WO2002016907A1 - Appareil d'essai de la resistance a la rayure - Google Patents

Appareil d'essai de la resistance a la rayure Download PDF

Info

Publication number
WO2002016907A1
WO2002016907A1 PCT/GB2001/003823 GB0103823W WO0216907A1 WO 2002016907 A1 WO2002016907 A1 WO 2002016907A1 GB 0103823 W GB0103823 W GB 0103823W WO 0216907 A1 WO0216907 A1 WO 0216907A1
Authority
WO
WIPO (PCT)
Prior art keywords
support
sample
holder
scratching tool
sample surface
Prior art date
Application number
PCT/GB2001/003823
Other languages
English (en)
Inventor
Adrian George Plint
Original Assignee
Plint & Partners Limited
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Plint & Partners Limited filed Critical Plint & Partners Limited
Priority to AU2001282343A priority Critical patent/AU2001282343A1/en
Publication of WO2002016907A1 publication Critical patent/WO2002016907A1/fr

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00—Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/40—Investigating hardness or rebound hardness
    • G01N3/42—Investigating hardness or rebound hardness by performing impressions under a steady load by indentors, e.g. sphere, pyramid
    • G01N3/46—Investigating hardness or rebound hardness by performing impressions under a steady load by indentors, e.g. sphere, pyramid the indentors performing a scratching movement
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0058—Kind of property studied
    • G01N2203/0091—Peeling or tearing

Definitions

  • the present invention relates to a testing apparatus for evaluating the scratch resistance of a sample and to a method of evaluating the scratch resistance of a sample.
  • the tool or indenter has a sharp pointed tip which engages the sample surface.
  • the tool or indenter is maintained at a constant angle of incidence to the surface.
  • the severity of the scratch resistance test depends on the condition of the pointed tip of the tool or indenter. If the pointed tip is worn, then the scratch resistance test is less severe. Accordingly, the known scratch resistance methods can exhibit poor repeatability. Second, the useful lifetime of the tool or indenter can be relatively low as a result of rapid wear of the pointed tip.
  • the present invention aims at least partially to overcome these problems by providing a scratch resistance testing apparatus and method which enables a higher testing repeatability and increased lifetime of the tool or indenter to be achieved.
  • the present invention accordingly provides a testing apparatus for evaluating the scratch resistance of a sample, the apparatus comprising a support for the sample to be tested, a holder for a scratching tool, a drive device for causing relative translational movement between the support and the holder and an inclination varying device for progressively varying an angle of incidence between the scratching tool and a sample surface during relative translational movement between the scratching tool and the sample surface .
  • the present invention further provides a method for evaluating the scratch resistance of a sample, the method comprising supporting a sample to be tested on a support, disposing a scratching tool having a pointed end in a holder whereby the pointed end engages a surface of the sample to be tested, causing relative translational movement between the support and the holder whereby the pointed end is translated relative to the sample surface, and progressively varying an angle of incidence between the scratching tool and the sample surface during relative translational movement between the scratching tool and the sample surface .
  • the present invention is predicated on the discovery by the present inventor that by varying the angle of incidence of the scratching tool or indenter relative to the surface of a sample to be tested, the testing method can more accurately simulate potential scratching conditions which a sample surface is likely to experience in use wherein the magnitude and severity of a scratch are not only dependent on the force of application and the shape of the scratching device, but also on the angle of incidence of the scratching device relative to the surface.
  • the angle of incidence of the scratching tool or indenter relative to the surface to be tested this enhances not only the repeatability of the scratching test, but also tends to increase the life of the scratching tool or indenter.
  • the load between the scratching tool or indenter and the sample surface can be maintained constant or varied, preferably so as to increase the load with corresponding variation of the angle of incidence between the scratching tool or indenter and the surface to be tested.
  • Figure 1 is a schematic perspective view of a testing apparatus for evaluating the scratch resistance of a sample in accordance with an embodiment of the present invention.
  • the apparatus 2 includes a platen 4, which in the illustrated embodiment is rectangular in plan, having an upper surface 6 on which, in use, a sample 8 to be tested is horizontally supported.
  • the sample 8 is firmly affixed to the platen 4 by a fixing device (not shown) . When so supported, the sample 8 presents an upper surface 10 to be tested for scratch resistance.
  • the platen 4 is supported at its opposed ends 12,14 by respective flexures 16,18. Each flexure 16,18 extends across the transverse width of the respective end 12,14 of the platen 4.
  • Each flexure 16,18 is substantially C- shaped in cross section and includes upper and lower horizontal wall members 20,22 connected by a vertical wall member 24.
  • the platen 4 is affixed to the upper horizontal wall members 20 and the lower horizontal wall members 22 are affixed to a linear slide body 26.
  • a pair of elongate upper and lower notches 21,23 are provided in the inner surface 25 of the flexures 16,18 at the junctions between the respective upper and lower wall members 20,22 and the vertical wall member 24.
  • the linear side body 26 is substantially rectangular in plan and at one end 28 thereof is engaged by one end 30 of an elongate threaded lead screw 32.
  • the lead screw 32 is horizontally oriented and extends through a correspondingly threaded hole 34 in an end base member 36 of a linear slide base 38.
  • the lead screw 32 is adapted to be rotated either manually or by an electric motor (not shown) so as translationally and horizontally to displace the linear slide body 26 relative to the end base member 36.
  • the linear slide base 38 further comprises a pair of parallel slide members 40,42 which extend orthogonally away from the end base member 36 and slidably engage the respective opposed longitudinal sides 44,46 of the linear slide body 26.
  • the linear slide base 38 is secured to the upper surface 48 of a base plate 50.
  • a vertically oriented bracket 52 is mounted on the base plate 50.
  • the bracket 52 comprises a pair of parallel spaced bracket .members 54,56.
  • An L-shaped arm 58 is rotatably mounted between the bracket members 54,56 by a pivot bearing 60.
  • the L-shaped arm 58 comprises a generally horizontally oriented support member 62 extending above the platen 4 and a generally vertically oriented urging member 64 which extends upwardly from the pivot bearing 60.
  • the pivot bearing 60 extends horizontally between the upper ends 66,68 of the bracket members 54,56 and through the L-shaped arm 58 at the' junction between the support member 62 and the urging member 64.
  • the support member 62 is provided at the free end 68 thereof with an elongate slot 70 for receiving a substantially upright-oriented holder 72 for holding a scratching tool, or indenter, 74.
  • the scratching tool 74 has a pointed tip 76 which, in use, engages the upper surface 10 of the sample 8 to be tested.
  • the holder 72 is pivotally mounted on the free end 68 of the support member 62 by a pivot bearing 78. Accordingly, in use, the angle of incidence between the pointed tip 76 of the tool 74 and the sample surface 10 can be varied by rotating the holder 72 about the pivot bearing 78.
  • the free upper end 80 of the holder 72 is provided with a downward directed slot 82, which may be a slotted hole or notched fork, in which is removably located one end 84 of a pin member 86.
  • the pin member 86 is substantially horizontally oriented and the other end 88 thereof is affixed to a support wall 90 which is fixed to and extends upwardly away from the linear slide body 26.
  • the first and second force transducers 92,94 are respectively attached to the opposed upright edges 96,98 of the support wall 90.
  • the first force transducer 92 is connected by a rod 100 to the end 12 of the platen 4 which faces toward the lead screw 32.
  • the second force transducer 94 is connected to the urging member 64 by means of a biasing device comprising a helical tension spring 102, a screw threaded adjuster rod 104 threadably mounted on the urging member 64, and a second adjuster rod 105 which is threadably mounted on an extension 107 of the second force transducer 94.
  • the sample 8 to be tested is fixedly mounted on the platen 4 and a scratching tool 74 is mounted in the holder 72 with the pointed tip 76 being engaged with the upper surface 10 of the sample 8.
  • the lead screw 32 is then rotated, causing linear translational movement of the linear slide body 26 over the base plate 50.
  • the sample surface 10 is translationally linearly moved relative to the pointed tip 76 of the tool 74, the translational position of the tip 76 being fixed (subject to rotation of the tip 76 as described below) relative to the base plate 48 by way of the support member 62 of the arm 58 and the bracket 52.
  • the pin member 86 which is mounted to the linear slide body 26 by the support wall 90 is accordingly translationally horizontally moved by rotation of the lead screw 32. This causes progressive rotation of the holder 72 and correspondingly the pointed tip 76 of the tool 74 about the pivot bearing 78. In this way, the angle of incidence between the scratching tool 74 and the sample surface 10 is progressively varied together with translational movement of the scratching tool 74 along the sample surface 10.
  • the first force transducer 92 senses any tangential force in a direction along the sample surface 10 which is applied to the sample 8 by the scratching tool 74. This is achieved by detecting the elastic movement of the platen 4 in a direction parallel to the tangential direction of movement of the scratching tool 74 over the sample surface 10. The variation of that tangential force together with the angle of incidence of the scratching tool 74 and/or with the translational distance of relative movement between the sample 8 and the scratching tool 74 can be correlated.
  • the force applied through the helical tension spring 102 by way of the urging member 64 and the support member 62 to the holder 72 varies with translational movement of the scratching tool 74 along the sample 8.
  • the force applied through the helical spring 102 is progressively increased as a result of progressive tensioning of the helical spring 102.
  • the arm 58 is caused to rotate in an anti-clockwise direction by the spring 102. This causes an increased load to be applied to the arm 58 which in turn applies an increasing downwardly directed load on the holder 72 and hence on the scratching tool 74.
  • the scratching tool 74 also rotates in an anticlockwise direction as the sample 8 is traversed in the direction from right to left in the drawing, thereby gradually increasing the angle of incidence between the scratching tool 74 and the sample surface 10.
  • the second force transducer 94 senses the force applied through the helical spring 102.
  • the output of the second force transducer 94 can be correlated with the translational movement of the sample 8 and/or the tangential force detected by the first force transducer 92 and/or the angle of incidence of the scratching tool 74.

Landscapes

  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Investigating Strength Of Materials By Application Of Mechanical Stress (AREA)

Abstract

L'invention concerne un appareil d'essai permettant d'évaluer la résistance à la rayure d'un échantillon, ledit appareil comportant un support destiné à l'échantillon à tester, un support destiné à l'outil de rayures, un dispositif d'entraînement servant à provoquer un mouvement de translation relatif entre le support de l'échantillon et celui dudit outil, et un dispositif de variation de l'inclinaison servant à faire varier de manière progressive un angle d'incidence entre ledit outil et une surface d'échantillon lors dudit mouvement de translation.
PCT/GB2001/003823 2000-08-23 2001-08-22 Appareil d'essai de la resistance a la rayure WO2002016907A1 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
AU2001282343A AU2001282343A1 (en) 2000-08-23 2001-08-22 Scratch resistance testing apparatus and method

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GB0020808.2 2000-08-23
GB0020808A GB2366391A (en) 2000-08-23 2000-08-23 Scratch resistance testing apparatus and method

Publications (1)

Publication Number Publication Date
WO2002016907A1 true WO2002016907A1 (fr) 2002-02-28

Family

ID=9898173

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/GB2001/003823 WO2002016907A1 (fr) 2000-08-23 2001-08-22 Appareil d'essai de la resistance a la rayure

Country Status (3)

Country Link
AU (1) AU2001282343A1 (fr)
GB (1) GB2366391A (fr)
WO (1) WO2002016907A1 (fr)

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2004040265A1 (fr) * 2002-10-24 2004-05-13 Asmec Advanced Surface Mechanics Gmbh Table d'essai pour la mesure de forces et de deplacements lateraux
WO2005106424A2 (fr) * 2004-05-04 2005-11-10 Bayer Materialscience Ag Procede pour tester la resistance aux rayures de surfaces en matiere plastique
WO2007071624A1 (fr) * 2005-12-23 2007-06-28 Vallourec Mannesmann Oil & Gas France Protection externe de joints filetes tubulaires expansibles
US20100206041A1 (en) * 2009-02-19 2010-08-19 Sungkyunkwan University Foundation Corporate Collaboration Scratch testing apparatus for performing scratching test while gradually increasing or decreasing load
CN102680381A (zh) * 2012-05-09 2012-09-19 浙江吉利汽车研究院有限公司杭州分公司 盐雾划痕试验设备
CN103196761A (zh) * 2013-04-01 2013-07-10 北京工业大学 一种山字形试件反复加载试验装置及制作方法
WO2014205402A1 (fr) * 2013-06-21 2014-12-24 Massachusetts Materials Technologies Llc Appareil d'essai de résistance au rayage et ses procédés d'utilisation
DE102014012042A1 (de) 2013-08-17 2015-03-12 Hans-Peter Schlegelmilch Probenhalter und Prüfvorrichtung
US9897523B2 (en) 2015-03-05 2018-02-20 Massachusetts Materials Technologies Llc Contact mechanic tests using stylus alignment to probe material properties
US9933346B2 (en) 2013-06-21 2018-04-03 Massachusetts Materials Technologies Llc Contact mechanic tests using stylus alignment to probe material properties
US10775288B1 (en) 2013-06-21 2020-09-15 Massachusetts Materials Technologies Llc Stylus engagement mechanism for contact mechanics testers

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103512818B (zh) * 2013-08-12 2015-08-05 浙江豪情汽车制造有限公司 一种汽车标贴耐磨损性能试验台
CN105675403B (zh) * 2016-01-06 2018-09-07 北京东方雨虹防水工程有限公司 固定螺钉撕裂保温板临界点测试仪及测试方法
KR102608599B1 (ko) * 2018-08-16 2023-12-01 삼성디스플레이 주식회사 압력 센서를 테스트하는 장치 및 방법 그리고 이를 이용한 표시 장치
CN109540524B (zh) * 2018-12-25 2020-08-21 中国航发哈尔滨轴承有限公司 航空轴承滚动接触试验疲劳信号检测系统及其监测方法
EP4050320A1 (fr) * 2021-02-24 2022-08-31 Wood Coatings Research Group, Inc. Dispositif pour mesurer diverses propriétés de revêtements et de matériaux et ses procédés d'utilisation

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE386266C (de) * 1922-07-09 1923-12-18 Heinrich Borofski Materialpruefverfahren
US2335235A (en) * 1941-05-14 1943-11-30 Donald F Clifton Hardness testing instrument
US3785198A (en) * 1971-06-14 1974-01-15 Lonza Ag Scratch resistance tester
JPS62245131A (ja) * 1986-04-17 1987-10-26 Nec Corp ひつかき試験機

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5027650A (en) * 1990-05-08 1991-07-02 Gte Laboratories Incorporated Method for characterization of adhesion between hard materials

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE386266C (de) * 1922-07-09 1923-12-18 Heinrich Borofski Materialpruefverfahren
US2335235A (en) * 1941-05-14 1943-11-30 Donald F Clifton Hardness testing instrument
US3785198A (en) * 1971-06-14 1974-01-15 Lonza Ag Scratch resistance tester
JPS62245131A (ja) * 1986-04-17 1987-10-26 Nec Corp ひつかき試験機

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
PATENT ABSTRACTS OF JAPAN vol. 012, no. 114 (P - 688) 12 April 1988 (1988-04-12) *

Cited By (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7316155B2 (en) 2002-10-24 2008-01-08 Asmec Advanced Surface Mechanics Gmbh Test table for measuring lateral forces and displacements
WO2004040265A1 (fr) * 2002-10-24 2004-05-13 Asmec Advanced Surface Mechanics Gmbh Table d'essai pour la mesure de forces et de deplacements lateraux
WO2005106424A2 (fr) * 2004-05-04 2005-11-10 Bayer Materialscience Ag Procede pour tester la resistance aux rayures de surfaces en matiere plastique
WO2005106424A3 (fr) * 2004-05-04 2006-02-09 Bayer Materialscience Ag Procede pour tester la resistance aux rayures de surfaces en matiere plastique
WO2007071624A1 (fr) * 2005-12-23 2007-06-28 Vallourec Mannesmann Oil & Gas France Protection externe de joints filetes tubulaires expansibles
FR2895485A1 (fr) * 2005-12-23 2007-06-29 Vallourec Mannesmann Oil & Gas Protection externe de joints filetes tubulaires aptes a etre expanses
US7980597B2 (en) 2005-12-23 2011-07-19 Vallourec Mannesmann Oil & Gas France External protection for expandable threaded tubular connections
US8375774B2 (en) * 2009-02-19 2013-02-19 Sungkyunkwan University Foundation For Corporate Collaboration Scratch testing apparatus for performing scratching test while gradually increasing or decreasing load
US20100206041A1 (en) * 2009-02-19 2010-08-19 Sungkyunkwan University Foundation Corporate Collaboration Scratch testing apparatus for performing scratching test while gradually increasing or decreasing load
CN102680381A (zh) * 2012-05-09 2012-09-19 浙江吉利汽车研究院有限公司杭州分公司 盐雾划痕试验设备
CN102680381B (zh) * 2012-05-09 2015-04-01 浙江吉利汽车研究院有限公司杭州分公司 盐雾划痕试验设备
CN103196761A (zh) * 2013-04-01 2013-07-10 北京工业大学 一种山字形试件反复加载试验装置及制作方法
WO2014205402A1 (fr) * 2013-06-21 2014-12-24 Massachusetts Materials Technologies Llc Appareil d'essai de résistance au rayage et ses procédés d'utilisation
US9778158B2 (en) 2013-06-21 2017-10-03 Massachusetts Materials Technologies Llc Scratch testing apparatus and methods of using same
US9933346B2 (en) 2013-06-21 2018-04-03 Massachusetts Materials Technologies Llc Contact mechanic tests using stylus alignment to probe material properties
US10775288B1 (en) 2013-06-21 2020-09-15 Massachusetts Materials Technologies Llc Stylus engagement mechanism for contact mechanics testers
DE102014012042A1 (de) 2013-08-17 2015-03-12 Hans-Peter Schlegelmilch Probenhalter und Prüfvorrichtung
DE202014006597U1 (de) 2013-08-17 2015-09-17 Hans Peter Schlegelmilch Probenhalter und Prüfvorrichtung
US9897523B2 (en) 2015-03-05 2018-02-20 Massachusetts Materials Technologies Llc Contact mechanic tests using stylus alignment to probe material properties

Also Published As

Publication number Publication date
AU2001282343A1 (en) 2002-03-04
GB2366391A (en) 2002-03-06
GB0020808D0 (en) 2000-10-11

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