US49009A - Improved crucible for metallic baths - Google Patents

Improved crucible for metallic baths Download PDF

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US49009A
US49009A US49009DA US49009A US 49009 A US49009 A US 49009A US 49009D A US49009D A US 49009DA US 49009 A US49009 A US 49009A
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crucible
sand
baths
metallic
lead
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    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/24Vacuum evaporation
    • C23C14/243Crucibles for source material
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/009After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated

Description

s. sToKEs.v CruCibIe for Metallic Baths. No. 49,009. Patent-ed July 25, 1865.
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.f'brzlzon fa I Svcb'an an fle Zine- JLB new and Improved Mode of Oonstructin g Gruci- UNITED STATES VPATENT GEEICE.
IMPROVED CRUCIBLE FOR METALLIC BATHS.
Specification forming part of Letters Patent No. "l 9,009, dated July 25, 1865.
To all whom fit may concern s Be it known that I, BENJAMIN S. SToKEs, of Manchester, in the county of Hillsborough and State of New Hampshire, have invented a bles forMetallic Baths; and I do hereby declare that the following is a full and exact description thereof, reference being had to the accompanying drawings, and to the letters ot' reference marked thereon, where similar parts are represented by like letters.
Figure l is a plan or horizontal view of top 5 Fig. 2, an elevation 5 Fig. 3, a horizontal section on the line A B of Figs. 2 and 4; Fig. 4, a vertical section on the line C D of Figs. l and 3.
al a represent the outer crucible or cylinder 5 b b, the inner crucible or cylinder 5 cc, the space between a and b.
The nature of my invention consists in constructing a crucible of two parts, so as to pre vent the wasting of the metal used in the same, and to render it durable and economical.
Single cast-iron crucibles lled with lead, for the purpose of heating les or other pieces of steel uniformly and evenly, have been long used, but experience shows thatsuch crucibles, afterafew weeks,so1netimesafewdays,use,be come so porous and spon gy by the action ofthe heat and air upon their outer surfaces that the lead lters through them and renders them worthless, although the crucible is not sensibly diminished in size or injured iu any other respect than in its capacity to retain the lead. A cast-iron crucible, one and a quarter inch thick, capable of holding two hundred pounds of lead, will leak and waste from six to twelve pounds of lead per day after being used about ten days.
To construct a crucible that will prevent this waste of its metallic bath by preserving the original structure of the lining or inner crucible in shielding it from atmospheric air is the object of my invention, which I will describe, to enable others skilled in the art to make and use the same.
In the rst place I cast of iron a crucible. (Represented by a a, Figs. 1,2, 3, 4.) I then make of best wrought-iron a crucible, b I), Figs. l, 3, 4, smaller in diameter than the inside of a a, and of less depth than inside of a, a section ot' which is shown in Fig. 4 byb b, this inner cruci ble being thinnerthan the outer one, but of sufticient thickness and strength for the purposes required of it. Next I take common tine sand, sift out the smaller particles, wash the sand and dry it, then sprinkle this on the bottom ot' inside of ai, Fig. 4, as indicated by the yellow color in space c, betweenthe bottoms of a and b. I then introduce b into a, resting b on the sand on the bottom of a until the entire space between a and b is filled with this sand, which is tamped down as it is filled in, and the sand forms, as it were, a third or middle crucible between a and b, as shown by c in the drawings. b is then filled with lead, and the two crucibles thus prepared are heated in the usual mode.
I use this crucible in the manufacture of files, which are placed in the lead bath after it is heated to the desired temperature; but all kinds of cutlery and other steel instruments are tempered by heating in lead baths, and my invention applies to all lead or other metal baths, and to all other kinds ot' crucibles, for whatever purposes they may be used.
I make b ot' wrought-iron on account of its structure and compactness, and its tendency to resist leakage from expansion by heat when it is protected from the air.
To protect b from atmospheric air on its outer surface I introduce the sand, as described, which experience shows entirely prevents the outer surface of b from oxidation or scaling and wearing away, and thus preservesto bits original size, structure, and compactness,and while so preserved bs power to retain its metallic bath is not diminished by heat, as several months use of such a crucible shows no sensible loss of the metal constituting its bath.
There is no reason why b will not last as long as a is thick enough to hold the sand around its outer surface; and when a shall have been burned so thin as to allow the escape ofthe sand, which could not be in many months, then a new cast-iron crucible can be substituted for a and b be re-inserted and packed therein, as before described, b meanwhile retaining its integrity. Another advan .tage ofthe sand is that when crucibles a and b are made of cast and wrought iron the sand will adapt itself to the different degrees of expansion such irons are subject to, and thus relieve any strain that would otherwise result to either a or b.
I do not wish to confine myself to making a of cast-iron, nor to filling the space between a and b with sand, for I contemplate that other materials may be used in their stead to prevent the. oxidation und wearingoft' of the outer surface ot' the inner Crucible, substantially as described, and that such are included in my invention. The inside surface of bis always protected from the air by its metallic bath-:t fact common to all crucbles.
What I claim, and desire to secure by Letters Patent, is
The construction, substantially as herein described, ot' a crucble of two parts, a and b, with space c between a and b filled with sand or its equivalent7 for the uses and purposes herein set forth.
BENJAMIN S. STOKES.
Witnesses:
JOHN B. MOCRILLIS, B. P. OILLEY.
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