US3689799A - Method of dosing lamps - Google Patents

Method of dosing lamps Download PDF

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Publication number
US3689799A
US3689799A US72051A US3689799DA US3689799A US 3689799 A US3689799 A US 3689799A US 72051 A US72051 A US 72051A US 3689799D A US3689799D A US 3689799DA US 3689799 A US3689799 A US 3689799A
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tubing
lamp
dosage material
sliced
dosage
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US72051A
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Stephen P Senft
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General Electric Co
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General Electric Co
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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J9/00Apparatus or processes specially adapted for the manufacture, installation, removal, maintenance of electric discharge tubes, discharge lamps, or parts thereof; Recovery of material from discharge tubes or lamps
    • H01J9/38Exhausting, degassing, filling, or cleaning vessels
    • H01J9/395Filling vessels

Definitions

  • the invention is in the field of gas-filled lamp manufacture, and is particularly applicable to the manufacture of compact lamps which operate at high temperature and which contain a gas filling of a halogen or halogen salt such as iodine or iodide.
  • the invention is directed to a method of dosing such lamps to provide the gas fill.
  • Such a gas fill causes a regenerative cycling action which prevents evaporated electrode material (in an arc lamp) of filament material (in a filament lamp) from depositing on the 'bulb and causing blackening.
  • A- particularly desirable gas fill consists of indium triiodide.
  • a dosing technique for such a fill has consisted of placing a small sphere of indium into the lamp bulb, and introducing iodine by passing argon gas over a heated reservoir of iodine crystals and hence into the lamp bulb.
  • the indium vaporizes and mixes with the iodine gas.
  • the fill gas partially condenses on the inside of the bulb.
  • the ratio of indium to iodine must be carefully controlled.
  • Such control is difficult due to the many variable parameters such the size of the indium sphere, and the temperature, rate of flow, and time period of introducing the iodine. If there is an excess of iodine in the lamp fill, the lamp is difficult to start (if an arc lamp) and the useful life of its seals is shortened. lfthere is an excess of indium, the operating voltage may be too low (if an arc lamp) and the inner wall of the lamp is likely to darken from evaporated filament or electrode material.
  • Objects of the invention are to provide an improved method of manufacturing gas-filled lamps, and to provide an improved method of dosing lamps with a gas fill.
  • the method of the invention comprises, briefly and in a preferred embodiment, the steps of placing lampdosage material in tubing of plastic material, slicing the tubing and its contents at intervals for providing desired quantities of dosage material, and removing the dosage material segments from the sliced tubing segments and placing them into respective lamp bulbs.
  • a preferred dosage material is indium triiodide, and a preferred plastic tubing material is Teflon.
  • FIG. 3 is a cross-sectional view of the tubing and its contents taken on the line 3--3 of FIG. 2;
  • FIG. 4 is a side view of a lamp bulb and a section of the slicedplastic tubing, showing the dosage material being ejected from the tubing segment and into the lamp bulb.
  • a length of tubing 11 of plastic material having a slippery surface is shown in FIG. 1, a length of tubing 11 of plastic material having a slippery surface, such as Teflon, is
  • lamp-dosage material 12 This may be accomplished by placing an end of the plastic tubing 11 into molten dosage material, such as indium triiodide, and applying sufficient vacuum at the other end of the plastic tubing 11 to drawindium triiodide into the tubing whereupon it cools and solidifies. If storage is desired, it should be sealed in dried-out glass tubing.
  • the tubing 11 and its contents are sliced, as shown in FIG. 2, by means'of a sharp thin knife or razor blade 13, to provide a plurality of segments '14 of sliced tubing each containing the proper amount of dosage material for a lamp.
  • the sliced segment or pellet 16 of indium triiodide is ejected from the sliced segment of tubing 14, by means of a plunger 17 inserted into the tubing segment 14, whereupon the pellet 16 drops into a lamp bulb 18.
  • the pellet 16 may be temporarily stored in a dispenser means from which it is placed into the bulb 18.
  • the bulb 18 is shown, by way of example, as being a partly assembled lamp of the type shown and described in the aforesaid US. Pat. No. 3,305,289, the bulb being made of quartz an containing a bulbous arc chamber region 19.
  • An electrode assembly consisting of an electrode 21, connection lead 22, and interconnecting metal foil 23, has been pinch-sealed at 26 in one stem of the bulb 18. After the lamp has been dosed with the pellet 16, it is evacuated and filled with argon at suitable pressure, and another electrode is sealed at the remaining stem of the bulb l8.
  • the lamp While making the aforesaid final electrode seal, or upon initial test operation of the lamp, the lamp becomes sufficiently hot so that the pellet 16 contained therein vaporizes, thus providing the desired final gas fill.
  • the invention achieves accurate dosing of a lamp in a low cost manner, as it is much quicker and more economical to dispense the pellet 16 into bulb 18, rather than to flow a gaseous vapor therethrough for a period of several seconds or minutes.
  • a solid compound such as indium triiodide can be utilized for generating the gas fill, in accordance with the method of the invention, to provide a gas fill of true stoichiometric characteristics, thereby insuring proper operation of the lamp.
  • the aforesaid desirable characteristics of the plastic tubing for the purposes of the invention are extremely important, due to the small size of the pellet 16, which, for use in a typical 300-watt arc discharge lamp having an arc chamber of approximately one cubic centimeter or v less, is only 0.020 inches diameter and approximately 0.050 inches long.
  • Teflon and similar plastic materials have a melting point of 300C or higher, whereas the dosage material indium triiodide has a melting point of 210C, so that there is no problem in the initial step of drawing molten indium triiodide into the plastic tubing.
  • a method of providing pellets of dosage material in lamp bulbs in the manufacture of gas-filled lamps comprising the steps of placing an end of a length of plastic tubing into molten dosage material, applying vacuum at the other end of said tubing to draw molten dosage material into the tubing, allowing said dosage material to cool and solidify in the tubing, slicing the tubing and its contents into segments each containing the desired amount of dosage material for a lamp, and ejecting the solid dosage material segments from the tubing segments by means of a plunger and placing them in respective lamp bulbs.

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  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Manufacture Of Electron Tubes, Discharge Lamp Vessels, Lead-In Wires, And The Like (AREA)

Abstract

Molten lamp-dosage material such as indium triiodide is drawn into tubing of slippery plastic material such as Teflon and allowed to solidify. The tubing and its contents are sliced at suitable intervals for providing desired quantities of dosage material per lamp, and the pellets of dosage material are forced out of the sliced tubing sections and into the lamp bulbs.

Description

United States Patent Senft [151 3,689,799 51 Sept. 5, 1972 [54] METHOD OF DOSING LAMPS [72] Inventor: Stephen P. Senft, Cleveland Heights,
Ohio
[73] Assignee: General Electric Company [22] Filed: Sept. 14, 1970 [2]] Appl. No.: 72,051
1,877,718 9/1932 Noble ..316/3 X 5/1970 Larson et a1 ..316/3 Primary Examiner-John F. Campbell Assistant Examiner-Richard Bernard Lazarus Attorney-Norman C. Fulmer, Henry P. Truesdell, Frank L. Neuhauser, Oscar B. Waddell and Joseph B. Forman ABSTRACT Molten lamp-dosage material such as indium triiodide is drawn into tubing of slippery plastic material such as Teflon and allowed to solidify. The tubing and its contents are sliced at suitable intervals for providing desired quantities of dosage material per lamp, and the pellets of dosage material are forced out of the sliced tubing sections and into the lamp bulbs.
5 Claims, 4 Drawing Figures BACKGROUND OF THE INVENTION The invention is in the field of gas-filled lamp manufacture, and is particularly applicable to the manufacture of compact lamps which operate at high temperature and which contain a gas filling of a halogen or halogen salt such as iodine or iodide. The invention is directed to a method of dosing such lamps to provide the gas fill. Such a gas fill causes a regenerative cycling action which prevents evaporated electrode material (in an arc lamp) of filament material (in a filament lamp) from depositing on the 'bulb and causing blackening.
. US. Pat. No. 3,305,289 to Elmer Fridrich, assigned to the same assignee as the present invention, describes a method which has been used for providing a gas fill in lamps, in which an inert gas is fed over heated iodine crystals so as to pick up iodine vapor. The vapor-carrying inert gas is then fed into the lamp bulb which is chilled to cause condensation of the iodine vapor.
A- particularly desirable gas fill consists of indium triiodide. A dosing technique for such a fill has consisted of placing a small sphere of indium into the lamp bulb, and introducing iodine by passing argon gas over a heated reservoir of iodine crystals and hence into the lamp bulb. When the lamp is next heated, as by sealing a lead or by test-operating it, the indium vaporizes and mixes with the iodine gas. Upon subsequent cooling, between operating periods, the fill gas partially condenses on the inside of the bulb. To achieve the desired lamp fill of the stoichiometric compound lnl the ratio of indium to iodine must be carefully controlled. Such control is difficult due to the many variable parameters such the size of the indium sphere, and the temperature, rate of flow, and time period of introducing the iodine. If there is an excess of iodine in the lamp fill, the lamp is difficult to start (if an arc lamp) and the useful life of its seals is shortened. lfthere is an excess of indium, the operating voltage may be too low (if an arc lamp) and the inner wall of the lamp is likely to darken from evaporated filament or electrode material.
SUMMARY OF THE INVENTION Objects of the invention are to provide an improved method of manufacturing gas-filled lamps, and to provide an improved method of dosing lamps with a gas fill.
The method of the invention comprises, briefly and in a preferred embodiment, the steps of placing lampdosage material in tubing of plastic material, slicing the tubing and its contents at intervals for providing desired quantities of dosage material, and removing the dosage material segments from the sliced tubing segments and placing them into respective lamp bulbs. A preferred dosage material is indium triiodide, and a preferred plastic tubing material is Teflon.
BRIEF DESCRIPTION OF THE DRAWING sliced into segments;
FIG. 3 is a cross-sectional view of the tubing and its contents taken on the line 3--3 of FIG. 2; and
FIG. 4 is a side view of a lamp bulb and a section of the slicedplastic tubing, showing the dosage material being ejected from the tubing segment and into the lamp bulb.
DESCRIPTION OF THE PREFERRED EMBODIMENT As shown in FIG. 1, a length of tubing 11 of plastic material having a slippery surface, such as Teflon, is
filled with lamp-dosage material 12. This may be accomplished by placing an end of the plastic tubing 11 into molten dosage material, such as indium triiodide, and applying sufficient vacuum at the other end of the plastic tubing 11 to drawindium triiodide into the tubing whereupon it cools and solidifies. If storage is desired, it should be sealed in dried-out glass tubing. The tubing 11 and its contents are sliced, as shown in FIG. 2, by means'of a sharp thin knife or razor blade 13, to provide a plurality of segments '14 of sliced tubing each containing the proper amount of dosage material for a lamp.
As shown in-FIG. 4, the sliced segment or pellet 16 of indium triiodide is ejected from the sliced segment of tubing 14, by means of a plunger 17 inserted into the tubing segment 14, whereupon the pellet 16 drops into a lamp bulb 18. Instead of ejecting the pellet 16 directly into the, bulb 18, the pellet 16 may be temporarily stored in a dispenser means from which it is placed into the bulb 18. The bulb 18 is shown, by way of example, as being a partly assembled lamp of the type shown and described in the aforesaid US. Pat. No. 3,305,289, the bulb being made of quartz an containing a bulbous arc chamber region 19. An electrode assembly consisting of an electrode 21, connection lead 22, and interconnecting metal foil 23, has been pinch-sealed at 26 in one stem of the bulb 18. After the lamp has been dosed with the pellet 16, it is evacuated and filled with argon at suitable pressure, and another electrode is sealed at the remaining stem of the bulb l8.
While making the aforesaid final electrode seal, or upon initial test operation of the lamp, the lamp becomes sufficiently hot so that the pellet 16 contained therein vaporizes, thus providing the desired final gas fill.
It will be apparent that the invention achieves accurate dosing of a lamp in a low cost manner, as it is much quicker and more economical to dispense the pellet 16 into bulb 18, rather than to flow a gaseous vapor therethrough for a period of several seconds or minutes. Also, a solid compound such as indium triiodide can be utilized for generating the gas fill, in accordance with the method of the invention, to provide a gas fill of true stoichiometric characteristics, thereby insuring proper operation of the lamp.
The method of first placing the dosage material into the plastic tubing, and slicing the tubing into accuratelength segments, insures proper amounts of dosage material for the lamp, and the plastic material is easily sliced accurately, and leaves no burrs at the sliced surfaces, such as would be the case if metal tubing were used, whereby the invention permits the pellet 16 to be readily forced out of the tubing segment 14. Ejection of the pellet 16 is also facilitated by the use of a plastic material such as Teflon, having a slippery surface, and the inherent slight resiliency of the plastic material 3. further aids in ejecting the pellet 16. Also, the plastic tubing does not contaminate the dosage material as would be like if metal tubing were used. The aforesaid desirable characteristics of the plastic tubing for the purposes of the invention are extremely important, due to the small size of the pellet 16, which, for use in a typical 300-watt arc discharge lamp having an arc chamber of approximately one cubic centimeter or v less, is only 0.020 inches diameter and approximately 0.050 inches long. Teflon and similar plastic materials have a melting point of 300C or higher, whereas the dosage material indium triiodide has a melting point of 210C, so that there is no problem in the initial step of drawing molten indium triiodide into the plastic tubing.
While a preferred embodiment of the invention has been shown and described, other embodiments and modifications thereof will become apparent to persons skilled in the art, and will fall within the scope of the invention as defined in the following claims.
What I claim as new and desire to secure by Letters Patent of the United States is:
l. A method of providing pellets of dosage material in lamp bulbs in the manufacture of gas-filled lamps, comprising the steps of placing an end of a length of plastic tubing into molten dosage material, applying vacuum at the other end of said tubing to draw molten dosage material into the tubing, allowing said dosage material to cool and solidify in the tubing, slicing the tubing and its contents into segments each containing the desired amount of dosage material for a lamp, and ejecting the solid dosage material segments from the tubing segments by means of a plunger and placing them in respective lamp bulbs.
2. A method as claimed in claim 1 in which said plastic tubing is of a material having a slippery surface.
3. A method as claimed in claim 2 in which said plastic tubing is made of Teflon.
4. A method as claimed in claim 1 in which said dosage material is indium triiodide.
5. A method as claimed in claim 1 in which said plastic tubing is made of Teflon and in which said dosage material is indium triiodide.

Claims (4)

  1. 2. A method as claimed in claim 1 in which said plastic tubing is of a material having a slippery surface.
  2. 3. A method as claimed in claim 2 in which said plastic tubing is made of Teflon.
  3. 4. A method as claimed in claim 1 in which said dosage material is indium triiodide.
  4. 5. A method as claimed in claim 1 in which said plastic tubing is made of Teflon and in which said dosage material is indium triiodide.
US72051A 1970-09-14 1970-09-14 Method of dosing lamps Expired - Lifetime US3689799A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0374679A2 (en) * 1988-12-19 1990-06-27 Patent-Treuhand-Gesellschaft für elektrische Glühlampen mbH Method for producing a two-sided high-pressure discharge lamp
EP0374676A2 (en) * 1988-12-19 1990-06-27 Patent-Treuhand-Gesellschaft für elektrische Glühlampen mbH Method for producing a two-sided high-pressure discharge lamp
EP0374677A2 (en) * 1988-12-19 1990-06-27 Patent-Treuhand-Gesellschaft für elektrische Glühlampen mbH Method for producing a two-sided high-pressure discharge lamp
US5108333A (en) * 1988-12-19 1992-04-28 Patent Treuhand fur elektrische Gluhlampen m.b.H. Method of making a double-ended high-pressure discharge lamp

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1565564A (en) * 1923-07-23 1925-12-15 Westinghouse Lamp Co Method of and means for introducing potassium or other vapors in lamps
US1623323A (en) * 1923-08-18 1927-04-05 Westinghouse Lamp Co Method of introducing volatile matter into lamps and the like
US1877718A (en) * 1929-12-12 1932-09-13 Claude Neon Lights Inc Method of inserting materials in envelopes
US3510189A (en) * 1967-11-13 1970-05-05 Westinghouse Electric Corp Method of dosing incandescible lamps with halogen

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1565564A (en) * 1923-07-23 1925-12-15 Westinghouse Lamp Co Method of and means for introducing potassium or other vapors in lamps
US1623323A (en) * 1923-08-18 1927-04-05 Westinghouse Lamp Co Method of introducing volatile matter into lamps and the like
US1877718A (en) * 1929-12-12 1932-09-13 Claude Neon Lights Inc Method of inserting materials in envelopes
US3510189A (en) * 1967-11-13 1970-05-05 Westinghouse Electric Corp Method of dosing incandescible lamps with halogen

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0374679A2 (en) * 1988-12-19 1990-06-27 Patent-Treuhand-Gesellschaft für elektrische Glühlampen mbH Method for producing a two-sided high-pressure discharge lamp
EP0374676A2 (en) * 1988-12-19 1990-06-27 Patent-Treuhand-Gesellschaft für elektrische Glühlampen mbH Method for producing a two-sided high-pressure discharge lamp
EP0374677A2 (en) * 1988-12-19 1990-06-27 Patent-Treuhand-Gesellschaft für elektrische Glühlampen mbH Method for producing a two-sided high-pressure discharge lamp
EP0374677A3 (en) * 1988-12-19 1991-05-08 Patent-Treuhand-Gesellschaft für elektrische Glühlampen mbH Method for producing a two-sided high-pressure discharge lamp
EP0374676A3 (en) * 1988-12-19 1991-05-08 Patent-Treuhand-Gesellschaft für elektrische Glühlampen mbH Method for producing a two-sided high-pressure discharge lamp
EP0374679A3 (en) * 1988-12-19 1991-05-08 Patent-Treuhand-Gesellschaft für elektrische Glühlampen mbH Method for producing a two-sided high-pressure discharge lamp
US5108333A (en) * 1988-12-19 1992-04-28 Patent Treuhand fur elektrische Gluhlampen m.b.H. Method of making a double-ended high-pressure discharge lamp

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