US3607098A - Containers for laboratory use - Google Patents
Containers for laboratory use Download PDFInfo
- Publication number
- US3607098A US3607098A US768229A US3607098DA US3607098A US 3607098 A US3607098 A US 3607098A US 768229 A US768229 A US 768229A US 3607098D A US3607098D A US 3607098DA US 3607098 A US3607098 A US 3607098A
- Authority
- US
- United States
- Prior art keywords
- container
- sedimentation tube
- closure
- tube
- sedimentation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000004062 sedimentation Methods 0.000 claims abstract description 36
- 239000007788 liquid Substances 0.000 abstract description 11
- 210000004369 blood Anatomy 0.000 abstract description 10
- 239000008280 blood Substances 0.000 abstract description 10
- 239000000203 mixture Substances 0.000 description 9
- 238000003780 insertion Methods 0.000 description 5
- 230000037431 insertion Effects 0.000 description 5
- KRKNYBCHXYNGOX-UHFFFAOYSA-K Citrate Chemical compound [O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O KRKNYBCHXYNGOX-UHFFFAOYSA-K 0.000 description 4
- 210000000601 blood cell Anatomy 0.000 description 4
- 230000002093 peripheral effect Effects 0.000 description 4
- 238000007789 sealing Methods 0.000 description 4
- 239000003814 drug Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 206010023126 Jaundice Diseases 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 208000015181 infectious disease Diseases 0.000 description 1
- 230000002458 infectious effect Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 210000002700 urine Anatomy 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
- B01L3/00—Containers or dishes for laboratory use, e.g. laboratory glassware; Droppers
- B01L3/50—Containers for the purpose of retaining a material to be analysed, e.g. test tubes
- B01L3/508—Containers for the purpose of retaining a material to be analysed, e.g. test tubes rigid containers not provided for above
- B01L3/5082—Test tubes per se
Definitions
- This invention relates to a container for laboratory use, particularly but not exclusively for use in collecting blood for sedimentation tests, i.e. determining the rate of sinking of blood corpuscles.
- the sedimentation tube has been provided with a nonreturn valve, which is not only expensive but also makes it difficult to fill the sedimentation tube to the correct height and in particular to clean the sedimentation tube after use.
- lntemally ground cylinders have also been proposed which have a diameter such that the sedimentation tube upon being inserted into the cylinder, acts as a piston so that the mixture is pressed upwardly into the tube.
- Such cylinders are expensive and therefore cannot be thrown away after use but must be cleaned. Also, without additional measures, they are not suited for transporting a specimen.
- the present invention provides a container for laboratory use, having a closure which has a thick peripheral part adapted to tighten against an edge of the container and having a thinner middle part adapted to tighten around a sedimentation tube or pipette upon being pierced by such tube or pipette.
- This arrangement ensures that the liquid, which is tightly enclosed in the container and which can therefore be readily transported, can be removed in the desired amounts from the container by insertion of a sedimentation tube or a pipette into the container, the liquid being forced into the sedimentation tube or the pipette following the insertion thereof. Moreover, it ensures that the laboratory technician does not get into contact with the liquid. The container, together with the remaining liquid, may be thrown away after use.
- the container is particularly suited for collecting blood for measurement of the rate of sinking of the blood corpuscles, in which case the container, together with the inserted sedimentation tube can be placed in a frame until the sedimentation test has been completed, after which both can be thrown away.
- the sedimentation tube can be drawn from the container, whereby the surface of the sedimentation tube is cleaned of the fluid mixture by its passage through the closure, while the container with its blood and citrate may be thrown away.
- the diameter of the thinner middle part of the closure may correspond to the outer diameter of asedimentation tube, so that the thinner middle part by insertion of a sedimentation tube into the container is pressed apart and the sedimentation tube bears against the inner side of the peripheral part of the closure to ensure good sealing.
- the middle part of the closure may have a rupturing mark.
- the middle part of the container may have a wall thickness which is so small that this part is resilient and can be pressed together, so that liquid can be readil pressed up from the contamer into, for example, a pipette.
- a sedimentation tube is to be filled with blood from the container the required height of liquid in the sedimentation tube can be adjusted by squeezing the middle part of the container.
- the invention is illustrated in the drawing, which shows a vertical, longitudinal section through one embodiment of the container.
- a container 1 is made of a suitable plastics material and is provided with an opening defined by annular wall and with a closure 2 which closes the opening of the container in an air: tight manner since the closure 2 has a thick peripheral part adapted to close tightly around the outer surface of the annu lar wall of the container.
- the closure 2 also has a thin middle part 5 which can be pierced by a sedimentation tube or a pipette.
- the closure has a substantial inner frustoconical part 6, located within the opening spaced from the inner surface of the annular wall and which is closed at the bottom by the mid dle part 5 and against the inner side of which the sediment..- tion tube can bear so that good sealing is obtained by insertion of the sedimentation tube.
- the upper part 4 of the container has a wall thickness which is sufficiently large to ensure that when the closure is fitted good sealing can be obtained, the upper part of the container having a corresponding stiffness.
- the middle part of the container has a wall thickness which is so small that this part can be easily pressed together, whereby for example liquid can be pressed upward to exactly the required height in a sedimentation tube.
- the position at which the large and small wall thicknesses meet each other can indicate the height which the mixture of blood and citrate solution should reach in the container.
- the lower part or bottom 3 of the container has such a shape that it fits closely around the tip or lower part of the sedimentation tube. In this way sufficient sealing is obtained to ensure that when the sedimentation tube is pushed right into the container the mixture of blood and citrate solution remains at the same height in the sedimentation tube until the rate of sinking of the blood corpuscles is measured.
- a device for laboratory use comprising a container having an opening defined by an annular wall having an outer surface; and closure means for tightly closing said opening, said closure means having an outer peripheral part tightly engaging said outer surface of said annular wall and wall means within said opening integral with said outer part, and a thin pierceable bottom portion integral with said wall means so as to close said opening, said bottom portion having a wall thickness smaller than that of said outer part, and said wall means being constructed to close fluidtightly about a sedimentation tube when said bottom portion is pierced by said tube.
- said wall means comprise an inner frustoconical part which is closed at the bottom by said pierceable bottom portion, said frustoconical part having an outer surface radially inwardly spaced from the inner surface of said annular wall.
Landscapes
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- General Health & Medical Sciences (AREA)
- Hematology (AREA)
- Clinical Laboratory Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Investigating Or Analysing Biological Materials (AREA)
- Measurement Of The Respiration, Hearing Ability, Form, And Blood Characteristics Of Living Organisms (AREA)
- Sampling And Sample Adjustment (AREA)
- Devices For Use In Laboratory Experiments (AREA)
- Automatic Analysis And Handling Materials Therefor (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DK525967 | 1967-10-23 |
Publications (1)
Publication Number | Publication Date |
---|---|
US3607098A true US3607098A (en) | 1971-09-21 |
Family
ID=8140916
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US768229A Expired - Lifetime US3607098A (en) | 1967-10-23 | 1968-10-17 | Containers for laboratory use |
Country Status (5)
Country | Link |
---|---|
US (1) | US3607098A (enrdf_load_stackoverflow) |
DE (1) | DE1803281C3 (enrdf_load_stackoverflow) |
ES (1) | ES159050Y (enrdf_load_stackoverflow) |
FR (1) | FR1586053A (enrdf_load_stackoverflow) |
GB (1) | GB1247520A (enrdf_load_stackoverflow) |
Cited By (35)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5034283U (enrdf_load_stackoverflow) * | 1973-07-24 | 1975-04-12 | ||
US4024857A (en) * | 1974-12-23 | 1977-05-24 | Becton, Dickinson And Company | Micro blood collection device |
US4056361A (en) * | 1975-06-11 | 1977-11-01 | The Secretary Of State For Social Services In Her Britannic Majesty's Government Of The United Kingdom Of Great Britain And Northern Ireland | Vial or other container, and carrier therefor |
US4106907A (en) * | 1976-02-13 | 1978-08-15 | The Radiochemical Centre Limited | Centrifuge tube and method for performing assay with same |
US4215700A (en) * | 1978-08-25 | 1980-08-05 | Sherwood Medical Industries Inc. | Blood collection device |
US4278437A (en) * | 1979-04-09 | 1981-07-14 | Jan Haggar | Fluid specimen holder for biological fluid testing |
US4308028A (en) * | 1980-04-14 | 1981-12-29 | Elkins Carlos D | Device and method for the chemical testing and microscopic examination of liquid specimens |
US4652429A (en) * | 1984-01-11 | 1987-03-24 | C. A. Greiner & Sohne Gesellschaft M.B.H. | Biological sampling tube |
US4769335A (en) * | 1985-12-02 | 1988-09-06 | Ncs Diagnostics Inc. | Method and apparatus for transporting photosensitive fluids |
US4799599A (en) * | 1982-07-30 | 1989-01-24 | Ciba Corning Diagnostics Corp. | Specimen cup and cap assembly for clinical analyzer |
US4933145A (en) * | 1985-05-10 | 1990-06-12 | Terumo Kabushiki Kaisha | Apparatus for inhibiting glycolysis in blood samples |
US4960219A (en) * | 1989-09-08 | 1990-10-02 | Abbott Laboratories | Snap cap |
US5092855A (en) * | 1990-01-22 | 1992-03-03 | Reseal International Limited Partnership | Enclosing sleeve for one-way valve |
US5224515A (en) * | 1992-01-30 | 1993-07-06 | Porex Technologies Corp. | Tube closure |
US5285253A (en) * | 1990-12-17 | 1994-02-08 | Bernd Kloth | Cuvette for holding substances to be analyzed by optical means |
US5573567A (en) * | 1993-06-30 | 1996-11-12 | Shigemi Co., Ltd. | Method of manufacturing sample tube for nuclear magnetic resonance |
US5602756A (en) * | 1990-11-29 | 1997-02-11 | The Perkin-Elmer Corporation | Thermal cycler for automatic performance of the polymerase chain reaction with close temperature control |
US5795784A (en) * | 1996-09-19 | 1998-08-18 | Abbott Laboratories | Method of performing a process for determining an item of interest in a sample |
USD401697S (en) | 1997-05-21 | 1998-11-24 | Abbott Laboratories | Container |
US5856194A (en) * | 1996-09-19 | 1999-01-05 | Abbott Laboratories | Method for determination of item of interest in a sample |
US5881596A (en) * | 1993-09-30 | 1999-03-16 | Itochu Corporation | Urine sampling vessel |
US5916525A (en) * | 1991-12-03 | 1999-06-29 | Eppendorf-Netheler-Hinz Gmbh | Closure vessel assembly |
US5915583A (en) * | 1997-05-21 | 1999-06-29 | Abbott Laboraties | Container |
US6056925A (en) * | 1996-11-19 | 2000-05-02 | Sarstedt Ag & Co. | Sample vessel for taking blood samples |
USD457247S1 (en) | 2000-05-12 | 2002-05-14 | Gen-Probe Incorporated | Cap |
US20020127147A1 (en) * | 2001-03-09 | 2002-09-12 | Kacian Daniel L. | Penetrable cap |
US6660228B1 (en) * | 1998-03-02 | 2003-12-09 | Cepheid | Apparatus for performing heat-exchanging, chemical reactions |
US6716396B1 (en) | 1999-05-14 | 2004-04-06 | Gen-Probe Incorporated | Penetrable cap |
US20070187353A1 (en) * | 2006-02-13 | 2007-08-16 | Tripath Imaging, Inc. | Container assembly and pressure-responsive penetrable cap for the same |
US7306129B2 (en) | 2005-11-03 | 2007-12-11 | Stewart Swiss | One way valve assembly |
US20150166219A1 (en) * | 2010-01-29 | 2015-06-18 | Integrity Products, Inc. | Perforable container cap |
WO2015126598A1 (en) * | 2014-02-21 | 2015-08-27 | ORIGIO Inc. | Pipette tip containers |
USD801545S1 (en) * | 2016-02-19 | 2017-10-31 | Treff Ag Degersheim | Test tube |
USD977142S1 (en) * | 2016-08-18 | 2023-01-31 | Sio2 Medical Products, Inc. | Vial |
US20230226541A1 (en) * | 2022-01-18 | 2023-07-20 | Hollister Incorporated | Fluid absorption test tube |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4187719A (en) * | 1977-08-11 | 1980-02-12 | B. Braun Melsungen Aktiengesellschaft | Apparatus to determine the sedimentation rate of red blood cells |
BR7808764A (pt) * | 1978-11-28 | 1981-06-30 | Dematex Dev & Invest | Tubo e rolha para sistemas de amostragem de sangue |
DE9006079U1 (de) * | 1990-05-30 | 1990-09-13 | Bethkenhagen, Jürgen, 5223 Nümbrecht | Deckel |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2693892A (en) * | 1949-07-07 | 1954-11-09 | William Jacques Herter | Container sealing means |
-
1968
- 1968-10-04 GB GB47264/68A patent/GB1247520A/en not_active Expired
- 1968-10-16 DE DE1803281A patent/DE1803281C3/de not_active Expired
- 1968-10-17 US US768229A patent/US3607098A/en not_active Expired - Lifetime
- 1968-10-22 FR FR1586053D patent/FR1586053A/fr not_active Expired
- 1968-10-23 ES ES1968159050U patent/ES159050Y/es not_active Expired
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2693892A (en) * | 1949-07-07 | 1954-11-09 | William Jacques Herter | Container sealing means |
Cited By (64)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5034283U (enrdf_load_stackoverflow) * | 1973-07-24 | 1975-04-12 | ||
US4024857A (en) * | 1974-12-23 | 1977-05-24 | Becton, Dickinson And Company | Micro blood collection device |
US4056361A (en) * | 1975-06-11 | 1977-11-01 | The Secretary Of State For Social Services In Her Britannic Majesty's Government Of The United Kingdom Of Great Britain And Northern Ireland | Vial or other container, and carrier therefor |
US4106907A (en) * | 1976-02-13 | 1978-08-15 | The Radiochemical Centre Limited | Centrifuge tube and method for performing assay with same |
US4215700A (en) * | 1978-08-25 | 1980-08-05 | Sherwood Medical Industries Inc. | Blood collection device |
US4278437A (en) * | 1979-04-09 | 1981-07-14 | Jan Haggar | Fluid specimen holder for biological fluid testing |
US4308028A (en) * | 1980-04-14 | 1981-12-29 | Elkins Carlos D | Device and method for the chemical testing and microscopic examination of liquid specimens |
US4799599A (en) * | 1982-07-30 | 1989-01-24 | Ciba Corning Diagnostics Corp. | Specimen cup and cap assembly for clinical analyzer |
US4652429A (en) * | 1984-01-11 | 1987-03-24 | C. A. Greiner & Sohne Gesellschaft M.B.H. | Biological sampling tube |
US4933145A (en) * | 1985-05-10 | 1990-06-12 | Terumo Kabushiki Kaisha | Apparatus for inhibiting glycolysis in blood samples |
US4769335A (en) * | 1985-12-02 | 1988-09-06 | Ncs Diagnostics Inc. | Method and apparatus for transporting photosensitive fluids |
US4960219A (en) * | 1989-09-08 | 1990-10-02 | Abbott Laboratories | Snap cap |
US5092855A (en) * | 1990-01-22 | 1992-03-03 | Reseal International Limited Partnership | Enclosing sleeve for one-way valve |
US5602756A (en) * | 1990-11-29 | 1997-02-11 | The Perkin-Elmer Corporation | Thermal cycler for automatic performance of the polymerase chain reaction with close temperature control |
US6015534A (en) * | 1990-11-29 | 2000-01-18 | The Perkin-Elmer Corporation | PCR sample tube |
US5285253A (en) * | 1990-12-17 | 1994-02-08 | Bernd Kloth | Cuvette for holding substances to be analyzed by optical means |
US5916525A (en) * | 1991-12-03 | 1999-06-29 | Eppendorf-Netheler-Hinz Gmbh | Closure vessel assembly |
US5224515A (en) * | 1992-01-30 | 1993-07-06 | Porex Technologies Corp. | Tube closure |
US5573567A (en) * | 1993-06-30 | 1996-11-12 | Shigemi Co., Ltd. | Method of manufacturing sample tube for nuclear magnetic resonance |
US5881596A (en) * | 1993-09-30 | 1999-03-16 | Itochu Corporation | Urine sampling vessel |
US5856194A (en) * | 1996-09-19 | 1999-01-05 | Abbott Laboratories | Method for determination of item of interest in a sample |
US6562298B1 (en) | 1996-09-19 | 2003-05-13 | Abbott Laboratories | Structure for determination of item of interest in a sample |
US5795784A (en) * | 1996-09-19 | 1998-08-18 | Abbott Laboratories | Method of performing a process for determining an item of interest in a sample |
US6056925A (en) * | 1996-11-19 | 2000-05-02 | Sarstedt Ag & Co. | Sample vessel for taking blood samples |
US5915583A (en) * | 1997-05-21 | 1999-06-29 | Abbott Laboraties | Container |
USD401697S (en) | 1997-05-21 | 1998-11-24 | Abbott Laboratories | Container |
US6660228B1 (en) * | 1998-03-02 | 2003-12-09 | Cepheid | Apparatus for performing heat-exchanging, chemical reactions |
US8535621B2 (en) | 1999-05-14 | 2013-09-17 | Gen-Probe Incorporated | Penetrable cap having rib structures |
US8211710B2 (en) | 1999-05-14 | 2012-07-03 | Dickey Kathleen A | Method for accessing the contents of a closed collection device |
US6716396B1 (en) | 1999-05-14 | 2004-04-06 | Gen-Probe Incorporated | Penetrable cap |
US6723289B2 (en) | 1999-05-14 | 2004-04-20 | Gen-Probe Incorporated | Fluid transfer device |
US6806094B2 (en) | 1999-05-14 | 2004-10-19 | Gen-Probe Incorporated | Method for removing a fluid substance from a collection device |
US8573072B2 (en) | 1999-05-14 | 2013-11-05 | Gen-Probe Incorporated | Method for removing a fluid substance from a sealed collection device |
US7927549B2 (en) | 1999-05-14 | 2011-04-19 | Gen-Probe Incorporated | Method for accessing the contents of a closed collection device with a modified pipette tip |
US8334145B2 (en) | 1999-05-14 | 2012-12-18 | Gen-Probe Incorporated | Pierceable cap having spaced-apart grooves |
US7276383B2 (en) | 1999-05-14 | 2007-10-02 | Gen-Probe Incorporated | Method for obtaining the contents of a fluid-holding vessel |
US7795036B2 (en) | 1999-05-14 | 2010-09-14 | Gen-Probe Incorporated | Method for accessing the contents of a closed collection device |
US8206662B2 (en) | 1999-05-14 | 2012-06-26 | Gen-Probe Incorporated | Collection device including a penetrable cap having an absorbent pile fabric |
US7309469B2 (en) | 1999-05-14 | 2007-12-18 | Gen-Probe Incorporated | Collection device |
US7435389B2 (en) | 1999-05-14 | 2008-10-14 | Gen-Probe Incorporated | Sealed collection device having striated cap |
US7648680B2 (en) | 1999-05-14 | 2010-01-19 | Gen-Probe Incorporated | Method for accessing the contents of a closed vessel containing a specimen retrieval device |
US8038967B2 (en) | 1999-05-14 | 2011-10-18 | Gen-Probe Incorporated | Method for accessing the contents of a closed vessel containing a specimen retrieval device |
US7462323B1 (en) | 1999-12-21 | 2008-12-09 | Cepheid | Apparatus for performing heat-exchanging chemical reactions |
USD457247S1 (en) | 2000-05-12 | 2002-05-14 | Gen-Probe Incorporated | Cap |
US20050079633A1 (en) * | 2001-03-09 | 2005-04-14 | Gen-Probe Incorporated | Method for transferring a substance to or from a closed system |
USRE45194E1 (en) | 2001-03-09 | 2014-10-14 | Gen-Probe Incorporated | Penetrable cap |
US7691332B2 (en) | 2001-03-09 | 2010-04-06 | Gen-Probe Incorporated | Penetrable cap |
US7824922B2 (en) | 2001-03-09 | 2010-11-02 | Gen-Probe Incorporated | Method for removing a fluid substance from a closed system |
US8052944B2 (en) | 2001-03-09 | 2011-11-08 | Gen-Probe Incorporated | Penetrable cap |
US8057762B2 (en) | 2001-03-09 | 2011-11-15 | Gen-Probe Incorporated | Penetrable cap |
US8685347B2 (en) | 2001-03-09 | 2014-04-01 | Gen-Probe Incorporated | Penetrable cap |
US20020127147A1 (en) * | 2001-03-09 | 2002-09-12 | Kacian Daniel L. | Penetrable cap |
US7294308B2 (en) | 2001-03-09 | 2007-11-13 | Gen-Probe Incorporated | Penetrable cap |
US6893612B2 (en) | 2001-03-09 | 2005-05-17 | Gen-Probe Incorporated | Penetrable cap |
US7306129B2 (en) | 2005-11-03 | 2007-12-11 | Stewart Swiss | One way valve assembly |
US7513396B2 (en) | 2005-11-03 | 2009-04-07 | Reseal International Limited Partnership | One way valve assembly |
US20070187353A1 (en) * | 2006-02-13 | 2007-08-16 | Tripath Imaging, Inc. | Container assembly and pressure-responsive penetrable cap for the same |
US8177084B2 (en) | 2006-02-13 | 2012-05-15 | Tripath Imaging, Inc. | Container assembly and pressure-responsive penetrable cap for the same |
US20150166219A1 (en) * | 2010-01-29 | 2015-06-18 | Integrity Products, Inc. | Perforable container cap |
WO2015126598A1 (en) * | 2014-02-21 | 2015-08-27 | ORIGIO Inc. | Pipette tip containers |
US9956560B2 (en) | 2014-02-21 | 2018-05-01 | ORIGIO Inc. | Pipette tip containers |
USD801545S1 (en) * | 2016-02-19 | 2017-10-31 | Treff Ag Degersheim | Test tube |
USD977142S1 (en) * | 2016-08-18 | 2023-01-31 | Sio2 Medical Products, Inc. | Vial |
US20230226541A1 (en) * | 2022-01-18 | 2023-07-20 | Hollister Incorporated | Fluid absorption test tube |
Also Published As
Publication number | Publication date |
---|---|
GB1247520A (en) | 1971-09-22 |
DE1803281C3 (de) | 1978-10-12 |
ES159050U (es) | 1970-08-01 |
DE1803281A1 (de) | 1969-08-07 |
ES159050Y (es) | 1971-04-16 |
FR1586053A (enrdf_load_stackoverflow) | 1970-02-06 |
DE1803281B2 (de) | 1978-02-09 |
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