WO1997019581A2 - Augmentation de reactions biologiques, biochimiques et chimiques a l'aide de liquide et de solides structures - Google Patents

Augmentation de reactions biologiques, biochimiques et chimiques a l'aide de liquide et de solides structures Download PDF

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Publication number
WO1997019581A2
WO1997019581A2 PCT/US1996/013992 US9613992W WO9719581A2 WO 1997019581 A2 WO1997019581 A2 WO 1997019581A2 US 9613992 W US9613992 W US 9613992W WO 9719581 A2 WO9719581 A2 WO 9719581A2
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WO
WIPO (PCT)
Prior art keywords
structured
water
enhance
solids
biological
Prior art date
Application number
PCT/US1996/013992
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English (en)
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WO1997019581A3 (fr
Inventor
Shui Uin Lo
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American Technologies Group
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by American Technologies Group filed Critical American Technologies Group
Priority to AU71053/96A priority Critical patent/AU7105396A/en
Priority to EP96932160A priority patent/EP0851789A2/fr
Publication of WO1997019581A2 publication Critical patent/WO1997019581A2/fr
Publication of WO1997019581A3 publication Critical patent/WO1997019581A3/fr

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L10/00—Use of additives to fuels or fires for particular purposes
    • C10L10/02—Use of additives to fuels or fires for particular purposes for reducing smoke development
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/005—Systems or processes based on supernatural or anthroposophic principles, cosmic or terrestrial radiation, geomancy or rhabdomancy
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/12—Inorganic compounds
    • C10L1/1233—Inorganic compounds oxygen containing compounds, e.g. oxides, hydroxides, acids and salts thereof
    • C10L1/125—Inorganic compounds oxygen containing compounds, e.g. oxides, hydroxides, acids and salts thereof water
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L10/00—Use of additives to fuels or fires for particular purposes
    • C10L10/04—Use of additives to fuels or fires for particular purposes for minimising corrosion or incrustation
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12C—BEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
    • C12C5/00—Other raw materials for the preparation of beer
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G1/00—Preparation of wine or sparkling wine
    • C12G1/02—Preparation of must from grapes; Must treatment and fermentation
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12N—MICROORGANISMS OR ENZYMES; COMPOSITIONS THEREOF; PROPAGATING, PRESERVING, OR MAINTAINING MICROORGANISMS; MUTATION OR GENETIC ENGINEERING; CULTURE MEDIA
    • C12N1/00—Microorganisms, e.g. protozoa; Compositions thereof; Processes of propagating, maintaining or preserving microorganisms or compositions thereof; Processes of preparing or isolating a composition containing a microorganism; Culture media therefor
    • C12N1/14—Fungi; Culture media therefor
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12N—MICROORGANISMS OR ENZYMES; COMPOSITIONS THEREOF; PROPAGATING, PRESERVING, OR MAINTAINING MICROORGANISMS; MUTATION OR GENETIC ENGINEERING; CULTURE MEDIA
    • C12N1/00—Microorganisms, e.g. protozoa; Compositions thereof; Processes of propagating, maintaining or preserving microorganisms or compositions thereof; Processes of preparing or isolating a composition containing a microorganism; Culture media therefor
    • C12N1/20—Bacteria; Culture media therefor
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/02—Preparation of oxygen-containing organic compounds containing a hydroxy group
    • C12P7/04—Preparation of oxygen-containing organic compounds containing a hydroxy group acyclic
    • C12P7/06—Ethanol, i.e. non-beverage
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel

Definitions

  • the invention is in the form of an aqueous solution which contains very small amounts of stable rigid structures in the sub-micron size range, similar to ice VI which, when added to a chemical or biological process produce a catalytic reaction or may be consumed in the reaction itself.
  • ice VI which, when added to a chemical or biological process produce a catalytic reaction or may be consumed in the reaction itself.
  • One object and advantage of the invention is a strucrured liquid or solid which can have great economic benefit in industrial and commercial applications, by speeding up chemical, biochemical and biological reactions.
  • Our object is to use the structured liquid and solid which has been invented in the previous patent applications listed, to enhance the reaction rates of chemical, biochemical and biological processes.
  • Figure 1 shows a structured water crystal with carbon atoms attached.
  • the carbon atoms are attracted by the electric field around the crystal.
  • the crystal being made of water, supplies oxygen which can then enhance the formation of carbon monoxide when heat is added. This action is discussed in detail in section i.l.
  • Figure 2 shows a typical catalytic converter where partially combusted fuel and air is brought in and further combusted.
  • the structured quartz inside the catalyst container replaces the normal precious metals.
  • the structured quartz attracts the carbon monoxide and oxygen together on its surface thus allowing further oxydation to occur to carbon dioxide.
  • L E -structured liquid is broadly defined as the structured liquids prepared by the earlier two inventions listed in section b above, L s -structure specifically means that the structure is induced by strong electric fields which can come about from the electric field of an ion or from the dipole moment of molecules. Structured water is one specific case of this L e -structure liquid.
  • S E -structured solid is broadly defined as the structured solids prepared by the earlier two inventions listed in section b above.
  • Structured water is water which is I E -structured and has a strong electric dipole moment. These electric dipole moments can induce electric dipole moments in neutral molecules that move near it. The electric attractive force draws the neutral molecules to the surface of the I E structures. The attraction is greater if the electric dipole moment of the I E structure is larger.
  • a and B to react into C and D in a chemical reaction, it is necessary for A and B to get close to each other. With the presence of the I E structures pulling both A and B together then the reaction rate will be increased and the I E structures become the catalyst for the reaction A and B to C and D.
  • I E structures For bacteria that live in water, when I E structures are present in the water, they exert strong electric fields near their surface. When the bacteria move near the I E structure they experience an electric shock which will stimulate growth. Hence we expect that I E structure water will stimulate the growth of biological entities such as bacteria, virus, plants, fungi, yeasts, molds or any biological entity, if mere are sufficient nutrients around.
  • the initial state consists of carbon and water:
  • the reaction rate R N of the I E crystal will be N 4 times that of an individual water molecule.
  • the enhancement rate is 1 million times.
  • a specific use the reactions of carbon with water molecules are the creation of coal gas for burning domestically or the removal of carbon deposits by I E crystals or the removal of carbon deposits by cracking with steam which contains I E crystals.
  • the carbon monoxide combines with oxygen to produce carbon dioxide. This reaction is particularly important in the reduction in pollution from the exhaust gas of a car engine.
  • the addition of I E crystals into the car engine will facilitate the above reactions in the following way.
  • the I E crystal attracts both the carbon monoxide and the oxygen to its surface due to its electric dipole moment.
  • the large electric dipole moment will induce the oxygen molecule electric dipole moment so that the oxygen molecule will be attracted to the I E crystal.
  • Carbon monoxide has its own permanent electric dipole moment and will be attracted to the I E crystal so that the carbon monoxide and oxygen molecules will spend much more tune in close proximity than would otherwise occur if the I E crystal were not present
  • the I E crystals serve as a catalyst to reduce carbon monoxide to carbon dioxide.
  • thermal cracking processes involve the use of steam on heavy hydrocarbons so as to reduce them to lighter hydrocarbons such as gasoline or diesel. This process will be accelerated by steam containing I E crystals.
  • S E structured solids it is sometimes more convenient to use structured solids now called S E structured solids. See previous patent application numbers 08/182410 and 08/217042 to find the creation of such structured solids.
  • the S E structured solids also have a large electric dipole moment like the I E crystal, hence it is also possible to substitute the above functions of the I E crystal in enhancing the rate of chemical reactions of the type:
  • a particular device of this type would be a catalytic converter in a car where currently platinum, rhodium, palladium and other precious metals are now used. These precious metals can be substituted by S. structured solids such as structured quartz or structured ceramic. This is as shown iD Figure 2. The general reaction of S B structured solids is
  • the homeopathic prepared solutions can enhance the growth of biological entities such as yeasts, wheat seedlings and mung seed sprouts (See: Discovering homeopathic medicine for the 21st century by Dana Ullman)
  • the solutions prepared by the horrjeoparhic method according to our studies has only a very small amount present of I E -structured crystals in water and L E -struct ⁇ red crystals in other liquids such as alcohol.(See: Novel Stable Structures of Water by Dr. Shui-Yin Lo, copy attached with this application).
  • the E Coli are used in the biotechnology industry to create human growth hormone and other valuable biochemical materials.
  • the B Subtilis are used extensively to break down starches into sugar and alcohol. These increases of activity of the bacteria will result in significant reductions in capital and operating costs in industrial and medical applications.
  • I E structures can increase the reproduction rare of biological entities such as bacteria, viruses fungi and yeasts.
  • the I E structures are made up of water molecules with large electrical dipole moments.
  • the electrical dipole moments will generate a strong elect field around the crystal.
  • Bacteria generally have an uneven charge distribution on the outside surface of their bodies and when they are close to the I E structures, parts of their body would be subject to the strong electric field of the I E structures. This will attract or repel them strongly to the I E structures. This amounts to an electric shock to the bacteria. This electric shock will stimulate the bacteria into a higher level of activity. The bacteria will then will accelerate their activity as desired. If sufficient nutrients are available, the reproduction rate will be obviously increased. However if there is no nutrients available, the bacteria may the from too many encounters with I E crystals and so we can also say that I E structured water has a mildly antiseptic effect when no nutrient is available.
  • the water solution prepared by normal homeopathic methods would show an absorbance of UV light at Lambda 190 nm of about 0.02 while the concentrated L, solution we prepared easily shows a UV absorbance at 190 nm above 0.10.
  • the solution we use in this experiment had UV absorbance at 190 nm above 0.5 so it can be described as at least 25 times stronger than what is presently available in the homeopathic industry.
  • the solutions were cultured at 37C for 23 hours and the optical density measurements of the solution were made at a wavelength of 540 nm.
  • the optical density measurements reflect the density of bacteria in the solutions.
  • the following table shows that the I E structured water has 5 to 7 times the amount of bacteria present than the distilled water sample.
  • E Coli bacteria A similar experiment was carried on E Coli bacteria.
  • the LB medium (5 ml) was inoculated with E Coli bacteria.
  • the LB was composed of 10g tryptone, 5g yeast extract and 5g NaCl. Again 3 types of I E structured water were used and one sample of distilled water as a control.
  • the solution was incubated overnight for 23 houres at 37C.
  • the culture was diluted 20 times with sterile water.
  • Three tubes were then inoculated with 1 ⁇ l, 10 ⁇ l and 100 ⁇ l of diluted culture. Also three control tubes were inoculated at the same time. These were then incubated for 20 hours at 37C. After the growth period, the optical density at 600 nm for all samples were measured. Test results are shown in the following table,
  • the stable, rigid L E structures formed in a liquid consists of large electric dipole moment, which generate strong electric fields that can attract the various components in a chemical reaction, increase the probability of collision between these opposing components and their contact time, and thereby increasing the overall rate of reaction which takes place.
  • the structures themselves vary in size from a few nanometers in length up to several micrometers. k. Conclusion, Discussion of Ramifications
  • L E and S E structures as described herein can be formed in liquids and solids respectively. Due to the strong electric field that exist around these structures, their inclusion into many different chemical and biological reactions can result in an acceleration of these reactions. This has many rarmifications in medical, biological and industrial processes where a simple, low cost catalyst or catalyst-like substance can be manufactured in liquids and solids and used directly, resulting in significant cost reductions in these processes.

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Genetics & Genomics (AREA)
  • Biotechnology (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Microbiology (AREA)
  • Tropical Medicine & Parasitology (AREA)
  • Biomedical Technology (AREA)
  • Virology (AREA)
  • Medicinal Chemistry (AREA)
  • Combustion & Propulsion (AREA)
  • General Chemical & Material Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Food Science & Technology (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Mycology (AREA)
  • Botany (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Apparatus Associated With Microorganisms And Enzymes (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

Il est bien connu que les molécules d'eau forment des structures rigides stables. La structure rigide la plus commune est la glace de type I qui se forme naturellement à 4 °C à une pression d'une atmosphère. On peut également former de la glace de type VI à température ambiante, dans des conditions artificielles en soumettant l'eau à une pression hydrostatique très élevée (⊃ 7 kilobars). Une telle pression élevée peut également exister au niveau microscopique entre un ion et les molécules d'eau voisines, sous l'effet de l'attraction électrostatique entre la charge d'un ion et les moments dipolaires d'une molécule d'eau. On peut ainsi former dans l'eau à température ambiante et sous pression atmosphérique des structures rigides de molécules d'eau similaires à la glace de type VI. Les structures rigides et stables ainsi formées peuvent être filtrées, concentrées et photographiées au moyen d'un microscope électronique à transmission. On a découvert que ces structures rigides et stables créent des réactions catalytiques dans différents systèmes chimiques et biologiques, ainsi que dans des systèmes structurés solides. Par exemple, la vitesse de prolifération des bactéries E. Coli et de B. Subtilis est sensiblement augmentée par la présence de petites quantités de ces structures rigides dans un milieu de culture aqueux. Cette découverte a d'importantes applications pour l'accélération des vitesses de réaction dans différents procédés de fermentation industriels et dans différents procédés chimiques industriels.
PCT/US1996/013992 1995-08-29 1996-08-29 Augmentation de reactions biologiques, biochimiques et chimiques a l'aide de liquide et de solides structures WO1997019581A2 (fr)

Priority Applications (2)

Application Number Priority Date Filing Date Title
AU71053/96A AU7105396A (en) 1995-08-29 1996-08-29 Enhancing biological, biochemical and chemical reactions using structured liquids and solids
EP96932160A EP0851789A2 (fr) 1995-08-29 1996-08-29 Augmentation de reactions biologiques, biochimiques et chimiques a l'aide de liquide et de solides structures

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US52063695A 1995-08-29 1995-08-29
US08/520,636 1995-08-29

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WO1997019581A2 true WO1997019581A2 (fr) 1997-06-05
WO1997019581A3 WO1997019581A3 (fr) 1997-09-04

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AU (1) AU7105396A (fr)
WO (1) WO1997019581A2 (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2384312A2 (fr) * 2008-12-04 2011-11-09 D&Y Laboratories Agrégats d eau, produits dotés d agrégats d eau et procédés de production

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2253860A (en) * 1991-03-12 1992-09-23 Kirk And Charashvili Internati Electrolytic treatment of water
WO1996006048A1 (fr) * 1994-08-22 1996-02-29 S.C. Tehman Srl Installation et procede d'obtention d'eaux structurees du type 'i' (activees dans un sens inhibiteur) et du type 's' (activees dans un sens stimulateur)

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2253860A (en) * 1991-03-12 1992-09-23 Kirk And Charashvili Internati Electrolytic treatment of water
WO1996006048A1 (fr) * 1994-08-22 1996-02-29 S.C. Tehman Srl Installation et procede d'obtention d'eaux structurees du type 'i' (activees dans un sens inhibiteur) et du type 's' (activees dans un sens stimulateur)

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
MODERN PHYSICS LETTERS B, vol. 10, no. 19, 20 August 1996, SINGAPORE, pages 909-919, XP000672451 S.-Y.LO: "Anomalous State of Ice" *
MODERN PHYSICS LETTERS B., vol. 10, no. 19, 20 August 1996, SINGAPORE, pages 921-930, XP000672449 S.-Y. LO ET AL.: "Physical Properties of Water with IE Structures" *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2384312A2 (fr) * 2008-12-04 2011-11-09 D&Y Laboratories Agrégats d eau, produits dotés d agrégats d eau et procédés de production
EP2384312A4 (fr) * 2008-12-04 2014-03-05 D & Y Lab Agrégats d eau, produits dotés d agrégats d eau et procédés de production

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Publication number Publication date
AU7105396A (en) 1997-06-19
EP0851789A2 (fr) 1998-07-08
WO1997019581A3 (fr) 1997-09-04

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