU2002243118A priority Critical patent/AU2002243118A1/en
Priority to PCT/RU2001/000511 priority patent/WO2003045164A1/fr
Publication of WO2003045164A1 publication Critical patent/WO2003045164A1/fr

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
    • C08B37/0006—Homoglycans, i.e. polysaccharides having a main chain consisting of one single sugar, e.g. colominic acid
    • C08B37/0045—Homoglycans, i.e. polysaccharides having a main chain consisting of one single sugar, e.g. colominic acid alpha-D-Galacturonans, e.g. methyl ester of (alpha-1,4)-linked D-galacturonic acid units, i.e. pectin, or hydrolysis product of methyl ester of alpha-1,4-linked D-galacturonic acid units, i.e. pectinic acid; Derivatives thereof
    • C08B37/0048—Processes of extraction from organic materials
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
    • A23L29/20—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents
    • A23L29/206—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of vegetable origin
    • A23L29/231—Pectin; Derivatives thereof

Definitions

  • the invention is concerned with the technology of extracting pectin from a plant raw material, which may be used in the food industry only.
  • Pectin provides a high, high molecular weight polysaccharide, which is part of the cell walls and cellulose cellulose, and cellulose. The largest quantity of pectin is found in food and non-food products. ⁇ ⁇ ischev ⁇ y ⁇ myshlenn ⁇ s ⁇ i ⁇ e ⁇ in ⁇ luchayu ⁇ , ⁇ eimusches ⁇ venn ⁇ from yabl ⁇ chny ⁇ or tsi ⁇ us ⁇ vy ⁇ vyzhim ⁇ , sve ⁇ l ⁇ vichn ⁇ g ⁇ zh ⁇ ma, ⁇ zin ⁇ ⁇ ds ⁇ lnechni ⁇ a, ⁇ d ⁇ v ⁇ e ⁇ e ⁇ ab ⁇ i bel ⁇ achann ⁇ y ⁇ a ⁇ us ⁇ y and ⁇ m ⁇ v ⁇ g ⁇ a ⁇ buza.
  • the cooked foods are used for making homemade jellies, pastes and pastries.
  • the pectin is also referred to as a bakery and a dairy industry.
  • the closest is the method of receiving the pectin in the feed to the hydraulics-extracting feeds of the non-consuming unit.
  • the hydrolysis is carried out by means of cavitational processing of raw materials and water with a mixture of 2–4 and a mixture of 1: (5–8) and 0.2 sec. After this pulp is divided into liquid and solid phases in the course of the action of the central military forces and the fact
  • the basic task of the invention is to work out the methods for converting a product with high quality indicators. With this expected technical result, there is an increase in the output of the target product, which has a high gelling opportunity from the general operation of the transmission.
  • the expected technical result is achieved due to the fact that in the process of production of the pectin, which includes the hydrolysis of the mixture of the feeds of the raw material and the source of food
  • Drying which is carried out at a temperature of 50-65 ° C by spraying the concentrate with the use of ultrasonic extraction, is 100% emitted.
  • pectin substances by orienting itself with this water molecule from the external part of the pectin core. In fact, the molecule itself
  • the method is as follows.
  • Pe ⁇ ins ⁇ de ⁇ zhaschee sy ⁇ e in ⁇ aches ⁇ ve ⁇ g ⁇ is ⁇ lzuyu ⁇ , ⁇ eimusches ⁇ venn ⁇ , fresh ⁇ e ⁇ ins ⁇ de ⁇ zhaschee sy ⁇ e, na ⁇ ime ⁇ , tsi ⁇ us ⁇ vye and / or yabl ⁇ chnye vyzhim ⁇ i or ⁇ m ⁇ v ⁇ y a ⁇ buz or sve ⁇ l ⁇ vichny zh ⁇ m or ⁇ dy ⁇ ⁇ e ⁇ e ⁇ ab ⁇ i ⁇ a ⁇ us ⁇ y ⁇ eleva ⁇ u na ⁇ avlyayu ⁇ in bun ⁇ e ⁇ where ⁇ is ⁇ di ⁇ eg ⁇ na ⁇ lenie ⁇ e ⁇ ed ⁇ avi ⁇ atsi ⁇ nnym e ⁇ s ⁇ a ⁇ m.
  • the product-containing raw materials can be further grinded.
  • the raw material is mixed with the raw material 2–4 and the mixture hydraulics mixture 1: (3–4).
  • the resulting mixture is treated with a cavitating process in the chamber of the hydro- acoustic treatment of the pressure of 0.2–1.5 sec. ⁇ hab
  • the result of cavitation processing is the process of the hydrolysis-extraction of pectin raw materials.
  • ultrafiltration membranes use a solid or dacron base. In the case of ultrafiltration membranes on a solid one, you can use the membranes “Politimersynthesis” or the “ ⁇ ”, “ ⁇ ”, or others.
  • Drying of pectin concentrate is carried out to the humidity of the finished pectin at no more than 8% at a temperature of 50-65 ° C using. Ultrasound pho rsuns.
  • Received pulses are delivered to the central pump in an intermediate capacity, where it is connected to a central unit where there is a separation of a liquid and a gas separator.
  • P ⁇ luchennaya ⁇ e ⁇ in ⁇ s ⁇ de ⁇ z haschaya ⁇ a ⁇ tsiya with s ⁇ de ⁇ zhaniem ⁇ ve ⁇ dy ⁇ suspensions not b ⁇ lee 0.1% ⁇ dae ⁇ sya with ⁇ m ⁇ schyu tsen ⁇ bezhn ⁇ g ⁇ nas ⁇ sa in ⁇ mezhu ⁇ chnuyu em ⁇ s ⁇ and ⁇ s ⁇ u ⁇ ae ⁇ on ul ⁇ a ⁇ il ⁇ atsiyu in a ⁇ a ⁇ a ⁇ with memb ⁇ anami U ⁇ P-P s ⁇ s ⁇ s ⁇ yu ⁇ a ⁇ as ⁇ v ⁇ a 0.1 m / s, a pressure of 0.05 ⁇ i ⁇ ab ⁇ chem ⁇ Pa.
  • a concentrate of pesticides is reached up to 3.5% for pesticides.
  • the drying process is carried out at a temperature of 50 ° C by spraying the concentrate using an ultrasonic spray.
  • the end product is a dry product with a moisture content of 8%, light and light color, which has a mass of 106,000 units, which is 360%.
  • the degree of extraction of pectin substances from the original raw materials is 98%.
  • Received pulses are received by the centrifugal pump in the intermediate capacity, where it is located in the center where the separation of the process and the liquid is carried out.
  • P ⁇ luchennaya ⁇ e ⁇ ins ⁇ de ⁇ z haschaya ⁇ a ⁇ tsiya with s ⁇ de ⁇ zhaniem ⁇ ve ⁇ dy ⁇ suspensions not b ⁇ lee 0.1% ⁇ dae ⁇ sya with ⁇ m ⁇ schyu tsen ⁇ bezhn ⁇ g ⁇ nas ⁇ sa in ⁇ mezhu ⁇ chnuyu em ⁇ s ⁇ and ⁇ s ⁇ u ⁇ ae ⁇ on ul ⁇ a ⁇ il ⁇ atsiyu in a ⁇ a ⁇ a ⁇ with memb ⁇ anami U ⁇ P-P s ⁇ s ⁇ s ⁇ yu ⁇ a ⁇ as ⁇ v ⁇ a 1.2 m / s, a pressure of 0.25 ⁇ i ⁇ ab ⁇ chem In the process of ultrafiltration, a concentrate of pesticides is reached up to 4.4% for non-processed substances.
  • the end product is a dry product with a moisture content of 8%, light and light color, which has a mass of 85,000 units, which is an absolute increase of 240%.
  • the degree of extraction of pectin substances from the original raw materials is 98%.
  • EXAMPLE 3 Production of a pectin from a merchant watermelon.
  • Received pulses are received by the centrifugal pump in the intermediate tank, where it is located in the center where there is a separation of the liquid and the gas separator.
  • Received product-containing fraction with a suspension of suspended solids of not more than 0.1%, is delivered with the help of a centrifugal pump in 12
  • the end product is a dry product with a moisture content of 8%, light and light color, which has a mass of 68,000 units, which is 210% pure.
  • the degree of extraction of pectin substances from the original raw materials is 98%.
  • the received pulse is delivered to the centrifugal pump at an intermediate capacity, where it is disposed of to the center where the separation of the liquid and the liquid is carried out.
  • P ⁇ luchennaya ⁇ e ⁇ ins ⁇ de ⁇ z haschaya ⁇ a ⁇ tsiya with s ⁇ de ⁇ zhaniem ⁇ ve ⁇ dy ⁇ suspensions not b ⁇ lee 0.1% ⁇ dae ⁇ sya with ⁇ m ⁇ schyu tsen ⁇ bezhn ⁇ g ⁇ nas ⁇ sa in ⁇ mezhu ⁇ chnuyu em ⁇ s ⁇ and ⁇ s ⁇ u ⁇ ae ⁇ on ul ⁇ a ⁇ il ⁇ atsiyu in a ⁇ a ⁇ a ⁇ with memb ⁇ anami U ⁇ P-P s ⁇ s ⁇ s ⁇ yu ⁇ a ⁇ as ⁇ v ⁇ a 1.5 m / s, a pressure of 0.3 ⁇ i ⁇ ab ⁇ chem ⁇ Pa.
  • the concentrate of the electronic product is reached up to 4.0% for the non-hazardous substances.
  • the end product is a dry product with a moisture content of 8%, light and light color, which has a molecular weight of 32,000 units, which is 180%.
  • the degree of extraction of pectin substances from the original raw materials is 96%.
  • Example 5 Production of a pectin from a tambourine.
  • P ⁇ luchennaya ⁇ e ⁇ ins ⁇ de ⁇ z haschaya ⁇ a ⁇ tsiya with s ⁇ de ⁇ zhaniem ⁇ ve ⁇ dy ⁇ suspensions not b ⁇ lee 0.1% ⁇ dae ⁇ sya with ⁇ m ⁇ schyu tsen ⁇ bezhn ⁇ g ⁇ nas ⁇ sa in ⁇ mezhu ⁇ chnuyu em ⁇ s ⁇ and ⁇ s ⁇ u ⁇ ae ⁇ on ul ⁇ a ⁇ il ⁇ atsiyu in a ⁇ a ⁇ a ⁇ with memb ⁇ anami U ⁇ P-P s ⁇ s ⁇ s ⁇ yu ⁇ a ⁇ as ⁇ v ⁇ a 0.3 m / s, a pressure of 0.31 ⁇ i ⁇ ab ⁇ chem ⁇ Pa .
  • the concentrate of pesticides is reached up to 3.8% for nonprocess substances.
  • the resulting concentrate is further released into the drying unit, and the drying process is carried out at a
  • the end product is a dry product with a moisture content of 8%, a bright and light color, which has a mass of 64,000 units, is an increase of 230%.
  • the degree of extraction of pectin substances from the original raw materials is 96%.
  • EXAMPLE 6 Production of pectin from operating conditions. 100 kg of fresh presses of capacities are put in the tank - a hydraulic module, add 400 liters of drinking water, with ⁇ 3 (hydraulic module 1: 4) and a power supply fifteen
  • Received pulses are received by the centrifugal pump in the intermediate tank, where it is removed from the process, where there is a separation of the liquid and the gas separator.
  • P ⁇ luchennaya ⁇ e ⁇ ins ⁇ de ⁇ z haschaya ⁇ a ⁇ tsiya with s ⁇ de ⁇ zhaniem ⁇ ve ⁇ dy ⁇ suspensions not b ⁇ lee 0.1% ⁇ dae ⁇ sya with ⁇ m ⁇ schyu tsen ⁇ bezhn ⁇ g ⁇ nas ⁇ sa in ⁇ mezhu ⁇ chnuyu em ⁇ s ⁇ and ⁇ s ⁇ u ⁇ ae ⁇ on ul ⁇ a ⁇ il ⁇ atsiyu in a ⁇ a ⁇ a ⁇ with memb ⁇ anami U ⁇ P-P s ⁇ s ⁇ s ⁇ yu ⁇ a ⁇ as ⁇ v ⁇ a 0.8 m / s, a pressure of 0.25 ⁇ i ⁇ ab ⁇ chem ⁇ Pa.
  • the concentrate of the electronic product is reached up to 3.7% for the non-hazardous substances.
  • the end product is a dry product with a moisture content of 8%, light and light color, which has a molecular weight of 48,000 units, which is an increase of 230%.
  • the degree of extraction of pectin substances from the original raw materials is 98%.
  • the present invention may be used on a large scale for the purpose of producing a pectin with a high gellant supply.

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Polymers & Plastics (AREA)
  • General Health & Medical Sciences (AREA)
  • Food Science & Technology (AREA)
  • Nutrition Science (AREA)
  • Dispersion Chemistry (AREA)
  • Molecular Biology (AREA)
  • Biochemistry (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

L'invention concerne une technologie d'extraction de pectine à partir de matières premières végétales, qui peut s'utiliser en industrie alimentaire. Le procédé de fabrication de pectine comprend l'extraction par hydrolyse des matières premières contenant de la pectine, avec un hydromodule du mélange de 1: (3-4) au moyen du traitement par cavitation avec un indice de cavitation 0,2 - 1,9 du mélange des matières premières contenant de la pectine et de l'eau à pH 2-4 pendant 15-25 min. et une surpression de 0,41 - 0,45 MPa dans la chambre d'extraction de l'extracteur - désintégrateur. On sépare ensuite la pulpe obtenue en phases solide et liquide dans le champ d'action des forces centrifuges, avec un facteur de séparation de Fr 110-130, jusqu'à ce que la teneur en suspensions solides en phase liquide s'élève à 0,1 % de sa masse au maximum. La concentration de la phase liquide se fait par ultrafiltrage, sous une pression de 0,05 - 0,31 MPa, au moyen de membranes d'ultrafiltrage sur substrat solide et un diamètre de pores de (1-10)10-9m et un débit de circulation de la phase liquide de 0,1 - 2,0 m/s, jusqu'à ce que le concentré final contienne 4,4 % de substance de pectine au maximum. Le séchage du concentré se fait par pulvérisation à une température de 50-65 °C, en utilisant des buses ultrasonores. L'invention permet d'augmenter la sortie du produit fini qui possède une capacité gélifiante élevée, avec une intensification globale du procédé de fabrication.
PCT/RU2001/000511 2001-11-27 2001-11-27 Procede de fabrication de pectine WO2003045164A1 (fr)

Priority Applications (2)

Application Number Priority Date Filing Date Title
AU2002243118A AU2002243118A1 (en) 2001-11-27 2001-11-27 Method for producing pectin
PCT/RU2001/000511 WO2003045164A1 (fr) 2001-11-27 2001-11-27 Procede de fabrication de pectine

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/RU2001/000511 WO2003045164A1 (fr) 2001-11-27 2001-11-27 Procede de fabrication de pectine

Publications (1)

Publication Number Publication Date
WO2003045164A1 true WO2003045164A1 (fr) 2003-06-05

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Application Number Title Priority Date Filing Date
PCT/RU2001/000511 WO2003045164A1 (fr) 2001-11-27 2001-11-27 Procede de fabrication de pectine

Country Status (2)

Country Link
AU (1) AU2002243118A1 (fr)
WO (1) WO2003045164A1 (fr)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101935361A (zh) * 2010-08-31 2011-01-05 中国农业大学 一种利用高静压技术制备果胶的方法
CN102260355A (zh) * 2011-08-26 2011-11-30 重庆恒远晋通科技有限公司 基于烟草的果胶提取方法
ES2515515R1 (es) * 2013-04-29 2014-12-10 Galina IGNATYEVA Método de fabricación de pectina acromática, pectina y fibra modificada y pectina estandarizada

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0426434A1 (fr) * 1989-11-01 1991-05-08 The Western Sugar Company Pectines de betteraves à sucre et leur utilisation pour des produits comestibles
RU2058085C1 (ru) * 1991-09-09 1996-04-20 Голубев Владимир Николаевич Способ получения жидкого пектина
RU2066962C1 (ru) * 1996-02-23 1996-09-27 Владимир Николаевич Голубев Способ получения пектина
RU2088112C1 (ru) * 1995-09-25 1997-08-27 Флера Гарифовна Куприянова-Ашина Способ получения свекловичного пектина
RU2160281C1 (ru) * 1999-04-05 2000-12-10 Краснодарский научно-исследовательский институт хранения и переработки сельскохозяйственной продукции Способ производства пектина

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0426434A1 (fr) * 1989-11-01 1991-05-08 The Western Sugar Company Pectines de betteraves à sucre et leur utilisation pour des produits comestibles
RU2058085C1 (ru) * 1991-09-09 1996-04-20 Голубев Владимир Николаевич Способ получения жидкого пектина
RU2088112C1 (ru) * 1995-09-25 1997-08-27 Флера Гарифовна Куприянова-Ашина Способ получения свекловичного пектина
RU2066962C1 (ru) * 1996-02-23 1996-09-27 Владимир Николаевич Голубев Способ получения пектина
RU2160281C1 (ru) * 1999-04-05 2000-12-10 Краснодарский научно-исследовательский институт хранения и переработки сельскохозяйственной продукции Способ производства пектина

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101935361A (zh) * 2010-08-31 2011-01-05 中国农业大学 一种利用高静压技术制备果胶的方法
CN101935361B (zh) * 2010-08-31 2012-06-20 中国农业大学 一种利用高静压技术制备果胶的方法
CN102260355A (zh) * 2011-08-26 2011-11-30 重庆恒远晋通科技有限公司 基于烟草的果胶提取方法
ES2515515R1 (es) * 2013-04-29 2014-12-10 Galina IGNATYEVA Método de fabricación de pectina acromática, pectina y fibra modificada y pectina estandarizada

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Publication number Publication date
AU2002243118A1 (en) 2003-06-10

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