US3542035A - Tobacco foils having improved wet strength - Google Patents

Tobacco foils having improved wet strength Download PDF

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Publication number
US3542035A
US3542035A US726552A US3542035DA US3542035A US 3542035 A US3542035 A US 3542035A US 726552 A US726552 A US 726552A US 3542035D A US3542035D A US 3542035DA US 3542035 A US3542035 A US 3542035A
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US
United States
Prior art keywords
water
tobacco
soluble
gum
xanthan
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US726552A
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English (en)
Inventor
Wolfgang Dierichs
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Henkel AG and Co KGaA
Original Assignee
Henkel AG and Co KGaA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Henkel AG and Co KGaA filed Critical Henkel AG and Co KGaA
Application granted granted Critical
Publication of US3542035A publication Critical patent/US3542035A/en
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Expired - Lifetime legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/12Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco

Definitions

  • This invention relates to a tobacco foil having improved wet strength comprising a dried aqueous mixture of tobacco powder and a water-soluble, film-forming agent, a portion of said water-soluble, film-forming agent consisting of a compound selected from the group consisting of water-soluble xanthan-gum and water-soluble derivatives of xanthangum in admixture with a water soluble cellulose ether.
  • the tobacco foils obtained according to the process of the invention, are distinguished by a considerably improved wet strength. This wet strength in dry condition is equal or superior to that of the known foils.
  • the foils, prepared according to the process of the invention, can be used as tobacco wrappers for cigars, cigarillos or small cigars, because they do not impair the taste of the tobacco, but effect a favorable influence on the burning of the tobacco goods.
  • EXAMPLES I 3 One hundred gram of tobacco powder were introduced into 160 g. of water and g. of ethylene glycol. The mixture was then thoroughly kneaded by hand.
  • binding agents were introduced into 600 g. of water, and the mixture was allowed to stand until it had completely swelled (l2 hours). Thereafter, while stirring, 8 g. of a 30 percent aqueous glyoxal solution were added.
  • the binding agent consisted of a mixture of methylcellulose 1,000 CP in 2 percent aqueous solution at 20C., according to Hoeppler) and xanthan-gum (4,000 CP in 2 percent aqueous solution at 20C., according to Hoeppler).
  • the binding agents for each example had the following quantitative compositions: (l) 18 g. of methylcellulose and 2 g. of xanthan-gum; (2) 16 g. of methylcellulose and 4 g. of xanthangum; (3) 12 g. of methylcellulose and 8 g. of xanthan-gum.
  • the foils of 100 X 15 mm. were subjected to a weight load of 200 mg. and suspended to a depth of 50 mm. in water, adjusted to a pH 7 at C.
  • the time, at which the tearing of the foils occurred, was measured as follows:
  • Example 1 binder 16 minutes.
  • Example 2 binder 220 minutes.
  • Example 3 binder 325 minutes.
  • EXAMPLES 49 One hundred gram of tobacco powder were introduced into a mixture of 160 g. of water and 5 g. of ethylene glycol, and this mixture was thoroughly kneaded by hand.
  • the binding agent consisted of a mixture of methylcellulose (1,000 CP in 2 percent aqueous solution at 20C., according to Hoeppler), and of deacetylated xanthan-gum.
  • composition of the binding agents is given in the following table.
  • the first columns indicate the consecutive number of the examples and the amounts of methylcellulose and deacetylated xanthan-gum utilized; the following columns indicate the wet strength and the dry strength measured on the tobacco foils.
  • the working up into foils and determination of the wet strength was effected in the same manner as described in the preceding examples.
  • the dry strength was determined by means of 10 different samples, each on a conventional tensite-testing apparatus.
  • a tobacco foil having improved wet strength comprising a dried aqueous mixture of tobacco powder and a water-soluble, film-forming agent in a ratio of from 10 to 30 parts of said water-soluble, film-forming agent to 100 parts of tobacco powder, of said water-soluble, film-forming agent consisting of a mixture of water-soluble cellulose ether and at least 3 percent of said mixture of xanthan-gum selected from the group consisting of water-soluble xanthan-gum and water-soluble derivatives of xanthan-gum, said xanthan-gum being prepared by the action of Xanthomonas campestris.
  • said water-soluble, film-forming agent is a mixture of from 97 percent to 40 percent of a water-soluble cellulose ether and from 3 percent to 60 percent of a compound selected from the group consisting of water-soluble xanthan-gum and water-soluble derivatives of xanthan-gum.
  • said water-soluble, film-forming agent is a mixture of from 94 percent to 55 percent of a water-soluble cellulose ether and from 6 percent to 45 percent of a compound selected from the group consisting of water-soluble xanthan-gum and water-soluble derivatives of xanthan-gum.
  • said water-soluble cellulose ether is a methylcellulose with a substitution degree of about 1 to 2 and with a viscosity of about 200 to 4,000 CP, in a 2 percent aqueous solution at 20C., according to Hoeppler.
  • the tobacco foil of claim 1 comprising a content of a bivalent aldehyde.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Paper (AREA)
US726552A 1967-06-05 1968-05-03 Tobacco foils having improved wet strength Expired - Lifetime US3542035A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DEH0062921 1967-06-05

Publications (1)

Publication Number Publication Date
US3542035A true US3542035A (en) 1970-11-24

Family

ID=7162082

Family Applications (1)

Application Number Title Priority Date Filing Date
US726552A Expired - Lifetime US3542035A (en) 1967-06-05 1968-05-03 Tobacco foils having improved wet strength

Country Status (6)

Country Link
US (1) US3542035A (pt)
BR (1) BR6899561D0 (pt)
CH (1) CH532371A (pt)
DE (1) DE1692918A1 (pt)
FR (1) FR1559278A (pt)
NL (1) NL6806496A (pt)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3878851A (en) * 1973-03-08 1975-04-22 Liggett & Myers Inc Tobacco casing material
US3908671A (en) * 1973-12-12 1975-09-30 Brown & Williamson Tobacco Thermoplastic cigarette wrapper
US4072155A (en) * 1976-07-15 1978-02-07 Lorillard, a division of Loews Theatres-Inc. Stiffening of tobacco with dialdehyde
US4143666A (en) * 1975-08-15 1979-03-13 Philip Morris Incorporated Smoking material
US4880018A (en) * 1986-02-05 1989-11-14 R. J. Reynolds Tobacco Company Extruded tobacco materials

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3878851A (en) * 1973-03-08 1975-04-22 Liggett & Myers Inc Tobacco casing material
US3908671A (en) * 1973-12-12 1975-09-30 Brown & Williamson Tobacco Thermoplastic cigarette wrapper
US4143666A (en) * 1975-08-15 1979-03-13 Philip Morris Incorporated Smoking material
US4072155A (en) * 1976-07-15 1978-02-07 Lorillard, a division of Loews Theatres-Inc. Stiffening of tobacco with dialdehyde
US4880018A (en) * 1986-02-05 1989-11-14 R. J. Reynolds Tobacco Company Extruded tobacco materials

Also Published As

Publication number Publication date
DE1692918A1 (de) 1971-10-28
BR6899561D0 (pt) 1973-02-06
NL6806496A (pt) 1968-12-06
CH532371A (de) 1973-01-15
FR1559278A (pt) 1969-03-07

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