US9522834B2 - Process for removing salts from a processing liquid - Google Patents
Process for removing salts from a processing liquid Download PDFInfo
- Publication number
- US9522834B2 US9522834B2 US14/379,345 US201314379345A US9522834B2 US 9522834 B2 US9522834 B2 US 9522834B2 US 201314379345 A US201314379345 A US 201314379345A US 9522834 B2 US9522834 B2 US 9522834B2
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- United States
- Prior art keywords
- processing liquid
- degassing vessel
- acid
- salts
- gases
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- 239000007788 liquid Substances 0.000 title claims abstract description 60
- 238000000034 method Methods 0.000 title claims abstract description 43
- 150000003839 salts Chemical class 0.000 title claims description 35
- 239000002253 acid Substances 0.000 claims abstract description 35
- 239000007789 gas Substances 0.000 claims abstract description 34
- 238000007872 degassing Methods 0.000 claims abstract description 29
- 239000000203 mixture Substances 0.000 claims abstract description 8
- 150000007513 acids Chemical class 0.000 claims abstract description 4
- 238000006243 chemical reaction Methods 0.000 claims abstract 2
- 238000000354 decomposition reaction Methods 0.000 claims description 5
- 150000001298 alcohols Chemical class 0.000 claims description 3
- 150000002334 glycols Chemical class 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 2
- 239000000356 contaminant Substances 0.000 abstract description 6
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 15
- 229910002092 carbon dioxide Inorganic materials 0.000 description 14
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical class OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 description 12
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- 229910001868 water Inorganic materials 0.000 description 8
- 239000003112 inhibitor Substances 0.000 description 7
- 230000015572 biosynthetic process Effects 0.000 description 6
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 6
- 239000007787 solid Substances 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 5
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 4
- 239000008398 formation water Substances 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 229930195733 hydrocarbon Natural products 0.000 description 3
- 150000002430 hydrocarbons Chemical class 0.000 description 3
- -1 monoethylene glycol) Chemical class 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 150000001342 alkaline earth metals Chemical class 0.000 description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical class OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 150000004677 hydrates Chemical class 0.000 description 2
- 238000002347 injection Methods 0.000 description 2
- 239000007924 injection Substances 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- NMJORVOYSJLJGU-UHFFFAOYSA-N methane clathrate Chemical compound C.C.C.C.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O NMJORVOYSJLJGU-UHFFFAOYSA-N 0.000 description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- MBMLMWLHJBBADN-UHFFFAOYSA-N Ferrous sulfide Chemical compound [Fe]=S MBMLMWLHJBBADN-UHFFFAOYSA-N 0.000 description 1
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 125000005587 carbonate group Chemical group 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000011143 downstream manufacturing Methods 0.000 description 1
- 239000002737 fuel gas Substances 0.000 description 1
- 238000001879 gelation Methods 0.000 description 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
- ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 description 1
- 239000001095 magnesium carbonate Substances 0.000 description 1
- 229910000021 magnesium carbonate Inorganic materials 0.000 description 1
- 235000014380 magnesium carbonate Nutrition 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000003345 natural gas Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000011736 potassium bicarbonate Substances 0.000 description 1
- 235000015497 potassium bicarbonate Nutrition 0.000 description 1
- 229910000028 potassium bicarbonate Inorganic materials 0.000 description 1
- 229910000027 potassium carbonate Inorganic materials 0.000 description 1
- 235000011181 potassium carbonates Nutrition 0.000 description 1
- TYJJADVDDVDEDZ-UHFFFAOYSA-M potassium hydrogencarbonate Chemical compound [K+].OC([O-])=O TYJJADVDDVDEDZ-UHFFFAOYSA-M 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 238000005201 scrubbing Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 230000009919 sequestration Effects 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 235000017550 sodium carbonate Nutrition 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 230000000153 supplemental effect Effects 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
- 238000013022 venting Methods 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F9/00—Multistage treatment of water, waste water or sewage
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D19/00—Degasification of liquids
- B01D19/0005—Degasification of liquids with one or more auxiliary substances
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D19/00—Degasification of liquids
- B01D19/0036—Flash degasification
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
- B01D53/1425—Regeneration of liquid absorbents
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/20—Treatment of water, waste water, or sewage by degassing, i.e. liberation of dissolved gases
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/70—Treatment of water, waste water, or sewage by reduction
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
- B01D53/1456—Removing acid components
- B01D53/1462—Removing mixtures of hydrogen sulfide and carbon dioxide
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
- B01D53/1456—Removing acid components
- B01D53/1468—Removing hydrogen sulfide
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
- B01D53/1456—Removing acid components
- B01D53/1475—Removing carbon dioxide
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/10—Inorganic compounds
Definitions
- the present invention relates to recovering processing liquids used in certain applications. More particularly, the present invention relates to the removal of certain acid decomposable salts prior to reclamation of the processing liquid for reuse.
- Carbonate and bicarbonate salts dissolved in the processing liquids can build up during the reclaiming process leading to undesirable effects. It would clearly be desirable if these salts or other acid decomposable salts could be removed prior to the spent processing liquid entering the reclaiming system.
- certain processing liquids such as alcohols, glycols, alkanolamines and other such materials can be used to prevent gas hydrate formation and/or remove acidic gases in oil and gas production, particularly on offshore platforms.
- Hydrate control is critical to oil and gas production to prevent blockage of production tubing, valves and other equipment with clathrates.
- Hydrate inhibitors may include, but are not limited to, thermodynamic hydrate inhibitors such as alcohols (e.g. methanol) and glycols (e.g. monoethylene glycol), kinetic hydrate inhibitors (e.g. polyvinylcaprolactam, polymers, co-polymers or blends thereof) and anti-agglomerate hydrate inhibitors (e.g.
- N-butyl-N(3-(cocamino)-3-oxopropyl)butan-1-aminium acetate) are injected at or near the production manifold and flow back with the formation water, water of condensation and hydrocarbon phases being produced from the reservoir(s) of interest.
- monoethylene glycol for example, can become contaminated, with, but not limited to, water of condensation, formation water, salts contained in the formation water, flow assurance loop corrosion inhibitors, flow assurance loop corrosion products such as mill scale and iron sulphide.
- Certain contaminants/salts render the hydrate control ability of the selected hydrate inhibitor unusable for reinjection, thus requiring the contaminants to be removed prior to injection.
- the teachings in U.S. Pat. Nos. 5,993,608 and 6,508,916 provide methods and apparatus to carry out such contaminant removal from such a spent processing liquid.
- the carbonate and/or bicarbonate salts can range from relatively low levels in the spent processing liquid to concentrations beyond saturation levels, leading to the potential for formation of crystalline (precipitated) salts.
- these salts are purposefully concentrated beyond saturation levels leading to the formation of crystalline (precipitated) salts.
- a further complication that acid soluble salts can induce is an uncontrolled increase in pH of the processing liquid over time.
- Testing has shown that bicarbonate can dissociate under temperature to carbonate and carbon dioxide. As the carbonate content of the process liquid increases, so does the pH. This may be beneficial for a period of time but if left unchecked extremely high pH values, in the neighbourhood of 12 can be achieved and for glycol based inhibitors it is possible to induce unwanted gelation.
- control on pH levels can be regained and maintained through selective addition
- a process for pretreating a processing liquid to be reclaimed to remove acid decomposable salts and thereby prevent the buildup of crystalline or undissolved versions of such salts in the reclaiming process As one example, if the spent processing solution contains carbonate and/or bicarbonate, it can be treated with an acid such as, but not limited to, hydrochloric acid to decompose the carbonate to CO 2 , water and sodium chloride.
- an acid such as, but not limited to, hydrochloric acid to decompose the carbonate to CO 2 , water and sodium chloride.
- FIG. 1 is a schematic flow diagram of one method of removing acid decomposable salts from a process liquid which is to be subjected to further reclamation.
- FIG. 2 is a schematic view similar to FIG. 1 but showing another aspect of the present invention.
- FIG. 3 is a schematic view similar to FIGS. 1 and 2 but showing yet another aspect of the present invention.
- acid decomposable salts refers to carbonates and/or bicarbonates of alkali and alkaline earth metals such as sodium carbonate, sodium bicarbonate, potassium carbonate, potassium bicarbonate, magnesium carbonate, etc. It is to be understood however that the process of the present invention is applicable to any acid decomposable salts whether or not it is a carbonate or bicarbonate of an alkali and/or alkaline earth metal, the presence of which can deleteriously affect the downstream reclamation process of the processing liquid.
- acids can be employed, the proviso being that the acid does not react with the acid decomposable salt to form other insoluble or slightly soluble salts which would again build up in the process during the reclaiming of the processing liquid.
- acids include hydrochloric acid, certain organic acids, etc.
- a processing liquid is introduced via line 9 into a heat exchanger 10 , wherein it is heated to the desired temperature depending on the nature of the processing liquid, and then passed to a degassing vessel 12 operated at a reduced pressure which in effect causes the entrained acid gases, such as CO 2 and H 2 S, as well as volatile hydrocarbons and other volatile gases to be released from the liquid via line 14 .
- a sweep gas e.g., nitrogen, fuel gas, or any gas which does not deleteriously react with any component in the processing liquid, can be introduced into degassing vessel 12 via line 11 to help flush the entrained gases as well as volatile hydrocarbons from vessel 12 .
- a sweep gas e.g., nitrogen, fuel gas, or any gas which does not deleteriously react with any component in the processing liquid, can be introduced into degassing vessel 12 via line 11 to help flush the entrained gases as well as volatile hydrocarbons from vessel 12 .
- a sweep gas when a sweep gas is used, it will be introduced at
- the proviso is that the contents of line 14 must be maintained in an oxygen free state. If sufficient pressure drop between the heat exchanger 10 and line 14 end point exists to properly remove the desired level of vessel 12 , then addition of the sweep gas is not required.
- the degassed liquid leaving the degassing vessel 12 is then mixed with acid via line 16 , the mixture passing through an inline mixer 18 or other mixing device and introduced into degassing vessel 20 where decomposition gases, e.g., CO 2 from the decomposed salts are removed via line 22 . Removal of the CO 2 from vessel 20 can be facilitated by addition of one of the sweep gases mentioned previously through line 21 at up to a maximum of 10 kg/h to the lower portion of the degassing vessel 20 .
- degassing vessel 20 will preferably operate at a reduced pressure to facilitate removal of the CO 2 gases from the liquid.
- Gases such as CO 2 vented from either degassing vessel 12 or degassing vessel 20 can be collected through a variety of means well known to those skilled in the art.
- the CO 2 can be sent to a low pressure flare header, a CO 2 injection facility, to atmosphere for venting, supplemental compression, sequestration, etc.
- FIG. 2 there is shown a variation of the process of FIG. 1 .
- the processing liquid is passed through heat exchanger 10 to be heated, acid is added via line 16 , and the mixture passed through inline mixer 18 to degassing vessel 20 where CO 2 is released via line 22 , the degassing vessel preferably being under reduced pressure, the processing liquid freed of carbonates/bicarbonates being removed for further processing via line 24 .
- the process in FIG. 2 differs from that in FIG. 1 in that the heating step and the acid addition step can be combined prior to the stream entering any of the degassing vessels. Provision to assist in removal of the CO 2 from vessel 20 can be facilitated as with FIG.
- the heating step may be omitted.
- acid is added to the spent processing liquid via line 16 , the mixture passing through mixer 18 and into degassing vessel 20 operated preferably at a lower pressure, e.g., under vacuum, the CO 2 being removed from the degassing vessel via line 22 , processing liquid freed of carbonate/bicarbonate being removed for further processing via line 24 .
- Sweep gas via line 21 can be applied to this configuration as process conditions require.
- any type of acid can be used to effect the removal of carbonates and/or bicarbonates from the process liquid.
- the acid employed should not react with the carbonate/bicarbonate to form water insoluble or slightly soluble salts or other solids which would simply pose another solids removal problem downstream.
- acid decomposable salts other than carbonates and/or bicarbonates are contemplated provided that the acid decomposition does not result in the formation of aqueous insoluble to slightly soluble salts which could again pose a solids buildup problem in the downstream process.
- the processing liquid can be any liquid that is used in a particular process such that it becomes contaminated with, or at least after use contains, components not normally present in the processing liquid.
- the processing liquid can be one from a gas scrubbing medium used to remove undesirable contaminants from gas streams, a selective solvent to recover desirable components from gases or liquid streams, a medium used to treat solids to selectively remove components of the solids, etc.
- the processing liquid can also be one used in the recovery of natural gas wherein the processing liquid is used to prevent the formation of gas hydrates.
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Organic Chemistry (AREA)
- Analytical Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Gas Separation By Absorption (AREA)
- Treating Waste Gases (AREA)
- Degasification And Air Bubble Elimination (AREA)
- Physical Water Treatments (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Removal Of Specific Substances (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US14/379,345 US9522834B2 (en) | 2012-02-20 | 2013-02-19 | Process for removing salts from a processing liquid |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201261600854P | 2012-02-20 | 2012-02-20 | |
| PCT/US2013/026729 WO2013126346A1 (en) | 2012-02-20 | 2013-02-19 | Process for removing salts from a processing liquid |
| US14/379,345 US9522834B2 (en) | 2012-02-20 | 2013-02-19 | Process for removing salts from a processing liquid |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| US20150034567A1 US20150034567A1 (en) | 2015-02-05 |
| US9522834B2 true US9522834B2 (en) | 2016-12-20 |
Family
ID=49006137
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US14/379,345 Active 2033-04-04 US9522834B2 (en) | 2012-02-20 | 2013-02-19 | Process for removing salts from a processing liquid |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US9522834B2 (da) |
| EP (1) | EP2817074B1 (da) |
| KR (1) | KR102047042B1 (da) |
| CN (1) | CN104271210B (da) |
| AU (1) | AU2013222631B2 (da) |
| BR (1) | BR112014020401B1 (da) |
| CA (1) | CA2864981C (da) |
| CY (1) | CY1120694T1 (da) |
| DK (1) | DK2817074T3 (da) |
| EA (1) | EA027854B1 (da) |
| IN (1) | IN2014KN01731A (da) |
| MX (1) | MX353048B (da) |
| WO (1) | WO2013126346A1 (da) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10221364B2 (en) * | 2013-08-12 | 2019-03-05 | NexoSolutions LLC | System for the treatment of a contaminated hydrocarbon streams |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101654457B1 (ko) | 2015-01-30 | 2016-09-05 | 경희대학교 산학협력단 | 고분자 나노층을 포함하는 생체재료 및 이의 제조방법 |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3119752A (en) | 1959-01-30 | 1964-01-28 | Singmaster & Breyer | Recovery of fresh water from sea water |
| EP0077492A2 (de) | 1981-10-21 | 1983-04-27 | Linde Aktiengesellschaft | Verfahren und Vorrichtung zum Regulieren des NH3-Gehaltes in der Waschflüssigkeit einer Gaswäsche |
| US4417961A (en) | 1981-03-30 | 1983-11-29 | The Dow Chemical Company | Membrane cell brine feed |
| WO2007073204A1 (en) | 2005-12-21 | 2007-06-28 | Statoilhydro Asa | Process and plant for the regeneration of glycol |
| CA2564590A1 (en) | 2006-10-19 | 2008-04-19 | Bitmin Resources Inc. | Method for treating a process water to obtain carbon dioxide therefrom |
| US20090032446A1 (en) | 2007-08-01 | 2009-02-05 | Triwatech, L.L.C. | Mobile station and methods for diagnosing and modeling site specific effluent treatment facility requirements |
| WO2010061811A1 (ja) | 2008-11-27 | 2010-06-03 | 栗田工業株式会社 | アミノ基を有する水溶性有機溶媒の分離回収装置及び方法 |
| EP2439176A1 (en) | 2010-10-07 | 2012-04-11 | EnCana Corporation | Treatment of water for use in hydraulic fracture stimulation |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA1325401C (en) | 1988-07-18 | 1993-12-21 | Dwight Merritt | Process and apparatus for reclaiming waste gas treating chemical |
| US5389208A (en) | 1988-07-18 | 1995-02-14 | Canadian Chemical Reclaiming Ltd. | Process for reclaiming and/or concentrating waste aqueous solutions of gas treating chemicals |
| US5993608A (en) | 1997-04-25 | 1999-11-30 | Canadian Chemical Reclaiming Ltd. | Process for recovering processing liquids |
| US6508916B1 (en) | 1999-06-14 | 2003-01-21 | Canadian Chemical Reclaiming Ltd. | Process for recovering processing liquids |
| CN100537456C (zh) * | 2004-11-05 | 2009-09-09 | 浙江欧美环境工程有限公司 | 一种工业超纯水的制备工艺 |
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2013
- 2013-02-19 BR BR112014020401-2A patent/BR112014020401B1/pt active IP Right Grant
- 2013-02-19 IN IN1731KON2014 patent/IN2014KN01731A/en unknown
- 2013-02-19 WO PCT/US2013/026729 patent/WO2013126346A1/en active Application Filing
- 2013-02-19 CA CA2864981A patent/CA2864981C/en active Active
- 2013-02-19 US US14/379,345 patent/US9522834B2/en active Active
- 2013-02-19 EP EP13752043.3A patent/EP2817074B1/en active Active
- 2013-02-19 DK DK13752043.3T patent/DK2817074T3/da active
- 2013-02-19 AU AU2013222631A patent/AU2013222631B2/en active Active
- 2013-02-19 KR KR1020147024836A patent/KR102047042B1/ko active IP Right Grant
- 2013-02-19 EA EA201491563A patent/EA027854B1/ru unknown
- 2013-02-19 CN CN201380020673.7A patent/CN104271210B/zh active Active
- 2013-02-19 MX MX2014009985A patent/MX353048B/es active IP Right Grant
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| US3119752A (en) | 1959-01-30 | 1964-01-28 | Singmaster & Breyer | Recovery of fresh water from sea water |
| US4417961A (en) | 1981-03-30 | 1983-11-29 | The Dow Chemical Company | Membrane cell brine feed |
| EP0077492A2 (de) | 1981-10-21 | 1983-04-27 | Linde Aktiengesellschaft | Verfahren und Vorrichtung zum Regulieren des NH3-Gehaltes in der Waschflüssigkeit einer Gaswäsche |
| WO2007073204A1 (en) | 2005-12-21 | 2007-06-28 | Statoilhydro Asa | Process and plant for the regeneration of glycol |
| CA2564590A1 (en) | 2006-10-19 | 2008-04-19 | Bitmin Resources Inc. | Method for treating a process water to obtain carbon dioxide therefrom |
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| WO2010061811A1 (ja) | 2008-11-27 | 2010-06-03 | 栗田工業株式会社 | アミノ基を有する水溶性有機溶媒の分離回収装置及び方法 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| US10221364B2 (en) * | 2013-08-12 | 2019-03-05 | NexoSolutions LLC | System for the treatment of a contaminated hydrocarbon streams |
Also Published As
| Publication number | Publication date |
|---|---|
| AU2013222631A1 (en) | 2014-09-11 |
| CA2864981C (en) | 2020-06-16 |
| EA201491563A1 (ru) | 2014-12-30 |
| EP2817074A4 (en) | 2015-10-07 |
| IN2014KN01731A (da) | 2015-10-23 |
| BR112014020401B1 (pt) | 2021-09-21 |
| EP2817074A1 (en) | 2014-12-31 |
| DK2817074T3 (da) | 2018-10-22 |
| CY1120694T1 (el) | 2019-12-11 |
| EA027854B1 (ru) | 2017-09-29 |
| CA2864981A1 (en) | 2013-08-29 |
| US20150034567A1 (en) | 2015-02-05 |
| EP2817074B1 (en) | 2018-07-11 |
| WO2013126346A1 (en) | 2013-08-29 |
| CN104271210A (zh) | 2015-01-07 |
| CN104271210B (zh) | 2018-01-09 |
| MX353048B (es) | 2017-12-18 |
| KR20140127304A (ko) | 2014-11-03 |
| MX2014009985A (es) | 2015-05-11 |
| BR112014020401A2 (pt) | 2020-10-27 |
| AU2013222631B2 (en) | 2017-01-12 |
| KR102047042B1 (ko) | 2019-11-20 |
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