WO1995018946A1 - Procede et dispositif de deshydratation de materiaux organiques et/ou inorganiques - Google Patents

Procede et dispositif de deshydratation de materiaux organiques et/ou inorganiques Download PDF

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Publication number
WO1995018946A1
WO1995018946A1 PCT/NO1994/000005 NO9400005W WO9518946A1 WO 1995018946 A1 WO1995018946 A1 WO 1995018946A1 NO 9400005 W NO9400005 W NO 9400005W WO 9518946 A1 WO9518946 A1 WO 9518946A1
Authority
WO
WIPO (PCT)
Prior art keywords
liquids
drying
rotor
process chamber
mist
Prior art date
Application number
PCT/NO1994/000005
Other languages
English (en)
Inventor
Olav Ellingsen
Original Assignee
Thermtech A/S
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to NO924421A priority Critical patent/NO176006C/no
Application filed by Thermtech A/S filed Critical Thermtech A/S
Priority to US08/666,567 priority patent/US5724751A/en
Priority to DE69418212T priority patent/DE69418212D1/de
Priority to RU96117256A priority patent/RU2125217C1/ru
Priority to EP94912706A priority patent/EP0736162B1/fr
Priority to AU65139/94A priority patent/AU682860B2/en
Priority to PCT/NO1994/000005 priority patent/WO1995018946A1/fr
Publication of WO1995018946A1 publication Critical patent/WO1995018946A1/fr
Priority to FI962764A priority patent/FI962764A/fi

Links

Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B5/00—Drying solid materials or objects by processes not involving the application of heat
    • F26B5/02—Drying solid materials or objects by processes not involving the application of heat by using ultrasonic vibrations
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/16—Evaporating by spraying
    • B01D1/18—Evaporating by spraying to obtain dry solids
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/34—Treatment of water, waste water, or sewage with mechanical oscillations
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F11/00—Treatment of sludge; Devices therefor
    • C02F11/12—Treatment of sludge; Devices therefor by de-watering, drying or thickening
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F11/00—Treatment of sludge; Devices therefor
    • C02F11/12—Treatment of sludge; Devices therefor by de-watering, drying or thickening
    • C02F11/13—Treatment of sludge; Devices therefor by de-watering, drying or thickening by heating
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B11/00—Machines or apparatus for drying solid materials or objects with movement which is non-progressive
    • F26B11/12—Machines or apparatus for drying solid materials or objects with movement which is non-progressive in stationary drums or other mainly-closed receptacles with moving stirring devices
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B7/00—Drying solid materials or objects by processes using a combination of processes not covered by a single one of groups F26B3/00 and F26B5/00

Definitions

  • the invention relates to a method of drying materials, as disclosed in the preamble of Patent Claim 1.
  • the invention further relates to a device for implementation of the drying of materials, as disclosed in the preamble of Patent Claim 3.
  • the invention relates to a method of removing liquids (drying) from various atomized organic or inorganic materials by transforming part of the liquids into mist acting as vapour or gas, thus saving evaporation heat, reducing energy consumption dramatically compared to pure evaporation of the same liquids.
  • the literature cites a number of different drying systems, in general comprising various ways of supplying energy to the materials with a view to evaporation of the liquids.
  • the reason for this need for different techniques has to do with the type of material, the atomization of the particles, the type of liquid, and not least the thermodynamic values of the materials throughout the process.
  • the prior art comprises the following drying methods and processes: Rotary drying, where the energy is either supplied through a flame blown into the dryer - a so-called through-heat dryer, or by means of thermal conductance elements of various designs (pipes, plates etc. ) - a so-called oil or steam dryer.
  • Fluidized dryer which normally consists of a vertical cylinder with a cloth, or some other perforated plate in the bottom, through which is blown some kind of heated gas, heating the material and expelling the liquids through evaporation.
  • infrared dryer where the energy is delivered as infrared radiation
  • tunnel furnaces different types of tunnel furnaces
  • turbo-driers where the material is dried in a vertical cylinder by means of spinning fans and a countercurrent of hot air or some other heated gas.
  • the objective of the present invention is to show a process or a method of drying such materials using less energy than current drying processes, in that the liquids are not evaporated but removed through the transformation of a considerable portion of the said liquids into mist.
  • x g is the weight proportion of solids
  • c g is specific heat of the solids
  • x y is the weight proportion of the water. If there are several different solids in the material, the equation is expanded for each solid ingredient with its respective weight proportion and specific heat.
  • N V/dV where V is the volume of one litre of water
  • the energy required to form these droplets can be assumed to equal the energy of the total surface tension between water and air.
  • the total surface of the mist droplets is:
  • Total energy is:
  • the equation relates to the cavitation in a liquid when it is exposed to sonic energy. Calculations for differently sized droplets show that the frequency would reside in the area of 10 4 to 10 6 Hz.
  • the materials to be dried are not, however, a homogeneous mass. They might consist of a number of different materials as well as one or more different types of liquids, although the predominant proportion would usually be water.
  • the liquids in such mixtures may exist as a free moveable liquid and as liquid bound by physical forces in the materials, consisting predominantly of capillary forces.
  • the steam pressure needs to conquer the capillary pressure which increases in proportion to the diminishing pore structure.
  • This is achieved by drying the material at a temperature such that the steam pressure conquers the capillary pressure. This will frequently require temperatures far above what is strictly necessary for evaporation.
  • Another aspect affecting pure thermal drying is the fact that the ther odynamic values of the material change during the process. They worsen. This must in its turn be compensated by higher temperatures and larger heating surfaces, which again leads to higher cost of equipment and operations.
  • the elements supplying the sonic and thermal energy to the material need to be able to supply these under such turbulent conditions that all parts of the material are treated.
  • an agitator In a vertical or horizontal cylindrical container, an agitator is arranged driven by a rotating source of energy - an electric engine or combustion engine. On the agitator are devised a series of blades which, when the rotor rotates, are flung outwards by the centrifugal force.
  • an input opening is deviced for the material which is to be dried, an output opening for the dried material, and an opening for the evacuation of steam and mi st ,
  • ribs are arranged running lengthwise over the whole internal periphery of the chamber.
  • the ribs are shaped so as to be approximately parallel with the blades where they pass the ribs.
  • gases, mist and steam leaving the process chamber through the output opening from these may either condense or be led to air - depending on the nature of the gases.
  • Another way of increasing the frequency and thus the mechanical effect on the liquids is to design the blades as tuning forks, so as to be set in natural oscillation on passing the ribs, thus contributing to the sonic energy.
  • they may be electro-magnetically stimulated by a magnetic oscillator arranged on the outside. This is devised so as to allow the magnetic field to go through the wall of the process chamber by designing the said chamber in a non ⁇ magnetic material (such as stainless steel).
  • the magnetic field will affect each of the blades designed as an oscillating element at the same frequency as the magnetic field.
  • a further way of reinforcing the effect would be to arrange a magnetostrictive material on the blades, such as Terfonol ⁇ made from the elements ferrum, terbium and dysprosium. Under the influence of a magnetic field, the alloy will expand by approx. 1-2 o/oo. This expansion may directly influence the blades and thus the material to be treated.
  • Yet another method of establishing a strong sonic field in the process chamber is to mount the ribs on piezoelectric ceramics or magnetostrictive materials.
  • a frequency modulator on the outside to make the ribs oscillate at any chosen frequency within the practical range in question. In the frequency range of 20,000 Hz no movement will be observable in the ribs, as they will be oscillating around their elasticity range.
  • vibrations may be envisaged, such as designing the blades to give off a sound analogous to that of a whistle during movement in the mass. This can be achieved simply and practically by designing the back ' s of the blades so as to form extreme turbulence behind the said blades. Apart from giving off vibrations, the turbulence will also form a lagging vacuum which will render mist formation and evaporation more efficient at a low temperature.
  • the output of dried material starts at a selected operating temperature and humidity.
  • the resulting reduced load on the engine will cause input to start until the load again peaks.
  • the temperature drops and output begins. In a correctly adjusted plant, this will be continuous, so that input will balance output, i.e. output and input will be continuous.
  • Figure 1 shows a schematic view of the process Figure 2 shows a detail of the process chamber and the blade at the moment of passing Figure 3 shows a detail of one of the blades designed as a tuning fork.
  • Figure 4 shows the same fork prestressed with the
  • Figure 5 shows a detail of a rib attached to a piezoelectric or magnetostrictive material.
  • Figure 6 shows a side view of an embodiment example for an apparatus of 450 kW Q .
  • Figure 7 shows a front view of the same embodiment example.
  • Figure 8 shows the embodiment example seen from one end.
  • Figure 1 shows a process chamber with rotor 2 and blades 3 driven by the engine 4.
  • the mass is fed into the process chamber by the feed conveyor 5 from the hopper 6.
  • the feed conveyor is driven by the engine 7.
  • the mass in the process chamber is whipped by the blades 3 and subjected to sonic energy or vibrations from the said blades and the ribs 8.
  • additional energy may be supplied some form of heated gas from the aggregate 9.
  • the gases, mist and vapours leave the process chamber 1 via the output opening via a vent fan 11 and on to either open air or to a condenser.
  • the dried material is led through the output opening 12 via the rotating gate 13.
  • Figure 2 shows, as mentioned, a detail of the process chamber and the blade at the moment of passing.
  • Figure 3 shows a detail of one of the blades designed as a tuning fork.
  • FIG 4 shows the same tuning fork prestressed with the magnetostrictive material Terfonol R 14, with an oscillating magnet generator 15.
  • Figure 5 shows a detail of a rib 4 attached to a piezoelectric or magnetostrictive material 20 receiving oscillating energy via the cables 21 and 22 from the generator 23.
  • Figure 6 where the reference numbers have the same significance as in Figure 1, also shows a screw conveyor 15 for the solids and the machine skid 16 on which the construction is resting. It further shows the blowoff pipe 17 for exhaust gases and mist being led to the open air.
  • the control cabinet 18 for the process is situated at the end of the engine. The whole assembly is built into a 20 foot standard ISO container 19.
  • Figure 7 shows a front view of the same embodiment example, including the blowoff aperture 10 for the exhaust gases and mist, the vent fan 11 and the feed conveyor 5 in the hopper

Landscapes

  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Hydrology & Water Resources (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Organic Chemistry (AREA)
  • General Engineering & Computer Science (AREA)
  • Molecular Biology (AREA)
  • Health & Medical Sciences (AREA)
  • Combustion & Propulsion (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Drying Of Solid Materials (AREA)

Abstract

L'invention se rapporte à un processus/procédé d'élimination des liquides (déshydratation) contenus dans divers matériaux atomisés, organiques ou inorganiques, ce procédé consistant à transformer une partie des liquides en un aérosol qui agit comme la vapeur ou le gaz, ce qui évite la chaleur d'évaporation et réduit considérablement la consommation d'énergie par rapport à celle observée lors de l'évaporation pure des mêmes liquides.
PCT/NO1994/000005 1992-11-17 1994-01-07 Procede et dispositif de deshydratation de materiaux organiques et/ou inorganiques WO1995018946A1 (fr)

Priority Applications (8)

Application Number Priority Date Filing Date Title
NO924421A NO176006C (no) 1992-11-17 1992-11-17 Fremgangsmåte ved törking av materialer
US08/666,567 US5724751A (en) 1994-01-07 1994-01-07 Process and apparatus for drying organic or inorganic materials
DE69418212T DE69418212D1 (de) 1994-01-07 1994-01-07 Verfahren und vorrichtung zur trocknung von organischen und/oder anorganischen materialien
RU96117256A RU2125217C1 (ru) 1992-11-17 1994-01-07 Процесс и устройство для сушки или органических и/или неорганических материалов
EP94912706A EP0736162B1 (fr) 1994-01-07 1994-01-07 Procede et dispositif de deshydratation de materiaux organiques et/ou inorganiques
AU65139/94A AU682860B2 (en) 1994-01-07 1994-01-07 A process and a device in drying of organic and/or unorganic materials
PCT/NO1994/000005 WO1995018946A1 (fr) 1992-11-17 1994-01-07 Procede et dispositif de deshydratation de materiaux organiques et/ou inorganiques
FI962764A FI962764A (fi) 1994-01-07 1996-07-05 Menetelmä ja laite orgaanisten ja/tai epäorgaanisten materiaalien kuivatuksessa

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
NO924421A NO176006C (no) 1992-11-17 1992-11-17 Fremgangsmåte ved törking av materialer
PCT/NO1994/000005 WO1995018946A1 (fr) 1992-11-17 1994-01-07 Procede et dispositif de deshydratation de materiaux organiques et/ou inorganiques

Publications (1)

Publication Number Publication Date
WO1995018946A1 true WO1995018946A1 (fr) 1995-07-13

Family

ID=26648379

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/NO1994/000005 WO1995018946A1 (fr) 1992-11-17 1994-01-07 Procede et dispositif de deshydratation de materiaux organiques et/ou inorganiques

Country Status (3)

Country Link
NO (1) NO176006C (fr)
RU (1) RU2125217C1 (fr)
WO (1) WO1995018946A1 (fr)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2000053535A1 (fr) * 1999-03-05 2000-09-14 Gestión Cerámica Ecológica, S.L. Recuperation et utilisation des boues contenues dans les eaux residuelles de l'industrie de la ceramique
WO2002093094A1 (fr) * 2001-05-16 2002-11-21 Thermtech As Procedes et dispositif pour le sechage de materiaux poisseux
DE102017010890A1 (de) * 2017-11-25 2019-05-29 Martin Wilke Verfahren und Vorrichtung zum Entzug von Wasser aus der Gülle
EP3553437A1 (fr) * 2018-04-13 2019-10-16 Shukhrat Balabekov Dispositif et procédé de séchage, de broyage et de séparation des produits à sécher
CN110482826A (zh) * 2019-07-19 2019-11-22 中国市政工程中南设计研究总院有限公司 基于mvr与真空组合工艺的污泥梯级干化系统及方法

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2007100477A (ru) * 2007-01-12 2008-07-20 Валерий Сергеевич Юрданов (RU) Способ сушки сырья и материалов растительного происхождения
RU2650912C1 (ru) * 2017-03-10 2018-04-18 Вячеслав Вениаминович Костин Способ измельчения и сушки термолабильных материалов и шнековый смеситель для его осуществления

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3808701A (en) * 1971-07-01 1974-05-07 Luwa Ag Apparatus for drying fluent materials
GB1458312A (en) * 1973-04-02 1976-12-15 Simon V Dehydration of manure
WO1993011396A1 (fr) * 1991-12-02 1993-06-10 Buss Ag Installation d'evaporation pour le traitement des boues

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3808701A (en) * 1971-07-01 1974-05-07 Luwa Ag Apparatus for drying fluent materials
GB1458312A (en) * 1973-04-02 1976-12-15 Simon V Dehydration of manure
WO1993011396A1 (fr) * 1991-12-02 1993-06-10 Buss Ag Installation d'evaporation pour le traitement des boues

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2000053535A1 (fr) * 1999-03-05 2000-09-14 Gestión Cerámica Ecológica, S.L. Recuperation et utilisation des boues contenues dans les eaux residuelles de l'industrie de la ceramique
ES2149130A1 (es) * 1999-03-05 2000-10-16 Goterris Manuel Fortuno Recuperacion y utilizacion de los lodos contenidos en las aguas residuales de la industria ceramica.
WO2002093094A1 (fr) * 2001-05-16 2002-11-21 Thermtech As Procedes et dispositif pour le sechage de materiaux poisseux
WO2002092187A1 (fr) * 2001-05-16 2002-11-21 Thermtech As Procede et dispositif permettant de separer du petrole de materiaux renfermant du petrole
US7396433B2 (en) 2001-05-16 2008-07-08 Thermtech As Process and arrangement for separating oil from oil containing materials
DE102017010890A1 (de) * 2017-11-25 2019-05-29 Martin Wilke Verfahren und Vorrichtung zum Entzug von Wasser aus der Gülle
EP3553437A1 (fr) * 2018-04-13 2019-10-16 Shukhrat Balabekov Dispositif et procédé de séchage, de broyage et de séparation des produits à sécher
CN110482826A (zh) * 2019-07-19 2019-11-22 中国市政工程中南设计研究总院有限公司 基于mvr与真空组合工艺的污泥梯级干化系统及方法

Also Published As

Publication number Publication date
NO176006B (no) 1994-10-10
NO924421D0 (no) 1992-11-17
NO176006C (no) 1995-01-18
NO924421L (no) 1994-05-18
RU2125217C1 (ru) 1999-01-20

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