US826389A - Chlorated explosive. - Google Patents
Chlorated explosive. Download PDFInfo
- Publication number
- US826389A US826389A US28936705A US1905289367A US826389A US 826389 A US826389 A US 826389A US 28936705 A US28936705 A US 28936705A US 1905289367 A US1905289367 A US 1905289367A US 826389 A US826389 A US 826389A
- Authority
- US
- United States
- Prior art keywords
- explosive
- chlorated
- chlorate
- materials
- mass
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000002360 explosive Substances 0.000 title description 3
- XTEGARKTQYYJKE-UHFFFAOYSA-M Chlorate Chemical compound [O-]Cl(=O)=O XTEGARKTQYYJKE-UHFFFAOYSA-M 0.000 description 10
- 239000000463 material Substances 0.000 description 6
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 239000011248 coating agent Substances 0.000 description 3
- 238000000576 coating method Methods 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 238000000354 decomposition reaction Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- DYSXLQBUUOPLBB-UHFFFAOYSA-N 2,3-dinitrotoluene Chemical compound CC1=CC=CC([N+]([O-])=O)=C1[N+]([O-])=O DYSXLQBUUOPLBB-UHFFFAOYSA-N 0.000 description 1
- SPSSULHKWOKEEL-UHFFFAOYSA-N 2,4,6-trinitrotoluene Chemical compound CC1=C([N+]([O-])=O)C=C([N+]([O-])=O)C=C1[N+]([O-])=O SPSSULHKWOKEEL-UHFFFAOYSA-N 0.000 description 1
- RMBFBMJGBANMMK-UHFFFAOYSA-N 2,4-dinitrotoluene Chemical compound CC1=CC=C([N+]([O-])=O)C=C1[N+]([O-])=O RMBFBMJGBANMMK-UHFFFAOYSA-N 0.000 description 1
- USXDFAGDIOXNML-UHFFFAOYSA-N Fulminate Chemical compound [O-][N+]#[C-] USXDFAGDIOXNML-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- XTEGARKTQYYJKE-UHFFFAOYSA-N chloric acid Chemical class OCl(=O)=O XTEGARKTQYYJKE-UHFFFAOYSA-N 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000013016 damping Methods 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000005065 mining Methods 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- VLTRZXGMWDSKGL-UHFFFAOYSA-M perchlorate Inorganic materials [O-]Cl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-M 0.000 description 1
- VLTRZXGMWDSKGL-UHFFFAOYSA-N perchloric acid Chemical compound OCl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-N 0.000 description 1
- OXNIZHLAWKMVMX-UHFFFAOYSA-N picric acid Chemical compound OC1=C([N+]([O-])=O)C=C([N+]([O-])=O)C=C1[N+]([O-])=O OXNIZHLAWKMVMX-UHFFFAOYSA-N 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 230000002269 spontaneous effect Effects 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011269 tar Substances 0.000 description 1
- 150000003613 toluenes Chemical class 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B47/00—Compositions in which the components are separately stored until the moment of burning or explosion, e.g. "Sprengel"-type explosives; Suspensions of solid component in a normally non-explosive liquid phase, including a thickened aqueous phase
- C06B47/14—Compositions in which the components are separately stored until the moment of burning or explosion, e.g. "Sprengel"-type explosives; Suspensions of solid component in a normally non-explosive liquid phase, including a thickened aqueous phase comprising a solid component and an aqueous phase
Definitions
- the coating materials used alone the coating materials attenuate the sensitiveness of the chlorate to such an extent that the explosive mixture explodes only with difiiculty under the shock of the fulminate and the decomposition is incomplete oreven impossible if the charge, though small, is arranged so as to form a row of cartridges, as is usual in mining'g erations.
- the inflammability however grea "'it may be, is never such that the simple .i 'tion of the on, and the ustion is too slow.
- the result is the same and the manufacture often more com plicated lfexciting materials be used with the coating material, the coating material the reaction of t e excitant from ta -ingplac e..
- the improvement constituting my invention obviates these disadvantages and consists as follows: First, melt in avessel heat-' ed by steam or hot water a solid nitrated derivative of t0luenosuch as paranitroto- 'luol, dinitrotoluol, trinitrotoluol, or a mixture of these bodies, which may be liquid; second, 'incor orate in the liquid thus obtained the chl orate or perchlorate of potassium or other chlorate or finely-ground state; third, a low the mass to cool until crystallization takes place ;fourth,
- a process which consists in melting a solid nitrated derivativeof toluene and incorporating in the liquid mass a chlorate'salt.
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Bridges Or Land Bridges (AREA)
Description
UNITED ST TES PATEN T OFFICE.
LEoN'THoMAs, OF PARIS, FRANCE.
' OHLORATYED -EXPLO-S'I'VE.
No. 826,389. r
Specification of Letters Patent.
.Patentecl July 17, 1906.
Application filed November 27, 1905. Serial No. 289.367.
. come by various means; but the processes charge can alone be depende com hitherto in use are lengthy and expensive and sometimes exceed the desired efi'ect, the said rocesses being generally based on the coatmg of thechlorate with mineral or vegetable, fatssuch as oils, tars, paratfins, or resinseither alone or mixed with other combustible or exciting materials by simple juxtaposition or by dissolution. Used alone the coating materials attenuate the sensitiveness of the chlorate to such an extent that the explosive mixture explodes only with difiiculty under the shock of the fulminate and the decomposition is incomplete oreven impossible if the charge, though small, is arranged so as to form a row of cartridges, as is usual in mining'g erations. The inflammability, however grea "'it may be, is never such that the simple .i 'tion of the on, and the ustion is too slow. The result is the same and the manufacture often more com plicated lfexciting materials be used with the coating material, the coating material the reaction of t e excitant from ta -ingplac e.. On the other hand, s eve'ralof these exciting -acting as a damping obstacle and reventing materials such as sulfur in the free state or in combination, picric acid, and raw tarare liable, owing to their natural or acquired acidity, toeventually cause sudden and spontaneous decompositions.
The improvement constituting my invention obviates these disadvantages and consists as follows: First, melt in avessel heat-' ed by steam or hot water a solid nitrated derivative of t0luenosuch as paranitroto- 'luol, dinitrotoluol, trinitrotoluol, or a mixture of these bodies, which may be liquid; second, 'incor orate in the liquid thus obtained the chl orate or perchlorate of potassium or other chlorate or finely-ground state; third, a low the mass to cool until crystallization takes place ;fourth,
to obtainit in ulverulent form sift this mass to the require size of grain.
put up in cartridges in the usual or any suitable way.
The following formula gives an example of such explosives, the (proportions of which may of course be varie according to requirements: dinitrotoluene, twenty-five per cent; chlorate, seventy-five per cent.
What I claim is.
1. A process which consists in melting a solid nitrated derivativeof toluene and incorporating in the liquid mass a chlorate'salt.
2. An article of manufacture consisting of a mixture of a nitrated derivative of toluene and a chlorate salt. A
In testimony whereof I have hereunto set my hand in presence oftwo subscribing witnesses.
A LEON. THOMAS.
-Witnesses:
' f" @PIERRE LEIKE,
:EMILE KLOTE.
erclilorate in a It may then be I
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US28936705A US826389A (en) | 1905-11-27 | 1905-11-27 | Chlorated explosive. |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US28936705A US826389A (en) | 1905-11-27 | 1905-11-27 | Chlorated explosive. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US826389A true US826389A (en) | 1906-07-17 |
Family
ID=2894869
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US28936705A Expired - Lifetime US826389A (en) | 1905-11-27 | 1905-11-27 | Chlorated explosive. |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US826389A (en) |
-
1905
- 1905-11-27 US US28936705A patent/US826389A/en not_active Expired - Lifetime
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