US5487602A - Multi-screw, extrusion-compounding machine with modular mixing elements - Google Patents

Multi-screw, extrusion-compounding machine with modular mixing elements Download PDF

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Publication number
US5487602A
US5487602A US08/253,397 US25339794A US5487602A US 5487602 A US5487602 A US 5487602A US 25339794 A US25339794 A US 25339794A US 5487602 A US5487602 A US 5487602A
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US
United States
Prior art keywords
modular mixing
symmetrical
mixing element
screw
extrusion
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US08/253,397
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English (en)
Inventor
Lefteris N. Valsamis
Eduardo L. Canedo
Jose M. Pereira
Douglas V. Poscich
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Farrel Corp
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Farrel Corp
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Assigned to FARREL CORPORATION reassignment FARREL CORPORATION ASSIGNMENT OF ASSIGNORS INTEREST (SEE DOCUMENT FOR DETAILS). Assignors: CANEDO, EDUARDO L., PEREIRA, JOSE M., POSCICH, DOUGLAS V., VALSAMIS, LEFTERIS N.
Priority to US08/253,397 priority Critical patent/US5487602A/en
Priority to TW084104470A priority patent/TW261569B/zh
Priority to EP95921588A priority patent/EP0764074B1/en
Priority to MXPA/A/1996/006025A priority patent/MXPA96006025A/xx
Priority to RU97100147A priority patent/RU2145281C1/ru
Priority to CA002191860A priority patent/CA2191860C/en
Priority to KR1019960706886A priority patent/KR100204118B1/ko
Priority to JP8501230A priority patent/JP2912021B2/ja
Priority to PCT/US1995/007025 priority patent/WO1995033608A1/en
Priority to CN95193412A priority patent/CN1051494C/zh
Priority to BR9508698A priority patent/BR9508698A/pt
Priority to AU26616/95A priority patent/AU680372B2/en
Priority to DK95921588T priority patent/DK0764074T3/da
Priority to AT95921588T priority patent/ATE197569T1/de
Priority to PL95317539A priority patent/PL177289B1/pl
Priority to DE69519431T priority patent/DE69519431T2/de
Priority to ES95921588T priority patent/ES2152403T3/es
Publication of US5487602A publication Critical patent/US5487602A/en
Application granted granted Critical
Assigned to LASALLE BUSINESS CREDIT, LLC reassignment LASALLE BUSINESS CREDIT, LLC SECURITY AGREEMENT Assignors: FARREL CORPORATION
Assigned to FARREL CORPORATION reassignment FARREL CORPORATION RELEASE OF SECURITY AGREEMENT Assignors: BANK OF AMERICA AS SUCCESSOR BY MERGER TO LASALLE BUSINESS CREDIT, LLC
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00—Mixing; Kneading
    • B29B7/30—Mixing; Kneading continuous, with mechanical mixing or kneading devices
    • B29B7/34—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices
    • B29B7/38—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary
    • B29B7/46—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with more than one shaft
    • B29B7/48—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with more than one shaft with intermeshing devices, e.g. screws
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00—Mixing; Kneading
    • B29B7/30—Mixing; Kneading continuous, with mechanical mixing or kneading devices
    • B29B7/34—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices
    • B29B7/38—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary
    • B29B7/46—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with more than one shaft
    • B29B7/465—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with more than one shaft each shaft comprising rotor parts of the Banbury type in addition to screw parts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00—Mixing; Kneading
    • B29B7/30—Mixing; Kneading continuous, with mechanical mixing or kneading devices
    • B29B7/34—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices
    • B29B7/38—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary
    • B29B7/46—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with more than one shaft
    • B29B7/48—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with more than one shaft with intermeshing devices, e.g. screws
    • B29B7/482—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with more than one shaft with intermeshing devices, e.g. screws provided with screw parts in addition to other mixing parts, e.g. paddles, gears, discs
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00—Mixing; Kneading
    • B29B7/30—Mixing; Kneading continuous, with mechanical mixing or kneading devices
    • B29B7/34—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices
    • B29B7/38—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary
    • B29B7/46—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with more than one shaft
    • B29B7/48—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with more than one shaft with intermeshing devices, e.g. screws
    • B29B7/482—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with more than one shaft with intermeshing devices, e.g. screws provided with screw parts in addition to other mixing parts, e.g. paddles, gears, discs
    • B29B7/483—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with more than one shaft with intermeshing devices, e.g. screws provided with screw parts in addition to other mixing parts, e.g. paddles, gears, discs the other mixing parts being discs perpendicular to the screw axis
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00—Mixing; Kneading
    • B29B7/30—Mixing; Kneading continuous, with mechanical mixing or kneading devices
    • B29B7/34—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices
    • B29B7/38—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary
    • B29B7/46—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with more than one shaft
    • B29B7/48—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with more than one shaft with intermeshing devices, e.g. screws
    • B29B7/488—Parts, e.g. casings, sealings; Accessories, e.g. flow controlling or throttling devices
    • B29B7/489—Screws
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
    • B29C48/25—Component parts, details or accessories; Auxiliary operations
    • B29C48/251—Design of extruder parts, e.g. by modelling based on mathematical theories or experiments
    • B29C48/2517—Design of extruder parts, e.g. by modelling based on mathematical theories or experiments of intermeshing screws
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
    • B29C48/25—Component parts, details or accessories; Auxiliary operations
    • B29C48/256—Exchangeable extruder parts
    • B29C48/2564—Screw parts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
    • B29C48/25—Component parts, details or accessories; Auxiliary operations
    • B29C48/36—Means for plasticising or homogenising the moulding material or forcing it through the nozzle or die
    • B29C48/395—Means for plasticising or homogenising the moulding material or forcing it through the nozzle or die using screws surrounded by a cooperating barrel, e.g. single screw extruders
    • B29C48/40—Means for plasticising or homogenising the moulding material or forcing it through the nozzle or die using screws surrounded by a cooperating barrel, e.g. single screw extruders using two or more parallel screws or at least two parallel non-intermeshing screws, e.g. twin screw extruders
    • B29C48/402—Means for plasticising or homogenising the moulding material or forcing it through the nozzle or die using screws surrounded by a cooperating barrel, e.g. single screw extruders using two or more parallel screws or at least two parallel non-intermeshing screws, e.g. twin screw extruders the screws having intermeshing parts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
    • B29C48/03—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor characterised by the shape of the extruded material at extrusion

Definitions

  • the invention relates to the field of co-rotating, intermeshing, multi-screw, extrusion-compounding machines for plastic material.
  • the invention relates to such machines having co-rotation screws incorporating sets of modular mixing elements of non-symmetrical geometries with relatively large wing tip clearances and wherein such sets of non-symmetrical modular mixing elements can be mounted at any suitable axial location along their respective screw shafts, wherein usage of kneading blocks or kneading discs may be avoided.
  • Intermeshing co-rotating twin-screw extruders as known in the art conventionally utilize a number of different elements mounted along the respective extruder shafts according to a sequence of process functions that the extruder is to perform.
  • the screws in such an extruder include a number of transporting (forward-conveying) screw elements designed to accept the plastic material and additives and to convey them to a special section of the extruder dedicated to transforming the plastic material into a thermally homogeneous compound melt including the additives.
  • This special section of the extruder conventionally includes a number of kneading elements, usually in the form of blocks or discs, designed to impart high energy per unit volume into the plastic material with the additives. Rotational drive energy imparted to the kneading elements on the extruder screws is dissipated into the plastic material causing heating and inducing mixing of the various additives into a plastic compound melt.
  • kneading elements conventionally employ a special cross-section profile which is designed to provide "effective scraping" (very small clearances such as a millimeter or less) between adjacent kneading elements and usually also effective scraping between an outer diameter of the kneading element and the inner wall of the barrel.
  • "effective scraping" very small clearances such as a millimeter or less
  • intensive energy is dissipated in the kneading section of the extruder, producing localized extreme heating. This heat energy, if not promptly and continuously removed, results in overheating of the compound melt with possible degradation of the plastic material.
  • kneading discs in general are their capability of generating localized high pressures, especially in the vicinity of the kneading disc tip. These localized high pressures result in shaft-deflecting forces which push the screw shafts towards the inner surfaces of the barrel walls, thus accelerating wear of the extruder. From a process point-of-view, such localized high pressures may re-fuse back together and agglomerate solid particles previously broken apart, thereby acting contrary to the objective of obtaining a homogeneous compound melt. Additionally, in such prior machines when dealing with dispersive or extensive mixing, various different fluid particles are being exposed to highly non-uniform kneading shear rates. Consequently, the kneading shearing action must be repeated many times to ensure that all fluid particles have been exposed to equal levels of shear and/or thermal history.
  • the invention is shown embodied in extrusion-compounding machines having co-rotating, intermeshing screws incorporating modular mixing elements of identical geometries having relatively large clearances and wherein their non-symmetrical geometries provide dynamic wedging pressurization for driving relatively large circumferential flows of the plastic material through large shear clearances.
  • the large circumferential flows of plastic material are driven repeatedly by dynamic wedging pressurization action so as to pass repeatedly through the large shear clearances.
  • the plastic material is being mixed at lower and more uniform temperatures than usually occurs with use of typical prior art kneading elements. In most plastic materials viscosity diminishes with elevating temperatures.
  • modular mixing elements can be arranged and assembled in various sets in a wide range of axial positions and configurations for enhancing processing characteristics, zonal temperature levels and magnitudes and axial locations of dynamic wedging-shearing actions within the twin barrels and for matching these dynamic effects with desired properties of plastic materials and additives being compounded.
  • FIG. 1 is a schematic longitudinal side elevational sectional view of a multi-screw, extrusion-compounding machine having intermeshing, co-rotating twin screws (only one is seen in FIG. 1) incorporating non-symmetrical modular mixing elements having relatively large wing tip clearances.
  • FIGS. 1A and 1B are enlargements of portions of FIG. 1 wherein a respective set of modular mixing elements is shown in each FIGURE.
  • FIG. 2 is an enlarged cross-sectional view looking downstream taken along either of the planes 2--2 in FIG. 1 or along the plane 2--2 in FIG. 1A or plane 2--2 in FIG. 1B near upstream ends of respective modular mixing elements.
  • FIG. 3 is a further enlarged view of one of the modular mixing elements of FIG. 2 for purposes of explaining advantageous non-symmetrical geometric relationships provided in these modular mixing elements.
  • FIG. 3A shows an upper half of FIG. 3 for purposes of further explanation.
  • FIG. 3B is a further enlargement of the top half of FIGS. 3 and 3A for purposes of explanation.
  • FIGS. 4A and 4B are end elevational and side elevational views, respectively, of a non-symmetrical modular mixing element with two axially-extending wings each having a right-hand (“RH") twist.
  • An RH twist is a forward-pumping twist, which may also be referred to as a downstream-pumping twist.
  • FIG. 4A is an end view of the mixing element in FIG. 4B as seen looking upstream, as indicated by arrows 4A--4A.
  • FIG. 4B is a side view of the mixing element in FIG. 4A, as shown by arrows 4B--4B.
  • FIGS. 5A and 5B are end elevational and side elevational views, respectively, of another non-symmetrical modular mixing element similar to that shown in FIGS. 4A and 4B, except that the two axially-extending wings each have a left-hand (“LH") twist.
  • An LH twist is a reverse-pumping twist, which may also be referred to as an upstream-pumping twist.
  • FIG. 5A is an end view of the mixing element in FIG. 5B as seen looking upstream, as shown by arrows 5A--5A.
  • FIG. 5B is a side view of the mixing element in FIG. 5A, as indicated by arrows 5B--5B.
  • FIGS. 6A and 6B are end elevational and side elevational views, respectively, of an RH-twist non-symmetrical modular mixing element like that shown in FIGS. 4A and 4B, expect that the element shown in FIGS. 6 has two-thirds of the axial length of the element shown in FIGS. 4.
  • FIG. 6A is an end view of the element in FIG. 6B as seen looking upstream, as indicated by arrows 6A--6A.
  • FIG. 6B is a side view of the element in FIG. 6A, as shown by arrows 6B--6B.
  • FIGS. 7A and 7B are end elevational and side elevational views, respectively, of an LH-twist non-symmetrical modular mixing element like that shown in FIGS. 5A and 5B, except the element shown in FIGS. 7 has two-thirds of the axial length of the element shown in FIGS. 5.
  • FIG. 7A is an end view of the element in FIG. 7B as seen looking upstream, as indicated by arrows 7A--7A.
  • FIG. 7B is a side view of the element in FIG. 7A, as indicated by arrows 7B--7B.
  • FIG. 8 is a cross-sectional profile view of a non-symmetrical modular mixing element taken along any of the respective planes 8--8 in FIGS. 4B, 5B, 6B or 7B.
  • This profile view of a modular mixing element is shown superimposed upon a twin-screw ideal self-wiping profile (shown shaded).
  • twin-screw ideal self-wiping profile is the maximum proportional area of such a profile which can be utilized in a co-rotating, intermeshing twin-screw extruder wherein the screw is continuously in contact with its co-rotating twin and also is continuously in contact with the inner surface of a cylindrical-shaped barrel wall of an extruder housing.
  • the comparison of profiles in FIG. 8 serves to emphasize the relatively large clearances provided around these non-symmetrical modular mixing elements.
  • FIGS. 1, 2, 3 and 3A show a multi-screw extrusion-compounding machine 20 having twin intermeshing co-rotating screws 21 and 22. Since FIG. 1 is a side elevational sectional view, only one of the screws 21 is seen. A downstream direction through the machine 20 is shown by an arrow 23.
  • a housing 24 for the screws 21 and 22 comprises a plurality of barrel segments 26-1 through 26-9 inclusive which are removably interconnected in axially aligned positions by suitable disconnectable fastening means as known in the art.
  • the first barrel segment 26-1 is shown having an inlet opening 25 for infeed into the housing of suitable materials indicated by arrow 27 to be processed.
  • a suitable drive mechanism 28 is shown with mechanical connections indicated by dashed line 29 to respective round shafts 30 (FIG. 2) of the screws 21 and 22 for rotating both screws at the same speed in the same direction.
  • Such a drive mechanism 28 and mechanical connections 29 with suitable thrust bearings are known in the art.
  • the direction of rotation of screws 21 and 22 around their respective axes 31 and 32 may be counterclockwise, as is indicated by arrows 34' as seen looking in downstream direction 23 along the screw axes 31 and 32. It is noted that counterclockwise rotation shown by arrows 34' as seen when looking downstream along these axes 31 and 32 is the same direction of rotation as clockwise rotation shown by arrows 34 as seen when looking upstream along these screw axes.
  • the seventh barrel segment 26-7 is shown having a vent port 36 for releasing volatiles indicated by an arrow 37.
  • the ninth barrel segment 26-9 at a downstream end of the housing 24 defines the outlet mouth 38 of the housing from which issues a compounded extrudate indicated by arrow 39.
  • a downstream tip end 33 of the shaft 30 of the screw 21 is seen at the right in FIG. 1. It is understood that a suitable die (not shown) normally is mounted to the outlet mouth 38, and the extrudate 39 exits from the machine 20 through such a die.
  • Each round screw shaft 30 includes one or more keyways 40 (FIG. 2) extending longitudinally of the respective shaft parallel with the respective axis 31 or 32 for receiving keys 42 engaging in corresponding keyways 44 in the elements mounted on the shaft for providing a positive rotational drive connection between each round screw shaft 30 and the elements removably mounted thereon.
  • each screw 21 and 22 includes a plurality of intermeshing co-rotating transport screw elements 45 and 46 mounted end-to-end on and keyed to their respective shafts.
  • transport screw elements 46 are longer than screw elements 45, and the helical screw flights 49 of elements 46 have a proportionately longer lead than the helical screw flights 47 of elements 45 for rapidly transporting infed materials 27 downstream away from the inlet 25.
  • Each of the transport screw elements 45 and 46 is shown having two helical screw flights 47 or 49, respectively. Each such flight extends around its respective screw axis 31 or 32 for one complete turn, i.e. 360°.
  • the infed materials 27 include suitable plastic material and suitable additives to be compounded and mixed in the machine 20.
  • Transport screw elements 45 and 46 in the respective screws 21 and 22 convey these materials to be processed to a first set 50-1 of modular mixing elements 51 and 52 mounted end-to-end on their respective shafts 30.
  • a mixing set 50-1 as shown includes an RH-twist non-symmetrical modular mixing element 51 contiguous with and positioned immediately upstream from an LH-twist non-symmetrical modular mixing element 52. It is noted, as seen most clearly in FIG. 1A, that the two helical screw flights 47 of the transport screw element 45 which is positioned immediately upstream of the modular mixing element 51 are aligned with respective wing tips 60 (FIGS.
  • the two wing tips 60 of the mixing element 51 effectively form downstream continuations of the two helical screw flights 47, but the helix angle and lead of the wing tips 60 are different from the helix angle and lead of the screw flights 47. In other words, there is a sharp change (decrease) in helical twist at the junctures where the respective helical screw flights 47 are met by the respective wing tips 60.
  • FIG. 1B Downstream from the first mixing set 50-1 in the respective screw 21 or 22 is another mixing set 50-2 (FIG. 1B) shown comprising non-symmetrical modular mixing elements 53 and 54 (FIGS. 6A, 6B and 7A, 7B, respectively).
  • a plurality of contiguous, sequentially-assembled transport screw elements 45 mounted on and keyed to the respective shaft 30.
  • Four of the elements 45 are shown, plus a short screw transport element 48 wherein its two helical screw flights 47 each extend around its respective axis 31 or 32 for one-half of a complete turn, i.e. 180°. It is noted, as seen most clearly in FIG.
  • the two flights 47 of the short screw transport element 48 are aligned with the wing tips 60 of wings 66 (FIGS. 2, 6A and 6B) of modular mixing element 53 so that these wing tips effectively form downstream continuations of these screw flights 47, but there is a sharp change (decrease) in helical twist at the junctures between these screw flights and the contiguous downstream wing tips 60.
  • a final sequence of screw transport elements comprising in sequence: two screw elements 45, two longer screw elements 46 with flights 49 of lower helical pitch and longer lead located near the vent 36 and seven more screw elements 45.
  • This final sequence of seven screw elements 45 serves for building pressure to expel the extrudate 39 through a die (not shown) at the outlet mouth 38.
  • the longer screw elements 46 with their longer lead normally provide increased speed of downstream conveyance for preventing complete filling of the barrels near vent 36 for facilitating release of volatiles 37.
  • each shaft end 33 includes suitable fastening means for example such as a retainer nut, with a washer, threaded onto the shaft end for capturing and holding the string of assembled elements 45, 46, 51, 52, 45, 48, 53, 54, 45, 46 and 45 mounted on their respective shafts 30 for forming the screws 21 and 22.
  • suitable fastening means for example such as a retainer nut, with a washer, threaded onto the shaft end for capturing and holding the string of assembled elements 45, 46, 51, 52, 45, 48, 53, 54, 45, 46 and 45 mounted on their respective shafts 30 for forming the screws 21 and 22.
  • each screw 21 and 22 the two flights 47 of the transport element 45 positioned immediately downstream from the modular mixing element 54 of the second mixing set 50-2, as seen more clearly in FIG. 1B, are aligned with the tips 60 of wings 68 (FIGS. 7A and 7B) of this mixing element effectively forming downstream continuations of the wing tips 60 of wings 68.
  • plastic material is intended to include any suitable plastic material or materials which may include any suitable additives for compounding in the extrusion-compounding machine 20.
  • keyway "key” and “keyed” are intended to be interpreted sufficiently broadly to include other equivalent means, for example, such as a spline, for providing a positive rotational drive relationship between a rotationally-driven shaft and a transport screw element or a non-symmetrical modular mixing element removably mounted on such shaft and being rotationally driven by the shaft.
  • D internal diameter (ID) of a barrel wall which also may be referred to as the barrel bore diameter or barrel inner diameter
  • ⁇ ⁇ 1 / ⁇ tip symmetry coefficient.
  • ranges are selected for the six independent variables, then resultant ranges for the dependent variables can be computed.
  • the six independent variables cannot be selected arbitrarily but are constrained by parameters, such as ⁇ 0, etc., which result in a series of complex bounds for all of them.
  • there are preferred, more preferred and most preferred ranges for the six independent variables as will be explained later, for enhancing the processing characteristics of extrusion-compounding machines in handling various plastic materials and additives being compounded.
  • the housing assembly 24 is shown including two adjoining barrel sections 83 and 84 having respective substantially cylindrical inside wall surfaces 81 and 82 (barrel inner surfaces) which intersect. These cylindrical surfaces 81 and 82, as seen in cross-section in FIG. 2, appear as two intersecting circles in the form of a figure eight.
  • Each non-symmetrical modular mixing element 51, 52, 53 or 54 has an axial bore 56 for mounting on a shaft 30.
  • the transport screw elements 45, 46 and 48 have bores and keyways (not shown) similar to those shown in FIG. 2 for the modular mixing elements.
  • FIGS. 3, 3A and 3B Shown most clearly in FIGS. 3, 3A and 3B is a profile 57 of a non-symmetrical modular mixing element 51, 52, 53 or 54.
  • Each modular mixing element 51, 52, 53, or 54 is shown in FIG. 3 having two non-symmetrical wings 62, 64, 66, or 68, respectively.
  • the dimensions of various components of a mixing element may be expressed later in terms of this barrel inner diameter D so that these dimensions are set forth in universal terms relative to D for being applicable to extrusion-compounding machines of various sizes, or alternatively such dimensions may be expressed in terms of the barrel inner radius R B for similar reasons to be set forth in universal terms.
  • Each of the wings 62, 64, 66 or 68 includes a convex leading face 70 of radius R 1 which meets the surface of the wing tip 60 along a corner 71.
  • This convex leading face 70 merges at a point 72 with a straight tangent portion 73 (called a "FLAT") of the non-symmetrical profile 57.
  • this merging tangent point 72 is located above the base line X by the same distance as the coordinate distance y 1 at which the leading face center point 74 is located above this base line.
  • the pair of base half-widths X 0 lie along the base line X on opposite sides of the axis 31 or 32.
  • Each of the wings 62, 64, 66 or 68 includes a convex trailing face 76 of radius R 2 which meets the surface of wing tip 60 along a corner 77. Trailing face radius R 2 is preferred to be always larger than leading face radius R 1 for reasons explained later.
  • a center point 78 for the trailing face radius R 2 is spaced a small coordinate distance y 2 above base line X. The coordinate distance x 1 for leading face center point 74 and the coordinate distance x 2 for trailing face center point 78 are measured normal to a center-line 75 (major chord) of the two non-symmetrical wings 62, 64, 66 or 68 of each modular mixing element 51, 52, 53 or 54.
  • This center-line major chord 75 is called a "center-line” because it extends through the axis 31 or 32.
  • the coordinate x 2 is always larger than x 1
  • the coordinate y 2 is always smaller than y 1 . Since the trailing face center point 78 is spaced slightly above the base line X, it is noted that the flat 73 extends a slight distance beyond the base line X and merges at a merging tangent point 79 with the convex trailing face 76.
  • This second radius R 1 is a line segment 86 extending from the leading face center point 74 to the corner 71 where the profile 57 of the leading face 70 intersects with the surface of the wing tip 60. Since this line segment 86 extending from point 74 to corner 71 is a radius of the arcuate leading face 70, it is normal (perpendicular) at point 71 to a tangent to this convex leading face 70 at point 71.
  • a line 90 is indicated extending from the axis 31 or 32 to the corner 71, and this line 90 is shown by a dash 91 being extended out to a point 92 on the barrel inner surface 81 or 82. Since this extended line 90, 91 radiates from the axis 31 or 32 (which is the axis of the barrel inner surface and is also the axis of the screw assembly 21 or 22), this extended line 90, 91 is a radius of the barrel inner surface and hence is perpendicular at point 92 to a tangent to the barrel inner surface at point 92.
  • a dashed line 93 is drawn tangent to the leading face 70 at the corner point 71.
  • Another dashed line 94 is drawn tangent to the barrel inner surface 81 or 82 at the point 92.
  • the angle ⁇ between tangent lines 93 and 94 is called the leading face wedge angle because it provides an essentially constant and uniform wedging action commencing near the flat-to-curve merge point 72 and continuing to the wing-tip-leading-corner 71. Since they are perpendicular to the respective tangents 93 and 94, the line segment 86 and line 90 also define between themselves this same leading face wedge angle ⁇ , as shown in FIG. 3B.
  • lines 86 and 90 which are respectively perpendicular to two intersecting lines (tangents 93 and 94), define between themselves the same angle as between the intersecting lines.
  • a line segment 87 extending from trailing face center point 78 to the wing-tip-trailing-corner 77 is another radius R 2 of the arcuate trailing face 76.
  • line 87 is perpendicular to a tangent 95 (shown dashed) to trailing face curve 76 at the corner point 77.
  • a line segment 96 radiating from axis 31 or 32 to the corner point 77 is extended as shown by dash 97 to a point 98 on the barrel inner surface 81 or 82.
  • a tangent 99 (shown dashed) to the barrel inner surface 81 or 82 at point 98 is perpendicular to line 96, 97.
  • the angle ⁇ between tangents 95 and 97 is called the trailing face wedge angle and is always larger than the leading face wedge angle ⁇ .
  • Lines 87 and 96 also define between themselves the same angle ⁇ as do the tangents 95 and 99 due to the same geometric principle as noted above for the angle ⁇ .
  • the plastic material experiences a sudden release, i.e. a reduction in circumferential flow rate and in shear rate, after it has passed the trailing wing tip corner 77.
  • This sudden release of the plastic material in a trailing wedge release zone 89 following passage of the corner 77 causes in effect a detachment of the plastic from the barrel inner surface 81 or 82, almost as though the plastic material were "rebounding" away from this inner surface. Consequently, less energy is needlessly imparted in this trailing wedge angle zone 89, thereby conserving energy and keeping the plastic material at a lower temperature than occurs with symmetric kneading blocks or kneading discs.
  • the temperatures of the eight successive barrel segments 26-2 through 26-9 were measured by suitable temperature sensors, one of which is indicated by T with the sensor 100 shown inserted in barrel segment 26-6 so as to be responsive to temperature of the respective barrel segment.
  • the exit temperature and pressure are, respectively, the temperature of the extrudate 39 and the pressure at which it was being extruded through the die.
  • the head temperature is the temperature of the exit head at the downstream end of the final barrel segment 26-9.
  • the die temperature is the temperature of the die (not shown) through which the extrudate 39 was expelled.
  • each test column There are two temperatures set forth in each test column for eight Barrel segments and the Head.
  • the left temperature value in each column is the set point (or target), and the right value is the temperature actually obtained as shown by the respective measured temperatures. It is noted that relatively low and relatively uniform temperatures were achieved along the full length of the barrel in all of the seven test runs.
  • FIGS. 4A and 4B show end elevational and side elevational views of the non-symmetrical modular mixing element 51, which was described with reference to FIGS. 1 and 1A. It is shown with two wings 62 located in diametrically opposite angular positions relative to the screw axis 31 or 32. The wings 62 with their wing tips 60 are shown having an RH-twist of 90° within the axial length L of the element 51. As will be appreciated from a close look at FIG. 1A, which shows a barrel segment 26-3, the axial length L is shown as being one-half of the axial length of a barrel segment. With two opposed keyways 44 as shown and with a 90° twist, such elements 51 are enabled to be assembled in multiple sets and combinations with their wing tips 60 being in alignment for forming an uninterrupted helix at their end-to-end junctures.
  • FIGS. 5A and 5B show end elevational and side elevational views of the non-symmetrical modular mixing element 52, which was described with reference to FIGS. 1 and 1A.
  • This mixing element 52 is shown with two wings 64 located in diametrically opposite angular positions relative to the screw axis 31 or 32.
  • the wings 64 with their wing tips 60 are shown having an LH-twist of 90° within the axial length L (one-half of the axial length of a barrel segment).
  • With two opposed keyways 44 as shown and with a 90° twist such elements 52 are enabled to be assembled in multiple sets and combinations with their wing tips 60 being aligned end-to-end for forming an uninterrupted helix.
  • elements 51 and 52 can be assembled in sets 50-1 (FIGS. 1 and 1A) as described. Their wing tips are aligned at a juncture 104 (FIG. 1A), but there is an abrupt reversal in twist forming a cusp at this juncture 104.
  • FIGS. 6A and 6B show end elevational and side elevational views of the non-symmetrical modular mixing element 53 seen in FIGS. 1 and 1B.
  • Element 53 is shown with two diametrically opposite wings 66. These wings 66 with their wing tips 60 are shown having an RH-twist of 90° within an axial length of two-thirds L. Thus, the length of element 53 is shown as being one-third the length of a barrel segment.
  • two opposed keyways 44 as shown and with a 90° twist such elements 53 are enabled to be assembled in multiple sets and combinations with their wing tips being in alignment at their end-to-end junctures for forming an uninterrupted helix.
  • RH-twist mixing elements 51 and 53 are enabled to be assembled with their wing tips in alignment for providing changes in RH helical pitch at their junctures.
  • RH-twist mixing elements 51 and 53 are enabled to be assembled upstream of LH-twist mixing elements 52 with wing tips in alignment but there is an abrupt reversal in twist forming a cusp at their junctures.
  • FIGS. 7A and 7B show end elevational and side elevational views of non-symmetrical LH-twist modular mixing element 54 of 90° twist.
  • This mixing element 54 is seen also in FIGS. 1 and 1B. It has an axial length of two-thirds L and is similar to the mixing element 53, except that their helical twists are of equal pitch but opposite senses.
  • mounted end-to-end in a set of 50-2 as shown in FIG. 1B they form a cusp 106 which has a steeper V-shape than cusp 104 (FIG. 1A) since their axial lengths are shorter, thereby creating a larger helix angle (shorter lead) in their wing tips 60 than the helix angle for the wing tips 60 of the longer mixing elements 51 and 52.
  • FIG. 8 the profile 57 of a non-symmetrical modular mixing element is shown superimposed upon a twin-screw ideal self-wiping profile 107 (shown shaded).
  • a twin-screw ideal self-wiping profile is the maximum proportional area of such a self-wiping profile which can be utilized in a co-rotating, intermeshing twin-screw extruder in which the screw remains continuously in wiping contact with its co-rotating twin and also remains continuously in wiping contact with a cylindrical-shaped barrel inner wall surface 81 or 82.
  • the substantial proportional amount of the shaded area between profiles 107 and 57 shows the relatively large clearances provided around the non-symmetrical profiles 57 of these modular mixing elements.
  • the downstream flow is primarily channel flow in regions along a barrel where the transport screw elements 45, 46 or 48 are intermeshing.
  • This channel flow occurs along the helical valleys between successive screw flights 47.
  • this channel flow are the relatively large amounts of circumferential flow produced in regions along a barrel where sets of non-symmetrical modular mixing elements 51, 52, 53 or 54 are mounted. By their dynamic wedging action and their relatively large shear clearances they produce relatively large proportional amounts of circumferential flow as is shown by arrows 88 in FIG. 3B.
  • tip clearance aspect ratio a about 1 to about 8
  • wing aspect ratio b about 0.5 to about 0.8
  • leading face wedge angle ⁇ about 5° to about 25°
  • trailing face wedge angle ⁇ about 10° to about 90°
  • ⁇ is at least about 1° larger than ⁇ .
  • ⁇ /R B about 0.02 to about 0.12
  • ⁇ about 10° to about 20°
  • ⁇ about 20° to about 30°
  • ⁇ is at least about 5° larger than ⁇ .
  • ⁇ is at least about 7° larger than ⁇ .
  • the helix angles for the wing tips 60 of modular mixing elements are preferred to be in the range of about 20° to about 60°.
  • the lead of the helical wing tips is preferred to be in the range of about 2D to about 8D.
  • twist of 90° shown for the modular mixing elements 51, 52, 53 and 54 is related to their two-keyway configuration. With a three-keyway configuration, twist angles of 60° are usable for providing alignment of wing tips 60 at end-to-end junctions. With a four-keyway configuration twist angles of either 90° or 45° may be used for providing such alignment of wing tips at junctures, and so forth.

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  • Engineering & Computer Science (AREA)
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  • Physics & Mathematics (AREA)
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  • General Physics & Mathematics (AREA)
  • Mathematical Analysis (AREA)
  • Mathematical Optimization (AREA)
  • Mathematical Physics (AREA)
  • Pure & Applied Mathematics (AREA)
  • Extrusion Moulding Of Plastics Or The Like (AREA)
  • Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)
US08/253,397 1994-06-03 1994-06-03 Multi-screw, extrusion-compounding machine with modular mixing elements Expired - Lifetime US5487602A (en)

Priority Applications (17)

Application Number Priority Date Filing Date Title
US08/253,397 US5487602A (en) 1994-06-03 1994-06-03 Multi-screw, extrusion-compounding machine with modular mixing elements
TW084104470A TW261569B (en) 1994-06-03 1995-05-04 Multi-screw, extrusion-compounding machine with modular mixing elements
BR9508698A BR9508698A (pt) 1994-06-03 1995-06-01 Máquina extrusora-compositora de roscas múltiplas e elemento modular de mistura não-simétrico
AT95921588T ATE197569T1 (de) 1994-06-03 1995-06-01 Mehrschneckenextruder mit modularen mischelementen
RU97100147A RU2145281C1 (ru) 1994-06-03 1995-06-01 Многошнековые экструдеры-смесители с модульными смесительными элементами
CA002191860A CA2191860C (en) 1994-06-03 1995-06-01 Multi-screw, extrusion-compounding machine with modular mixing elements
KR1019960706886A KR100204118B1 (ko) 1994-06-03 1995-06-01 모듈믹싱장치들을 갖춘 멀티스크류의 압출-혼합기계
JP8501230A JP2912021B2 (ja) 1994-06-03 1995-06-01 モジュール混合要素を有する多軸スクリュー押出配合機
PCT/US1995/007025 WO1995033608A1 (en) 1994-06-03 1995-06-01 Multi-screw, extrusion-compounding machine with modular mixing elements
CN95193412A CN1051494C (zh) 1994-06-03 1995-06-01 带有模式混料件的多螺杆配混挤塑机
EP95921588A EP0764074B1 (en) 1994-06-03 1995-06-01 Multi-screw, extrusion-compounding machine with modular mixing elements
AU26616/95A AU680372B2 (en) 1994-06-03 1995-06-01 Multi-screw, extrusion-compounding machine with modular mixing elements
DK95921588T DK0764074T3 (da) 1994-06-03 1995-06-01 Flersnekkeekstruder med modulære blandingselementer
MXPA/A/1996/006025A MXPA96006025A (en) 1994-06-03 1995-06-01 Machine to form compounds by extrusion multiple detachments with elements of mixcladomodula
PL95317539A PL177289B1 (pl) 1994-06-03 1995-06-01 Urządzenie do mieszania i wytłaczania materiałów, zwłaszcza plastycznych
DE69519431T DE69519431T2 (de) 1994-06-03 1995-06-01 Mehrschneckenextruder mit modularen mischelementen
ES95921588T ES2152403T3 (es) 1994-06-03 1995-06-01 Maquina de combinar y extruir de multiples husillos con elementos de mezclar modulares.

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EP (1) EP0764074B1 (ja)
JP (1) JP2912021B2 (ja)
KR (1) KR100204118B1 (ja)
CN (1) CN1051494C (ja)
AT (1) ATE197569T1 (ja)
AU (1) AU680372B2 (ja)
BR (1) BR9508698A (ja)
CA (1) CA2191860C (ja)
DE (1) DE69519431T2 (ja)
DK (1) DK0764074T3 (ja)
ES (1) ES2152403T3 (ja)
PL (1) PL177289B1 (ja)
RU (1) RU2145281C1 (ja)
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US6116771A (en) * 1999-02-05 2000-09-12 Krupp Werner & Pfleiderer Corporation Multi-shaft extruder screw bushing and extruder
US6116770A (en) * 1998-10-02 2000-09-12 Krupp Werner & Pfleiderer Corporation Mixing element for screw extruder
US6179460B1 (en) * 1998-12-24 2001-01-30 Krupp Werner & Pfleiderer, Gmbh Twin screw extruder with single-flight kneading disks
US6258302B1 (en) 1999-02-10 2001-07-10 Spalding Sports Worldwide, Inc. Process for producing polybutadiene golf ball cores
US6284814B1 (en) 1998-08-31 2001-09-04 Chakra V. Gupta Method of making masterbatches of liquid additives and, in particular, antimicrobial masterbatches
US20020123556A1 (en) * 2000-11-03 2002-09-05 Giammattei Mark Howard Extruder transition section
US20030185090A1 (en) * 2000-10-17 2003-10-02 Toshiyuki Otsuka Closed kneader
US20050024986A1 (en) * 2003-07-30 2005-02-03 Mattingly Joseph E. Kneading element and related articles
US20050127559A1 (en) * 2002-03-13 2005-06-16 Eggen Svein S. Homogenizing multimodal polymer
EP1757420A1 (en) * 2004-06-03 2007-02-28 Mitsubishi Heavy Industries, Ltd. Continuous kneading device and kneading system using the same
US20070211560A1 (en) * 2006-03-10 2007-09-13 The Japan Steel Works, Ltd. Kneading extruder
US7350960B2 (en) * 2004-07-07 2008-04-01 Tech. Process & Engineering, Inc. Dual flight rotors for continuous mixer assembly
US20090213681A1 (en) * 2005-07-12 2009-08-27 Carl-Gustaf Ek Counter-rotating twin screw extruder
WO2009152948A1 (de) * 2008-06-20 2009-12-23 Bayer Materialscience Ag Verfahren zur extrusion plastischer massen
WO2009152973A1 (de) * 2008-06-20 2009-12-23 Bayer Technology Services Gmbh Scheckenelemente mit reduziertem kammwinkel
US20110112255A1 (en) * 2008-06-20 2011-05-12 Bayer Technology Services Gmbh Single-Flighted Screw Elements With a Reduced Tip Angle
US20110184089A1 (en) * 2008-06-20 2011-07-28 Bayer Materialscience Ag Method for the extrusion of plastic materials
EP2374600A1 (en) 2010-04-12 2011-10-12 Borealis AG Kneading disk with tapered crest surface
WO2012007501A1 (de) * 2010-07-14 2012-01-19 Bayer Materialscience Ag Vorrichtung und verfahren zur herstellung von produkten aus pigmenthaltigen polymermischungen
US20120320702A9 (en) * 2009-09-29 2012-12-20 Ulrich Burkhardt Treatment element for treating material in a multi-shaft worm machine and multi-shaft worm machine
CN103038034A (zh) * 2010-08-05 2013-04-10 株式会社神户制钢所 连续捏合机和捏合方法
WO2013045623A3 (de) * 2011-09-28 2013-06-13 Lanxess Deutschland Gmbh Verfahren zum entgasen, entgasungsvorrichtung und verwendung von schneckenelementen
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JP2016522108A (ja) * 2013-06-24 2016-07-28 コベストロ、ドイチュラント、アクチエンゲゼルシャフトＣｏｖｅｓｔｒｏ Ｄｅｕｔｓｃｈｌａｎｄ Ａｇ 多軸スクリュー式機械用のスクリューエレメント
TWI560041B (ja) * 2009-08-26 2016-12-01 Polyplastics Co
CN112643996A (zh) * 2020-12-03 2021-04-13 欧宝聚合物江苏有限公司 一种单螺杆混合挤出机

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EP0850738A3 (en) * 1996-12-24 1998-09-09 KABUSHIKI KAISHA KOBE SEIKO SHO also known as Kobe Steel Ltd. Twin-screw kneading apparatus
US5947593A (en) * 1996-12-24 1999-09-07 Kabushiki Kaisha Kobe Seiko Sho Twin-screw kneading apparatus
EP0850738A2 (en) * 1996-12-24 1998-07-01 KABUSHIKI KAISHA KOBE SEIKO SHO also known as Kobe Steel Ltd. Twin-screw kneading apparatus
WO1999025537A1 (en) * 1997-11-19 1999-05-27 The Dow Chemical Company High efficiency extruder
US6284814B1 (en) 1998-08-31 2001-09-04 Chakra V. Gupta Method of making masterbatches of liquid additives and, in particular, antimicrobial masterbatches
US6116770A (en) * 1998-10-02 2000-09-12 Krupp Werner & Pfleiderer Corporation Mixing element for screw extruder
US6179460B1 (en) * 1998-12-24 2001-01-30 Krupp Werner & Pfleiderer, Gmbh Twin screw extruder with single-flight kneading disks
US6116771A (en) * 1999-02-05 2000-09-12 Krupp Werner & Pfleiderer Corporation Multi-shaft extruder screw bushing and extruder
US6258302B1 (en) 1999-02-10 2001-07-10 Spalding Sports Worldwide, Inc. Process for producing polybutadiene golf ball cores
US20010026027A1 (en) * 1999-02-10 2001-10-04 Spalding Sports Worldwide, Inc. Process for producing polybutadiene golf ball cores
US6881049B2 (en) 1999-02-10 2005-04-19 Callaway Golf Company Process for producing polybutadiene golf ball cores
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EP1757420A4 (en) * 2004-06-03 2012-12-19 Mitsubishi Heavy Ind Ltd CONTINUOUS FILLING DEVICE AND FILLING SYSTEM USING THE SAME
US7350960B2 (en) * 2004-07-07 2008-04-01 Tech. Process & Engineering, Inc. Dual flight rotors for continuous mixer assembly
US20110170369A1 (en) * 2005-07-12 2011-07-14 Carl-Gustaf Ek Counter-rotating twin screw extruder
US20090213681A1 (en) * 2005-07-12 2009-08-27 Carl-Gustaf Ek Counter-rotating twin screw extruder
US8079747B2 (en) * 2005-07-12 2011-12-20 Borealis Technology Oy Counter-rotating twin screw extruder
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US20190061200A1 (en) * 2008-06-20 2019-02-28 Covestro Deutschland Ag Process for extruding plastic compositions
US20110184089A1 (en) * 2008-06-20 2011-07-28 Bayer Materialscience Ag Method for the extrusion of plastic materials
CN102066066A (zh) * 2008-06-20 2011-05-18 拜尔技术服务有限责任公司 具有减小的顶锥角的螺杆元件
US9944008B2 (en) 2008-06-20 2018-04-17 Covestro Deutschland Ag Method for extruding plastic materials
US10836076B2 (en) * 2008-06-20 2020-11-17 Covestro Deutschland Ag Process for extruding plastic compositions
WO2009152973A1 (de) * 2008-06-20 2009-12-23 Bayer Technology Services Gmbh Scheckenelemente mit reduziertem kammwinkel
WO2009152948A1 (de) * 2008-06-20 2009-12-23 Bayer Materialscience Ag Verfahren zur extrusion plastischer massen
RU2522624C9 (ru) * 2008-06-20 2015-02-20 Байер Интеллектуэль Проперти Гмбх Шнековые элементы с уменьшенным наклоном гребня
RU2531279C2 (ru) * 2008-06-20 2014-10-20 Байер Интеллектуэль Проперти Гмбх Одноходовые шнековые элементы с уменьшенным наклоном линии гребня
US20110112255A1 (en) * 2008-06-20 2011-05-12 Bayer Technology Services Gmbh Single-Flighted Screw Elements With a Reduced Tip Angle
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EP0764074A1 (en) 1997-03-26
AU2661695A (en) 1996-01-04
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JPH09506568A (ja) 1997-06-30
WO1995033608A1 (en) 1995-12-14
EP0764074B1 (en) 2000-11-15
BR9508698A (pt) 1997-08-12
PL177289B1 (pl) 1999-10-29
CA2191860C (en) 2001-01-30
EP0764074A4 (en) 1997-10-15
DE69519431T2 (de) 2001-05-10
KR970703230A (ko) 1997-07-03
DK0764074T3 (da) 2001-02-05
PL317539A1 (en) 1997-04-14
JP2912021B2 (ja) 1999-06-28
CN1149852A (zh) 1997-05-14
AU680372B2 (en) 1997-07-24
TW261569B (en) 1995-11-01
KR100204118B1 (ko) 1999-06-15
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CA2191860A1 (en) 1995-12-14
CN1051494C (zh) 2000-04-19

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