WO1998004774A1 - Method and apparatus for bleaching wood pulp, especially containing waste paper - Google Patents

Method and apparatus for bleaching wood pulp, especially containing waste paper Download PDF

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Publication number
WO1998004774A1
WO1998004774A1 PCT/SE1997/001305 SE9701305W WO9804774A1 WO 1998004774 A1 WO1998004774 A1 WO 1998004774A1 SE 9701305 W SE9701305 W SE 9701305W WO 9804774 A1 WO9804774 A1 WO 9804774A1
Authority
WO
WIPO (PCT)
Prior art keywords
pulp
screw
plug
steam
bleaching
Prior art date
Application number
PCT/SE1997/001305
Other languages
English (en)
French (fr)
Inventor
Rolf Kurtz
Original Assignee
Cellwood Machinery Ab
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Cellwood Machinery Ab filed Critical Cellwood Machinery Ab
Priority to JP50830998A priority Critical patent/JP2000515205A/ja
Priority to EP19970933977 priority patent/EP0914517A1/en
Priority to US09/230,059 priority patent/US6419786B1/en
Publication of WO1998004774A1 publication Critical patent/WO1998004774A1/en
Priority to NO990309A priority patent/NO990309L/no

Links

Classifications

    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C9/00After-treatment of cellulose pulp, e.g. of wood pulp, or cotton linters ; Treatment of dilute or dewatered pulp or process improvement taking place after obtaining the raw cellulosic material and not provided for elsewhere
    • D21C9/10Bleaching ; Apparatus therefor
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21BFIBROUS RAW MATERIALS OR THEIR MECHANICAL TREATMENT
    • D21B1/00Fibrous raw materials or their mechanical treatment
    • D21B1/04Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres
    • D21B1/12Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres by wet methods, by the use of steam
    • D21B1/30Defibrating by other means
    • D21B1/32Defibrating by other means of waste paper
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C5/00Other processes for obtaining cellulose, e.g. cooking cotton linters ; Processes characterised by the choice of cellulose-containing starting materials
    • D21C5/02Working-up waste paper
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/50Reuse, recycling or recovery technologies
    • Y02W30/64Paper recycling

Definitions

  • the present invention relates to a method of the kind defined in the preamble of Claim 1 for treating wood-fibre pulp, particularly pulp that contains recycled paper.
  • the invention also relates to plant for carrying out the method.
  • Wood-fibre pulp of the kind with which the invention is concerned is treated typically in a number of stages which include dewatering of the pulp in a dewatering zone with the aid of a screw press, so as to increase pulp consistency from an input value of 4-6% to an output value of about 30%.
  • the pulp is then passed from the dewatering zone to a heating zone, through which the pulp is advanced while delivering steam thereto.
  • the pulp is preferably shredded in this treatment zone, so as to enable the pulp to be heated with saturated steam to a desired temperature, both quickly and uniformly. On average, 300 kg of steam are consumed with each tonne of pulp treated.
  • the heated and finely-divided pulp is then passed to a disperser which enables the material to be treated mildly at high pulp consistencies.
  • a disperser which enables the material to be treated mildly at high pulp consistencies. This is made possible by the mutually opposing toothed refiner discs, of which one rotates relative to the other.
  • the disc clearance or gap can be adjusted during operation with the aid of an electro-hydraulic system.
  • the temperature of the treated pulp can vary from between 80°C and 120°C for instance, depending on the nature of the pulp being treated, among other things. There is a risk that pulp fibres will be damaged at excessively high temperatures.
  • the pulp consistency may be as high as 30% when leaving the heating zone. Pulp consistency is reduced to some extent by the pressurized steam delivered to the pulp.
  • Pulp consist- ency may, however, reach about 15% in some cases.
  • the sealing plug also enables the steam temperature to be increased in the heating zone, which has particular advantages when treating highly contaminated recycled paper. It has thus been possible to utilize temperatures of 120°C and higher. It has also been possible to increase steam pressure and therewith improve process yields.
  • the disperser includes a rotor that carries a disc which has provided around a peripheral region teeth that coact with teeth on an opposing toothed ring or disc mounted in a surrounding housing, said ring or disc preferably being fixedly mounted and functioning to finely divide the pulp.
  • the disperser also includes a pulp outlet.
  • the pulp outlet includes a connection with a screw press for advancing the pulp to an end of the press that is closed or sealed by valve means so as to form a sealing pulp-plug at said end, without separate departure of steam.
  • US-A 4,909,900 (Matzke, et al) teaches a bleaching method in which, subsequent to dispersion, the bleached wood-fibre pulp is delivered to a tank or container in which the bleaching method is carried out.
  • the method thus lacks the step in which finely-divided pulp is delivered to a screw press or plug screw without separate steam departure.
  • the object of this known method is to shorten the bleaching process to a duration of some few seconds.
  • WO 96/012062 (AGA) teaches a method which is characterized mainly by supplying oxygen to the process with the intention of limiting the amount of peroxide used. This known method also lacks the step of delivering the pulp to a screw press or plug screw downstream of the disperser, and the prevention of separate departure of steam.
  • An object of the present invention is to provide a method of the kind defined in the introduction that will make instaneous effective bleaching of the wood-fibre pulp possible to achieve.
  • a further object is to provide a method of the aforedescri- bed kind which includes a bleaching process and which is adapted to the different temperature conditions required by the various chemicals used, in order to obtain the best possible result.
  • Still another object of the invention is to provide a method which includes a wood-fibre pulp bleaching process and which functions effectively with the exclusion of atmospheric oxygen.
  • an object of the invention is to provide a treatment plant, particularly for the treatment of wood-fibre pulp that includes recycled paper, with which pulp can be bleached effectively in the absence of any essential auxiliary devices.
  • the most significant advantages afforded by the invention reside in the ability of bleaching wood-fibre pulp at temperatures higher than 100°C, by providing a sealed, pressurized system that will prevent the ingress of air. This also overcomes the serious drawback that certain chemicals have a poorer bleaching effect in the presence of air, or may even be destroyed.
  • the invention is also beneficial from an environmental aspect, since no chemicals are able to leak from the plant while the plant is operating.
  • the invention enables the temperature to be reduced by supplying water of relatively low temperature to the system. This can be achieved by cooling the wood-fibre pulp with a comparative- ly large amount of low-temperature water in conjunction with the chemical supply, and thereafter reheating the pulp. This enables the thermal energy contained in the pulp immediately downstream of the disperser to be used in an optimal manner.
  • the pulp residence time in the reaction screw can be adjusted by varying the speed of the screw. It has been found in practice that in order for the bleaching chemicals used to give the best result, the pulp should have a screw residence time of longer than six minutes. A residence time of about ten minutes is usually the most effective resi- dence time.
  • the bleaching chemicals may be charged to a shredder that is preceded by a preheater in the dispersing part of the plant and from there to the disperser itself and then to a screw press or to a plug screw downstream of the screw press .
  • the active phase of the bleaching process takes place thereafter in the bleaching section of the plant, which in one preferred embodiment of the invention commences with a shredder that disintegrates the pulp plug formed in the screw press or in the plug screw.
  • the major part of the bleaching process then takes place in the reaction screw where the pulp residence time is controlled with the aid of the speed at which the screw rotates, as mentioned earlier.
  • the invention also relates to a wood-fibre pulp treatment plant, particularly wood-fibre pulp that contains recycled paper, the main characteristic features of said plant being set forth in Claim 4.
  • the drawing illustrates a number of essential components of a plant for treating pulp that contains recycled paper.
  • the pulp is passed through a conduit 2 to a screw-type dewatering device 3 in which the pulp is dewatered from an input consistency of 2% to an output consistency of 8%, for instance. Water pressed from the pulp is discharged through a conduit 19.
  • the dewatering zone also includes a screw press 4 which operates in the dispersing system from an input consistency of from 4-6% to an output concentration of about 30%.
  • the screw is coated with hardmetal.
  • the screw press is designed so that all parts of the dispersing system will be readily accessible.
  • the pulp is then transferred to a preheater 7 in the heating zone of the plant, via a plug screw 5 and a shredder 6. Steam is introduced at different locations along the axial length of the preheater. The pressure and temperature of the steam delivered will be varied in accordance with the extent to which the pulp is contaminated, among other things.
  • the disperser 10 includes a rotor which is driven by an electric motor and coacts with a toothed disc 12 accommodated in the housing 10a.
  • the teeth on the disc 12 coact with teeth on an opposing disc 13 fixedly mounted in the housing, such as to finely-divide the pulp delivered to the disperser.
  • Dilution water is delivered to the disperser through suitable conduits (not shown) .
  • the disperser includes an outlet 16 which connects with an inlet of a screw press or outfeed plug screw having a screw 20 mounted in a housing 20a.
  • a pulp plug of desired pulp consistency for instance a consistency of 30% or more, is formed in that end of the housing 20a which lies distal from the inlet.
  • the pulp plug functions to seal the system so that the heat content of the steam delivered to the system at overpressure and relatively high temperature, e.g. a temperature of 110-120°C, can be utilized in the most effective manner possible.
  • bleaching chemical delivery means e.g. conduits.
  • These chemicals may be hydrosulphide or peroxide for effective bleaching of fibres present in the pulp.
  • Bleaching can also be effected with oxygen gas in some cases.
  • FAS Formadine sulphinic acid
  • the illustrated embodiment thus includes supply means 30 connected to the vertical transport shaft between the screw press 4 and the plug screw 5, supply means 31 connected to the actual disperser 10, and supply means 32 connected to the screw press or plug screw 20.
  • bleaching chemicals can be delivered at these locations, or at other locations, in accordance with the properties of the wood-fibre pulp concerned.
  • Those components located downstream of the plug screw 20 belong to the bleaching section of the plant and include a shredder 25 which extends vertically in a housing or casing 25a and which functions to disintegrate the pulp plug formed in the screw press or plug screw 20.
  • the disintegrated pulp is then delivered to a reaction screw 26 which is accommodated in a casing 26a and in which the major part of the bleaching process takes place.
  • Steam is delivered to the casing 26a through a conduit 27.
  • water e.g. water of relatively low temperature, is delivered through the conduit 27 or through a further conduit (not shown) .
  • the residence time of the pulp in the reaction screw is controlled by the speed at which the screw rotates and will usually be about ten minutes.
  • a further screw press or plug screw 28 accommodated in a housing or casing 28a is connected to the outfeed end of the reaction screw, said screw press or plug screw being essentially of the same kind as the screw press 20.
  • the screw press 28 may include a pivotally mounted valve flap 35 that is actuated by a pneumatic cylinder 36 and associated piston rod. There may also be included a valve flap regulator which causes the valve flap to exert a predetermined counterpressure against the pulp plug formed in the end of the plug screw 28. When this pressure is exceeded, the flap will open and therewith allow the pulp plug of desired pulp consistency to leave the outfeed plug screw.
  • the pulp plug formed in the plug screw 28 also seals the system such as to enable recovery of the heat content of the steam delivered to the system to the best extent possible.
  • the pulp plugs formed in the plug screws 20 and 28 also contribute towards insuring that essentially no air that is capable of influencing negatively the bleaching operation in the reaction screw 26 will enter the plant.
  • the arrangement of said bleaching chemical supply means 30, 31 and 32 at respective different locations in the system enables the best result to be achieved in dependence on prevailing conditions and circumstances.
  • a plant of the type described and illustrated here will enable different types of bleaching processes to be carried out simultaneously in different sections of the plant, so- called sequence bleaching. It can also be ensured that different temperatures prevail in these different sections of the plant, so as to achieve optimal bleaching.

Landscapes

  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Mechanical Engineering (AREA)
  • Paper (AREA)
PCT/SE1997/001305 1996-07-25 1997-07-22 Method and apparatus for bleaching wood pulp, especially containing waste paper WO1998004774A1 (en)

Priority Applications (4)

Application Number Priority Date Filing Date Title
JP50830998A JP2000515205A (ja) 1996-07-25 1997-07-22 特に廃紙を含んだ木材パルプをブリーチ処理する方法及び装置
EP19970933977 EP0914517A1 (en) 1996-07-25 1997-07-22 Method and apparatus for bleaching wood pulp, especially containing waste paper
US09/230,059 US6419786B1 (en) 1996-07-25 1997-07-22 Method for bleaching wood pulp containing recycled paper
NO990309A NO990309L (no) 1996-07-25 1999-01-22 FremgangsmÕte og apparat for bleking av tremasse, sµrlig inneholdende returpapir

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
SE9602858A SE506803C2 (sv) 1996-07-25 1996-07-25 Sätt och anläggning för blekning av returpappersmassa
SE9602858-4 1996-07-25

Publications (1)

Publication Number Publication Date
WO1998004774A1 true WO1998004774A1 (en) 1998-02-05

Family

ID=20403466

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/SE1997/001305 WO1998004774A1 (en) 1996-07-25 1997-07-22 Method and apparatus for bleaching wood pulp, especially containing waste paper

Country Status (7)

Country Link
US (1) US6419786B1 (sv)
EP (1) EP0914517A1 (sv)
JP (1) JP2000515205A (sv)
CA (1) CA2260935A1 (sv)
NO (1) NO990309L (sv)
SE (1) SE506803C2 (sv)
WO (1) WO1998004774A1 (sv)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1031657A1 (en) * 1999-02-25 2000-08-30 Degussa-Hüls Aktiengesellschaft A method for bleaching secondary fibres
EP1096062A1 (de) * 1999-10-29 2001-05-02 Voith Paper Patent GmbH Verfahren zur Erhöhung der Homogenität und des Weissgrades von Papierfaserstoff
DE19954246A1 (de) * 1999-10-29 2001-07-26 Voith Paper Patent Gmbh Verfahren zur Erhöhung der Homogenität und des Weißgrades von Papierfaserstoff
EP1348802A1 (de) * 2002-03-27 2003-10-01 Andritz AG Verfahren und Vorrichtung zur Dispergierung eines Papierfaserstoffes
EP2758589A4 (en) * 2011-09-20 2015-08-26 Iogen Energy Corp METHOD FOR HEATING A FEEDING LOAD

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FI109135B (sv) * 1999-09-21 2002-05-31 Metso Paper Inc Förfarande och anordning för behandling av träfibermassa
DE10018262A1 (de) * 2000-04-13 2001-10-18 Voith Paper Patent Gmbh Verfahren zur Dispergierung eines Papierfaserstoffes sowie Anlage zur Durchführung des Verfahrens
JP2003119679A (ja) * 2001-10-17 2003-04-23 Aikawa Iron Works Co Ltd パルプ加熱装置
JP2006144148A (ja) * 2004-11-17 2006-06-08 Fukoku Kogyo Kk 古紙パルプの不純物分離促進方法
CN102704301B (zh) * 2012-06-19 2017-10-20 连城县东方经济开发有限公司 一种涂布牛卡废纸再生隔层纸工艺
FI125635B (sv) * 2015-02-05 2015-12-31 Valmet Technologies Oy Anordning för förvärmning av returfibermassa som skall dispergeras
CN109173963A (zh) * 2018-09-30 2019-01-11 山东世纪阳光纸业集团有限公司 一种生物反应横管

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4909900A (en) * 1986-03-04 1990-03-20 Sulzer-Escher Wyss Gmbh Method for high temperature, high consistency quick bleaching of raw paper pulp
US5176793A (en) * 1988-08-30 1993-01-05 Cellwood Machinery Ab Method of treating and a disperger for disintegrating wood pulp, especially containing waste paper
WO1996012062A1 (en) * 1994-10-13 1996-04-25 Aga Aktiebolag A method and apparatus for bleaching secondary fibres

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4909900A (en) * 1986-03-04 1990-03-20 Sulzer-Escher Wyss Gmbh Method for high temperature, high consistency quick bleaching of raw paper pulp
US5176793A (en) * 1988-08-30 1993-01-05 Cellwood Machinery Ab Method of treating and a disperger for disintegrating wood pulp, especially containing waste paper
WO1996012062A1 (en) * 1994-10-13 1996-04-25 Aga Aktiebolag A method and apparatus for bleaching secondary fibres

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1031657A1 (en) * 1999-02-25 2000-08-30 Degussa-Hüls Aktiengesellschaft A method for bleaching secondary fibres
EP1096062A1 (de) * 1999-10-29 2001-05-02 Voith Paper Patent GmbH Verfahren zur Erhöhung der Homogenität und des Weissgrades von Papierfaserstoff
DE19954246A1 (de) * 1999-10-29 2001-07-26 Voith Paper Patent Gmbh Verfahren zur Erhöhung der Homogenität und des Weißgrades von Papierfaserstoff
EP1348802A1 (de) * 2002-03-27 2003-10-01 Andritz AG Verfahren und Vorrichtung zur Dispergierung eines Papierfaserstoffes
CN1306113C (zh) * 2002-03-27 2007-03-21 安德里茨有限公司 分散再生纤维纸浆的装置
EP2758589A4 (en) * 2011-09-20 2015-08-26 Iogen Energy Corp METHOD FOR HEATING A FEEDING LOAD

Also Published As

Publication number Publication date
JP2000515205A (ja) 2000-11-14
CA2260935A1 (en) 1998-02-05
SE506803C2 (sv) 1998-02-16
EP0914517A1 (en) 1999-05-12
SE9602858D0 (sv) 1996-07-25
SE9602858L (sv) 1998-01-26
US6419786B1 (en) 2002-07-16
NO990309L (no) 1999-03-24
NO990309D0 (no) 1999-01-22

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