US3270118A - Process for the vacuum melting of metals by means of electron beam - Google Patents

Process for the vacuum melting of metals by means of electron beam Download PDF

Info

Publication number
US3270118A
US3270118A US293355A US29335563A US3270118A US 3270118 A US3270118 A US 3270118A US 293355 A US293355 A US 293355A US 29335563 A US29335563 A US 29335563A US 3270118 A US3270118 A US 3270118A
Authority
US
United States
Prior art keywords
electron beam
melt
mold
rod
melted
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US293355A
Inventor
Gaydou Francois
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bendix Balzers Vacuum Inc
Original Assignee
Bendix Balzers Vacuum Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bendix Balzers Vacuum Inc filed Critical Bendix Balzers Vacuum Inc
Application granted granted Critical
Publication of US3270118A publication Critical patent/US3270118A/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/30Electron-beam or ion-beam tubes for localised treatment of objects
    • H01J37/305Electron-beam or ion-beam tubes for localised treatment of objects for casting, melting, evaporating, or etching
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B9/00General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
    • C22B9/04Refining by applying a vacuum
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B9/00General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
    • C22B9/16Remelting metals
    • C22B9/22Remelting metals with heating by wave energy or particle radiation
    • C22B9/228Remelting metals with heating by wave energy or particle radiation by particle radiation, e.g. electron beams

Definitions

  • the present invention relates generally to processes for the vacuum melting of metals by means of electron beams.
  • the metal to be melted in a rod shaped piece combined with an electron beam directed onto the rod can be used for continuous melting and the melted drops are caught in a mold. Without further precautions the dropping metal solidifies immediately in the mold and an ingot with nonuniform density and great stratification is produced. This can be minimized if during the melting the mold is kept hot at least on the upper surface so that a continuous fluid mass can be formed while the mold is tilled in the course of the melting gradually solidifying from the bottom up.
  • the keeping the mold hot can be done by the use of an induction heating coil wrapped around it or by bombarding the upper surface of the melt with an electron beam from an additional electron gun.
  • These well known processes have the disadvantage of a relatively large additional expenditure for either a high frequency generator for supplying the induction heating or for the additional electron gun.
  • the object of the invention will be to propose a new process for the vacuum melting of metals by means of electron beams, which eliminates these difiiculties, by which the metal is to be melted from a solid, preferably rod formed piece, and falls dropwise into a mold, which is further characterized by the fact that the one and the same electron beam being deflectable by well known means is used to melt from the solid metal piece and also to keep the melt hot in the mold. It is alternately directed onto the metal piece to be melted from and onto the upper surface of the melt in the mold.
  • Numeral 4 indicates the vacuum connection
  • 5 shows a holder and feed arrangement, for a melt rod of the metal to be melted away, flanged to the furnace housing.
  • the electron beam generator is essentially composed of the cathode part 7 and an electron optical system with electron lenses and deflectors 8, 9 and 10 well known in the art which focus the electrons coming from 3,2 70,1 18 Patented August 30, 1966 the cathode into a beam 11.
  • the chamber 12 of the electron beam generator is separated from the furnace space by a diaphragm '13 with a small diaphragm opening therein and is evacuated by a separate pump through the connection 14. This makes it possible to hold a better vacuum in 12 than in the furnace space.
  • the beam 11 produced by the electron beam generator passes through the existing means for deflection, is directed according to choice onto the forward end 15 of the melt rod 6 or onto the upper surface '16 of the melt in the mold, during which, by means of a prearranged suitable duty cycle according to a program defined from the metallurgical point of view, for example by carrying out calculations on the stronger cooling in the neighborhood of the mold wall, the different zones of the melt surface and the rod to be melted off can be swept over with different rates and intensities, for example, it can be guided in circular paths over the melt surface or definite areas of the rod to be melted off can be heated stronger than the others.
  • a focused electron beam is especially adapted to this purpose.
  • the invention proposes further that the distribution of the total available performance of the electron beam be in proportion to the times of duration during which the beam is directed on the melt rod and on the melt surface.
  • the process that is the object of this invention provides great advantages. It is simple and more economical, since only one electron beam generator must be used, which naturally is increased in capacity to give an adequate performance, than a greater number of electron guns, which must be supplied and controlled separately.
  • the process of alternating bombardment of the single spot to be heated through a deflected electron beam is also easier to handle than the above mentioned already known proposal, with one electron beam directed onto the surface of the molten pool in the mold and which strikes the rod to be melted at the same time, melting it.
  • the metal melted ofi of the melt rod will be solidified without gradation in the center 6 of the melt pool and also, that the delay time of the fluid materials on the surface of the rod to be melted will be optimal for the needs of degassing.
  • the invention refers further to an electron beam melting furnace for the carrying out of the novel process.
  • One such furnace which, as described, shows a mold and attachments and a feed arrangement for a laterally arranged rod of the metal to be melted as well as an electron beam generator, is characterized by the fact that well known means for the deflection, at will, of the electron beam is provided on the one hand onto the end of the melt rod situated over the mold and on the other hand onto the upper surface of the molten pool in the mold.
  • a method for the vacuum melting of metals with an electron beam wherein the melt stock is drip melted into a mold which is disposed below the melt stock comprising the steps of:

Landscapes

  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Manufacturing & Machinery (AREA)
  • Physics & Mathematics (AREA)
  • Plasma & Fusion (AREA)
  • Analytical Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Description

Aug. 30, 1966 F. GAYDOU 3,270,118
PROCESS FOR THE VACUUM MELTING OF METALS BY MEANS OF ELECTRON BEAM Filed July 8, 1963 United States Patent 3,270,118 PROCESS FOR THE VACUUM MELTING 0F METALS BY MEANS OF ELECTRON BEAM Francois Gaydou, Balzers, Liechtenstein, assignor to Bendix Balzers Vacuum Inc., Rochester, N.Y., a corporation of Delaware Filed July 8, 1963, Ser. No. 293,355 Claims priority, application Austria, July 10, 1962, A 5,541/ 62 1 Claim. (CI. 13-34) The present invention relates generally to processes for the vacuum melting of metals by means of electron beams. It is well known that the metal to be melted in a rod shaped piece combined with an electron beam directed onto the rod can be used for continuous melting and the melted drops are caught in a mold. Without further precautions the dropping metal solidifies immediately in the mold and an ingot with nonuniform density and great stratification is produced. This can be minimized if during the melting the mold is kept hot at least on the upper surface so that a continuous fluid mass can be formed while the mold is tilled in the course of the melting gradually solidifying from the bottom up.
The keeping the mold hot can be done by the use of an induction heating coil wrapped around it or by bombarding the upper surface of the melt with an electron beam from an additional electron gun. These well known processes have the disadvantage of a relatively large additional expenditure for either a high frequency generator for supplying the induction heating or for the additional electron gun.
It has also already been proposed to permit the forward part of the electron beam directed onto the upper surface of the melt to wander at the same time over the end of the rod to be melted, located over the mold, in order to slowly melt it. This method has the decided disadvantage that a shadowing of a part of the beam by the rod to be melted is inevitable and therefore the upper surface of the molten pool will be unequally heated. Moreover the effects to be carried out on the surface of the molten pool and on the rod to be melted cannot be controlled independently of one another.
The object of the invention will be to propose a new process for the vacuum melting of metals by means of electron beams, which eliminates these difiiculties, by which the metal is to be melted from a solid, preferably rod formed piece, and falls dropwise into a mold, which is further characterized by the fact that the one and the same electron beam being deflectable by well known means is used to melt from the solid metal piece and also to keep the melt hot in the mold. It is alternately directed onto the metal piece to be melted from and onto the upper surface of the melt in the mold.
How the process according to the invention can be materialized by way of example and what special advantages it offers will be described in the following detailed descrip tion taken in connection with the accompanying drawing in which the single figure shows an electron beam melting furnace with the following parts:
Furnace housing 1 to which an electron beam generator 2 above and a water cooled mold 3 below can be flanged vacuum tight. Numeral 4 indicates the vacuum connection, 5 shows a holder and feed arrangement, for a melt rod of the metal to be melted away, flanged to the furnace housing. The electron beam generator is essentially composed of the cathode part 7 and an electron optical system with electron lenses and deflectors 8, 9 and 10 well known in the art which focus the electrons coming from 3,2 70,1 18 Patented August 30, 1966 the cathode into a beam 11. The chamber 12 of the electron beam generator is separated from the furnace space by a diaphragm '13 with a small diaphragm opening therein and is evacuated by a separate pump through the connection 14. This makes it possible to hold a better vacuum in 12 than in the furnace space.
The beam 11 produced by the electron beam generator passes through the existing means for deflection, is directed according to choice onto the forward end 15 of the melt rod 6 or onto the upper surface '16 of the melt in the mold, during which, by means of a prearranged suitable duty cycle according to a program defined from the metallurgical point of view, for example by carrying out calculations on the stronger cooling in the neighborhood of the mold wall, the different zones of the melt surface and the rod to be melted off can be swept over with different rates and intensities, for example, it can be guided in circular paths over the melt surface or definite areas of the rod to be melted off can be heated stronger than the others. A focused electron beam is especially adapted to this purpose. The invention proposes further that the distribution of the total available performance of the electron beam be in proportion to the times of duration during which the beam is directed on the melt rod and on the melt surface.
The arrangements which are necessary to operate the electron beam generator or to achieve the feed of the melt rod or for its rotation during the melting off or means for tilting a mold with a spout will not be more precisely described here because they are well known.
The process that is the object of this invention provides great advantages. It is simple and more economical, since only one electron beam generator must be used, which naturally is increased in capacity to give an adequate performance, than a greater number of electron guns, which must be supplied and controlled separately. The process of alternating bombardment of the single spot to be heated through a deflected electron beam is also easier to handle than the above mentioned already known proposal, with one electron beam directed onto the surface of the molten pool in the mold and which strikes the rod to be melted at the same time, melting it.
By the melting off method according to the invention the metal melted ofi of the melt rod will be solidified without gradation in the center 6 of the melt pool and also, that the delay time of the fluid materials on the surface of the rod to be melted will be optimal for the needs of degassing.
The invention refers further to an electron beam melting furnace for the carrying out of the novel process. One such furnace, which, as described, shows a mold and attachments and a feed arrangement for a laterally arranged rod of the metal to be melted as well as an electron beam generator, is characterized by the fact that well known means for the deflection, at will, of the electron beam is provided on the one hand onto the end of the melt rod situated over the mold and on the other hand onto the upper surface of the molten pool in the mold.
I claim:
A method for the vacuum melting of metals with an electron beam wherein the melt stock is drip melted into a mold which is disposed below the melt stock comprising the steps of:
axially aligning and focusing the electron beam on the melt in said mold adjacent the radial outward edge thereof and radially spaced from the end of the melt stock,
3 4 deflecting said beam to scan the surface of the melt in 3,068,309 12/ 1962 Hanks 1331 said mold for a controlled time duration, 3,105,275 10/ 1963 Hanks. alternately deflecting said focused beam to strike the FOREIGN PATENTS melt stock for a controlled time duration whereby the respective quantities of heat supplied to the melt 5 1,274,810 9/1961 Francestock and to the melt in the mold are controlled by 1334547 7/1963 Franceregula-ting the first and second mentioned time dura- 1,100,835 3/1961 Germany;
' 972,908 10/1964 Great Brltain.
tions.
References Cited by the Examiner BARTIS, Acting Primary Examiner.
UNITED STATES PATENTS RICHARD M. WOOD, Examiner. 3 005 359 10/196 1 Candidus 1 V. YJMAYEWSKY, Assistant Examiner.
3,040,112 6/ 1962 Smith 1331
US293355A 1962-07-10 1963-07-08 Process for the vacuum melting of metals by means of electron beam Expired - Lifetime US3270118A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
AT554162 1962-07-10

Publications (1)

Publication Number Publication Date
US3270118A true US3270118A (en) 1966-08-30

Family

ID=3576907

Family Applications (1)

Application Number Title Priority Date Filing Date
US293355A Expired - Lifetime US3270118A (en) 1962-07-10 1963-07-08 Process for the vacuum melting of metals by means of electron beam

Country Status (1)

Country Link
US (1) US3270118A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3390222A (en) * 1965-08-17 1968-06-25 Air Reduction Electron beam apparatus with variable orientation of transverse deflecting field
US3409729A (en) * 1966-12-16 1968-11-05 Air Reduction Electron beam furnace and method for heating a target therein
US5064989A (en) * 1957-06-27 1991-11-12 Lemelson Jerome H Surface shaping and finishing apparatus and method
US5263044A (en) * 1989-09-05 1993-11-16 Bremer Siegfried M K Remelting method for recognition and recovery of noble metals and rare metals

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1100835B (en) * 1952-03-01 1961-03-02 Zeiss Carl Fa Device for milling profiles, for cutting templates or for drilling nozzle channels by means of a charge carrier beam
US3005859A (en) * 1958-04-24 1961-10-24 Nat Res Corp Production of metals
FR1274810A (en) * 1960-07-12 1961-10-27 Vakutronik Veb Furnace focusing and deflecting an electron beam
US3040112A (en) * 1960-06-03 1962-06-19 Stauffer Chemical Co Electron-beam furnace with beam emission suppressors
US3068309A (en) * 1960-06-22 1962-12-11 Stauffer Chemical Co Electron beam furnace with multiple field guidance of electrons
FR1334547A (en) * 1962-06-29 1963-08-09 Alsacienne D Electronique Et D Improvements in electron bombardment fusion
US3105275A (en) * 1960-05-27 1963-10-01 Stauffer Chemical Co Electron-beam furnace with double-coil magnetic beam guidance
GB972908A (en) * 1962-07-20 1964-10-21 Balzers Patent Beteilig Ag Improvements in and relating to the zone-wise melting of metals and of semi-conductors

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1100835B (en) * 1952-03-01 1961-03-02 Zeiss Carl Fa Device for milling profiles, for cutting templates or for drilling nozzle channels by means of a charge carrier beam
US3005859A (en) * 1958-04-24 1961-10-24 Nat Res Corp Production of metals
US3105275A (en) * 1960-05-27 1963-10-01 Stauffer Chemical Co Electron-beam furnace with double-coil magnetic beam guidance
US3040112A (en) * 1960-06-03 1962-06-19 Stauffer Chemical Co Electron-beam furnace with beam emission suppressors
US3068309A (en) * 1960-06-22 1962-12-11 Stauffer Chemical Co Electron beam furnace with multiple field guidance of electrons
FR1274810A (en) * 1960-07-12 1961-10-27 Vakutronik Veb Furnace focusing and deflecting an electron beam
FR1334547A (en) * 1962-06-29 1963-08-09 Alsacienne D Electronique Et D Improvements in electron bombardment fusion
GB972908A (en) * 1962-07-20 1964-10-21 Balzers Patent Beteilig Ag Improvements in and relating to the zone-wise melting of metals and of semi-conductors

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5064989A (en) * 1957-06-27 1991-11-12 Lemelson Jerome H Surface shaping and finishing apparatus and method
US3390222A (en) * 1965-08-17 1968-06-25 Air Reduction Electron beam apparatus with variable orientation of transverse deflecting field
US3409729A (en) * 1966-12-16 1968-11-05 Air Reduction Electron beam furnace and method for heating a target therein
US5263044A (en) * 1989-09-05 1993-11-16 Bremer Siegfried M K Remelting method for recognition and recovery of noble metals and rare metals

Similar Documents

Publication Publication Date Title
JP5781710B2 (en) Method for producing a processing material which is cast or sprayed into a powder
NO148062B (en) PROCEDURE FOR THE PREPARATION OF THERMOPLAST LAMINATED STRENGTH FILM.
US2423729A (en) Vaporization of substances in a vacuum
US3896258A (en) Electron beam gun system
US3219435A (en) Method and apparatus for producing metal blocks by electron beams
US3068309A (en) Electron beam furnace with multiple field guidance of electrons
JP2013503259A (en) Ion plasma electron emitter for melting furnace
GB959367A (en) High vacuum furnace
JPS5810989B2 (en) Target profile for sputtering equipment
US3235647A (en) Electron bombardment heating with adjustable impact pattern
US3226223A (en) Method and apparatus for melting metals by inductive heating and electron bombardment
US3607222A (en) Method for evaporating alloy
US3270118A (en) Process for the vacuum melting of metals by means of electron beam
US3177535A (en) Electron beam furnace with low beam source
US3101515A (en) Electron beam furnace with magnetically guided axial and transverse beams
US3303320A (en) Vapor-coating apparatus
CN216585179U (en) Crucible system of vacuum evaporation machine
US2981823A (en) Production of metals
US3265801A (en) Electron beam furnaces
US6391164B1 (en) Deposition of coatings and thin films using a vacuum arc with a non-consumable hot anode
US3267529A (en) Apparatus for melting metals under high vacuum
US3183077A (en) Process for vacuum degassing
US4153005A (en) Multiple electron beam vacuum vapor deposition apparatus
US3040112A (en) Electron-beam furnace with beam emission suppressors
NO153507B (en) FIREOWS FOR ROTATION PROJECTIL.