US4347672A - Inflow bottom for a fluidized bed reactor - Google Patents
Inflow bottom for a fluidized bed reactor Download PDFInfo
- Publication number
- US4347672A US4347672A US06/226,703 US22670381A US4347672A US 4347672 A US4347672 A US 4347672A US 22670381 A US22670381 A US 22670381A US 4347672 A US4347672 A US 4347672A
- Authority
- US
- United States
- Prior art keywords
- flow
- floor
- approach
- approach flow
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000013459 approach Methods 0.000 claims abstract description 63
- 238000009826 distribution Methods 0.000 claims abstract description 7
- 238000012856 packing Methods 0.000 claims description 7
- 239000000463 material Substances 0.000 claims description 6
- 239000011810 insulating material Substances 0.000 claims description 4
- 239000011148 porous material Substances 0.000 claims description 3
- 239000012535 impurity Substances 0.000 claims description 2
- 125000006850 spacer group Chemical group 0.000 claims description 2
- 230000002093 peripheral effect Effects 0.000 claims 1
- 239000000725 suspension Substances 0.000 abstract description 5
- 239000007789 gas Substances 0.000 description 23
- 239000002245 particle Substances 0.000 description 10
- 239000007787 solid Substances 0.000 description 10
- 238000006243 chemical reaction Methods 0.000 description 8
- 238000010944 pre-mature reactiony Methods 0.000 description 4
- 230000000254 damaging effect Effects 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 230000005526 G1 to G0 transition Effects 0.000 description 2
- 238000005299 abrasion Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000002309 gasification Methods 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 238000013021 overheating Methods 0.000 description 2
- 239000011343 solid material Substances 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical class [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 229910002090 carbon oxide Inorganic materials 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 238000001311 chemical methods and process Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000005243 fluidization Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 230000002028 premature Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000010349 pulsation Effects 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000036632 reaction speed Effects 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- 238000009827 uniform distribution Methods 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
- B01J8/1818—Feeding of the fluidising gas
Definitions
- the invention concerns an approach flow floor for a fluidized bed reactor with approach flow nozzles in floor openings for feeding a charging gas into a fluidized bed above the approach flow floor.
- a fluidized bed is usually produced by causing a carrier medium to undergo a pressure loss due to the flow resistance as it passes through fine-grained loose material, thereby exerting a force on the ballast.
- Fluidized beds are used in various chemical processes. Fluidized beds are particularly suitable for certain processes as they make possible good temperature control and continuous operation, are distinguished by good heat transfer and high reaction speed and guarantee steadily uniform contact activity in catalytic processes. However it has been found that the introduction of materials, in particular charging gases, into the fluidized bed, causes difficulties.
- sieve floors are known in conjunction with which the charging gas is blown in from below through the sieve openings at a certain speed.
- a flow-back of solid particles takes place, already after a brief period of operation, from the fluidized bed through the openings in the sieve floor. This causes a narrowing and blocking of the sieve openings and also unwanted and, consequently, intolerable premature catalytic reactions which finally necessitate taking the fluidized bed out of service.
- the invention is based on the problem of providing an approach flow floor with which blockages are reliably excluded and consequently unwanted premature reactions do not occur.
- approach flow bodies each with a central approach flow hole, are disposed in the floor openings and a gas-permeable distributor plate is disposed on the approach flow body at a short distance above the discharge opening of the approach flow hole.
- the relatively large-surfaced outflow of the charging gas results in a laminar flow of the gas flowing through the distributor plate and a largely homogeneous fluidized bed, whereby high relative speeds on the, for the most part, catalytically active solid particles are avoided. This causes a relatively slight abrasion of solid material.
- the charging gas forms a uniform suspension phase with the fluidized bed, so that damaging local overheating in markedly exothermal reactions is avoided.
- the distribution plate consists preferably of porous material. It is also advisable to use distributor plates made of thermally insulating material. This prevents a transition of heat from the fluidized bed compartment into the approach flow bodies and eliminates damaging premature reactions, particularly as the charging gas flowing into the approach flow bodies has a cooling effect. It is also advantageous for the distributor plates to consist of catalytically inert material, in order to prevent unwanted premature reactions.
- the distributor plates should have discharge openings 10 to 200 times the size of any possible impurities. This ensures that, even when the charging gas is polluted, no blockages occur on the correspondingly large-pore plate distributors and uniform reliability of operation is guaranteed. As pulsation surges can be prevented, inter alia, it is ensured that no solid particles will get into the approach flow holes of the approach flow bodies from the fluidized bed in any operational or stationary phase, thus excluding all danger of blockage.
- a pick-up pocket for the distributor plate may be located in the upper part of the approach flow body.
- the approach flow hole can also open into the pick-up pocket via a conical widening.
- the latter can be elastically mounted on spaces disposed in the pick-up pocket.
- This packing consists preferably of themally insulating material which should also be catalytically inert.
- a baffle plate can be disposed on the distributor plate above the conical widening. The approaching gas is hereby deflected out of the median region of the distributor plate.
- FIG. 1 shows a cross-section through an approach flow floor
- FIG. 2 shows an enlarged representation of a portion of FIG. 1.
- An approach flow floor 2 with floor opening 3 is disposed in a fluidized bed reactor in which gas distributors 4 are located.
- the gas distributors 4 consist of an approach flow body 5 and a distributor plate 6.
- heat exchangers 7 are disposed for taking away the reaction heat generated by exothermal reactions.
- the surfaces 9 of the approach flow floor 2 display an upward incline towards the reactor wall 1 between the distributor plates 6 and the reactor wall 1.
- a pick-up pocket 12 is worked into the upper region of the approach flow body 5 in which the distributor plate 6 is mounted on elastic spacers 13.
- a packing 15 of thermally insulating and catalytically inert material is disposed between the distributor plate 6 and the wall 14 of the approach flow body 5.
- a mounting support 16 which projects into the pick-up pocket 12 so far that the distributor plate 6 cannot involuntarily lift out of its position is located some distance above the packing 15.
- baffle plate 17 which is located at right angles above a conical widening 18 of an approach flow hole 19.
- One basic body 5 is secured from beneath to the approach flow floor 2 by means of screws in holes 20, not shown.
- the gasification gas passes out of the gas chamber 11 through the approach flow holes 19 of the gas distributors 4 into the conical widening 18 and from here, after deflection from the baffle boards 17 through the distributor plates 6 into the reaction chamber 10 above the approach flow floor 2 in which the fluidized bed is located.
- the wedge-shaped elevations 8 and the sloping surfaces 9 of the approach flow floor 2 ensure that solid particles dropping out of the fluidized bed slide down to the distributor plates 6 and are carried back from here into the suspension phase 10 again.
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
- Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)
- Industrial Gases (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE3001961A DE3001961C2 (de) | 1980-01-21 | 1980-01-21 | Anströmboden für einen Wirbelschichtreaktor |
DE3001961 | 1980-01-21 |
Publications (1)
Publication Number | Publication Date |
---|---|
US4347672A true US4347672A (en) | 1982-09-07 |
Family
ID=6092525
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US06/226,703 Expired - Lifetime US4347672A (en) | 1980-01-21 | 1981-01-21 | Inflow bottom for a fluidized bed reactor |
Country Status (4)
Country | Link |
---|---|
US (1) | US4347672A (enrdf_load_stackoverflow) |
JP (1) | JPS56115633A (enrdf_load_stackoverflow) |
AU (1) | AU542228B2 (enrdf_load_stackoverflow) |
DE (1) | DE3001961C2 (enrdf_load_stackoverflow) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4968492A (en) * | 1988-08-19 | 1990-11-06 | Charbonages De France | Device for feeding fluidizing gas to the openings in a grid for supporting a bed of particles to be fluidized |
US20100255099A1 (en) * | 2007-10-26 | 2010-10-07 | Rexahn Pharmaceuticals, Inc. | Clavulanate formulation for neuroprotection and treatment of neurodegenerative disorders |
US20110083593A1 (en) * | 2009-10-12 | 2011-04-14 | AirClean Technologies, Inc. | Fluidized combustor |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4841884A (en) * | 1988-05-26 | 1989-06-27 | A. Ahlstrom Corporation | Distributor plate for fluidized bed reactor |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3746516A (en) * | 1970-03-10 | 1973-07-17 | Thann Fab Prod Chem | Sole plate for fluidized bed reactor |
US3896560A (en) * | 1973-06-18 | 1975-07-29 | United States Steel Corp | Two-stage fluidized bed reactor with nozzle tuyeres |
US3995771A (en) * | 1975-05-19 | 1976-12-07 | Kaiser Aluminum & Chemical Corporation | Feeding device for particulate matter |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5847216B2 (ja) * | 1975-07-23 | 1983-10-21 | バブコツク日立株式会社 | チヨクレツタダンリユウドウソウガスブンサンソウチツキハンノウロ |
JPS5743697Y2 (enrdf_load_stackoverflow) * | 1979-03-30 | 1982-09-27 |
-
1980
- 1980-01-21 DE DE3001961A patent/DE3001961C2/de not_active Expired
-
1981
- 1981-01-21 US US06/226,703 patent/US4347672A/en not_active Expired - Lifetime
- 1981-01-21 JP JP776681A patent/JPS56115633A/ja active Granted
- 1981-01-21 AU AU66516/81A patent/AU542228B2/en not_active Ceased
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3746516A (en) * | 1970-03-10 | 1973-07-17 | Thann Fab Prod Chem | Sole plate for fluidized bed reactor |
US3896560A (en) * | 1973-06-18 | 1975-07-29 | United States Steel Corp | Two-stage fluidized bed reactor with nozzle tuyeres |
US3995771A (en) * | 1975-05-19 | 1976-12-07 | Kaiser Aluminum & Chemical Corporation | Feeding device for particulate matter |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4968492A (en) * | 1988-08-19 | 1990-11-06 | Charbonages De France | Device for feeding fluidizing gas to the openings in a grid for supporting a bed of particles to be fluidized |
US20100255099A1 (en) * | 2007-10-26 | 2010-10-07 | Rexahn Pharmaceuticals, Inc. | Clavulanate formulation for neuroprotection and treatment of neurodegenerative disorders |
US20110083593A1 (en) * | 2009-10-12 | 2011-04-14 | AirClean Technologies, Inc. | Fluidized combustor |
Also Published As
Publication number | Publication date |
---|---|
AU6651681A (en) | 1981-07-30 |
JPS6312652B2 (enrdf_load_stackoverflow) | 1988-03-22 |
DE3001961A1 (de) | 1981-08-13 |
AU542228B2 (en) | 1985-02-14 |
JPS56115633A (en) | 1981-09-10 |
DE3001961C2 (de) | 1984-08-16 |
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Legal Events
Date | Code | Title | Description |
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AS | Assignment |
Owner name: THYSSENGAS GMBH, DUISBURGER STRASSE 161 4100 DUISB Free format text: ASSIGNMENT OF ASSIGNORS INTEREST.;ASSIGNOR:FRIEDRICHS, GREGOR;REEL/FRAME:003966/0997 Effective date: 19810119 Owner name: DIDIER ENGINEERING GMBH, ALFREDSTRASSE 28, 4300 ES Free format text: ASSIGNMENT OF ASSIGNORS INTEREST.;ASSIGNOR:FRIEDRICHS, GREGOR;REEL/FRAME:003966/0997 Effective date: 19810119 Owner name: THYSSENGAS GMBH Free format text: ASSIGNMENT OF ASSIGNORS INTEREST;ASSIGNOR:FRIEDRICHS, GREGOR;REEL/FRAME:003966/0997 Effective date: 19810119 Owner name: DIDIER ENGINEERING GMBH Free format text: ASSIGNMENT OF ASSIGNORS INTEREST;ASSIGNOR:FRIEDRICHS, GREGOR;REEL/FRAME:003966/0997 Effective date: 19810119 |
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