US3270118A - Process for the vacuum melting of metals by means of electron beam - Google Patents
Process for the vacuum melting of metals by means of electron beam Download PDFInfo
- Publication number
- US3270118A US3270118A US293355A US29335563A US3270118A US 3270118 A US3270118 A US 3270118A US 293355 A US293355 A US 293355A US 29335563 A US29335563 A US 29335563A US 3270118 A US3270118 A US 3270118A
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- Prior art keywords
- electron beam
- melt
- mold
- rod
- melted
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- Expired - Lifetime
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- 238000010894 electron beam technology Methods 0.000 title description 25
- 238000002844 melting Methods 0.000 title description 14
- 230000008018 melting Effects 0.000 title description 14
- 239000002184 metal Substances 0.000 title description 14
- 229910052751 metal Inorganic materials 0.000 title description 14
- 238000000034 method Methods 0.000 title description 13
- 150000002739 metals Chemical class 0.000 title description 6
- 239000000155 melt Substances 0.000 description 22
- 239000012530 fluid Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 230000006698 induction Effects 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 240000005369 Alstonia scholaris Species 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000007872 degassing Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 238000013517 stratification Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/30—Electron-beam or ion-beam tubes for localised treatment of objects
- H01J37/305—Electron-beam or ion-beam tubes for localised treatment of objects for casting, melting, evaporating, or etching
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B9/00—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
- C22B9/04—Refining by applying a vacuum
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B9/00—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
- C22B9/16—Remelting metals
- C22B9/22—Remelting metals with heating by wave energy or particle radiation
- C22B9/228—Remelting metals with heating by wave energy or particle radiation by particle radiation, e.g. electron beams
Definitions
- the present invention relates generally to processes for the vacuum melting of metals by means of electron beams.
- the metal to be melted in a rod shaped piece combined with an electron beam directed onto the rod can be used for continuous melting and the melted drops are caught in a mold. Without further precautions the dropping metal solidifies immediately in the mold and an ingot with nonuniform density and great stratification is produced. This can be minimized if during the melting the mold is kept hot at least on the upper surface so that a continuous fluid mass can be formed while the mold is tilled in the course of the melting gradually solidifying from the bottom up.
- the keeping the mold hot can be done by the use of an induction heating coil wrapped around it or by bombarding the upper surface of the melt with an electron beam from an additional electron gun.
- These well known processes have the disadvantage of a relatively large additional expenditure for either a high frequency generator for supplying the induction heating or for the additional electron gun.
- the object of the invention will be to propose a new process for the vacuum melting of metals by means of electron beams, which eliminates these difiiculties, by which the metal is to be melted from a solid, preferably rod formed piece, and falls dropwise into a mold, which is further characterized by the fact that the one and the same electron beam being deflectable by well known means is used to melt from the solid metal piece and also to keep the melt hot in the mold. It is alternately directed onto the metal piece to be melted from and onto the upper surface of the melt in the mold.
- Numeral 4 indicates the vacuum connection
- 5 shows a holder and feed arrangement, for a melt rod of the metal to be melted away, flanged to the furnace housing.
- the electron beam generator is essentially composed of the cathode part 7 and an electron optical system with electron lenses and deflectors 8, 9 and 10 well known in the art which focus the electrons coming from 3,2 70,1 18 Patented August 30, 1966 the cathode into a beam 11.
- the chamber 12 of the electron beam generator is separated from the furnace space by a diaphragm '13 with a small diaphragm opening therein and is evacuated by a separate pump through the connection 14. This makes it possible to hold a better vacuum in 12 than in the furnace space.
- the beam 11 produced by the electron beam generator passes through the existing means for deflection, is directed according to choice onto the forward end 15 of the melt rod 6 or onto the upper surface '16 of the melt in the mold, during which, by means of a prearranged suitable duty cycle according to a program defined from the metallurgical point of view, for example by carrying out calculations on the stronger cooling in the neighborhood of the mold wall, the different zones of the melt surface and the rod to be melted off can be swept over with different rates and intensities, for example, it can be guided in circular paths over the melt surface or definite areas of the rod to be melted off can be heated stronger than the others.
- a focused electron beam is especially adapted to this purpose.
- the invention proposes further that the distribution of the total available performance of the electron beam be in proportion to the times of duration during which the beam is directed on the melt rod and on the melt surface.
- the process that is the object of this invention provides great advantages. It is simple and more economical, since only one electron beam generator must be used, which naturally is increased in capacity to give an adequate performance, than a greater number of electron guns, which must be supplied and controlled separately.
- the process of alternating bombardment of the single spot to be heated through a deflected electron beam is also easier to handle than the above mentioned already known proposal, with one electron beam directed onto the surface of the molten pool in the mold and which strikes the rod to be melted at the same time, melting it.
- the metal melted ofi of the melt rod will be solidified without gradation in the center 6 of the melt pool and also, that the delay time of the fluid materials on the surface of the rod to be melted will be optimal for the needs of degassing.
- the invention refers further to an electron beam melting furnace for the carrying out of the novel process.
- One such furnace which, as described, shows a mold and attachments and a feed arrangement for a laterally arranged rod of the metal to be melted as well as an electron beam generator, is characterized by the fact that well known means for the deflection, at will, of the electron beam is provided on the one hand onto the end of the melt rod situated over the mold and on the other hand onto the upper surface of the molten pool in the mold.
- a method for the vacuum melting of metals with an electron beam wherein the melt stock is drip melted into a mold which is disposed below the melt stock comprising the steps of:
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- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Manufacturing & Machinery (AREA)
- Physics & Mathematics (AREA)
- Plasma & Fusion (AREA)
- Analytical Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Manufacture And Refinement Of Metals (AREA)
Description
Aug. 30, 1966 F. GAYDOU 3,270,118
PROCESS FOR THE VACUUM MELTING OF METALS BY MEANS OF ELECTRON BEAM Filed July 8, 1963 United States Patent 3,270,118 PROCESS FOR THE VACUUM MELTING 0F METALS BY MEANS OF ELECTRON BEAM Francois Gaydou, Balzers, Liechtenstein, assignor to Bendix Balzers Vacuum Inc., Rochester, N.Y., a corporation of Delaware Filed July 8, 1963, Ser. No. 293,355 Claims priority, application Austria, July 10, 1962, A 5,541/ 62 1 Claim. (CI. 13-34) The present invention relates generally to processes for the vacuum melting of metals by means of electron beams. It is well known that the metal to be melted in a rod shaped piece combined with an electron beam directed onto the rod can be used for continuous melting and the melted drops are caught in a mold. Without further precautions the dropping metal solidifies immediately in the mold and an ingot with nonuniform density and great stratification is produced. This can be minimized if during the melting the mold is kept hot at least on the upper surface so that a continuous fluid mass can be formed while the mold is tilled in the course of the melting gradually solidifying from the bottom up.
The keeping the mold hot can be done by the use of an induction heating coil wrapped around it or by bombarding the upper surface of the melt with an electron beam from an additional electron gun. These well known processes have the disadvantage of a relatively large additional expenditure for either a high frequency generator for supplying the induction heating or for the additional electron gun.
It has also already been proposed to permit the forward part of the electron beam directed onto the upper surface of the melt to wander at the same time over the end of the rod to be melted, located over the mold, in order to slowly melt it. This method has the decided disadvantage that a shadowing of a part of the beam by the rod to be melted is inevitable and therefore the upper surface of the molten pool will be unequally heated. Moreover the effects to be carried out on the surface of the molten pool and on the rod to be melted cannot be controlled independently of one another.
The object of the invention will be to propose a new process for the vacuum melting of metals by means of electron beams, which eliminates these difiiculties, by which the metal is to be melted from a solid, preferably rod formed piece, and falls dropwise into a mold, which is further characterized by the fact that the one and the same electron beam being deflectable by well known means is used to melt from the solid metal piece and also to keep the melt hot in the mold. It is alternately directed onto the metal piece to be melted from and onto the upper surface of the melt in the mold.
How the process according to the invention can be materialized by way of example and what special advantages it offers will be described in the following detailed descrip tion taken in connection with the accompanying drawing in which the single figure shows an electron beam melting furnace with the following parts:
Furnace housing 1 to which an electron beam generator 2 above and a water cooled mold 3 below can be flanged vacuum tight. Numeral 4 indicates the vacuum connection, 5 shows a holder and feed arrangement, for a melt rod of the metal to be melted away, flanged to the furnace housing. The electron beam generator is essentially composed of the cathode part 7 and an electron optical system with electron lenses and deflectors 8, 9 and 10 well known in the art which focus the electrons coming from 3,2 70,1 18 Patented August 30, 1966 the cathode into a beam 11. The chamber 12 of the electron beam generator is separated from the furnace space by a diaphragm '13 with a small diaphragm opening therein and is evacuated by a separate pump through the connection 14. This makes it possible to hold a better vacuum in 12 than in the furnace space.
The beam 11 produced by the electron beam generator passes through the existing means for deflection, is directed according to choice onto the forward end 15 of the melt rod 6 or onto the upper surface '16 of the melt in the mold, during which, by means of a prearranged suitable duty cycle according to a program defined from the metallurgical point of view, for example by carrying out calculations on the stronger cooling in the neighborhood of the mold wall, the different zones of the melt surface and the rod to be melted off can be swept over with different rates and intensities, for example, it can be guided in circular paths over the melt surface or definite areas of the rod to be melted off can be heated stronger than the others. A focused electron beam is especially adapted to this purpose. The invention proposes further that the distribution of the total available performance of the electron beam be in proportion to the times of duration during which the beam is directed on the melt rod and on the melt surface.
The arrangements which are necessary to operate the electron beam generator or to achieve the feed of the melt rod or for its rotation during the melting off or means for tilting a mold with a spout will not be more precisely described here because they are well known.
The process that is the object of this invention provides great advantages. It is simple and more economical, since only one electron beam generator must be used, which naturally is increased in capacity to give an adequate performance, than a greater number of electron guns, which must be supplied and controlled separately. The process of alternating bombardment of the single spot to be heated through a deflected electron beam is also easier to handle than the above mentioned already known proposal, with one electron beam directed onto the surface of the molten pool in the mold and which strikes the rod to be melted at the same time, melting it.
By the melting off method according to the invention the metal melted ofi of the melt rod will be solidified without gradation in the center 6 of the melt pool and also, that the delay time of the fluid materials on the surface of the rod to be melted will be optimal for the needs of degassing.
The invention refers further to an electron beam melting furnace for the carrying out of the novel process. One such furnace, which, as described, shows a mold and attachments and a feed arrangement for a laterally arranged rod of the metal to be melted as well as an electron beam generator, is characterized by the fact that well known means for the deflection, at will, of the electron beam is provided on the one hand onto the end of the melt rod situated over the mold and on the other hand onto the upper surface of the molten pool in the mold.
I claim:
A method for the vacuum melting of metals with an electron beam wherein the melt stock is drip melted into a mold which is disposed below the melt stock comprising the steps of:
axially aligning and focusing the electron beam on the melt in said mold adjacent the radial outward edge thereof and radially spaced from the end of the melt stock,
3 4 deflecting said beam to scan the surface of the melt in 3,068,309 12/ 1962 Hanks 1331 said mold for a controlled time duration, 3,105,275 10/ 1963 Hanks. alternately deflecting said focused beam to strike the FOREIGN PATENTS melt stock for a controlled time duration whereby the respective quantities of heat supplied to the melt 5 1,274,810 9/1961 Francestock and to the melt in the mold are controlled by 1334547 7/1963 Franceregula-ting the first and second mentioned time dura- 1,100,835 3/1961 Germany;
' 972,908 10/1964 Great Brltain.
tions.
References Cited by the Examiner BARTIS, Acting Primary Examiner.
UNITED STATES PATENTS RICHARD M. WOOD, Examiner. 3 005 359 10/196 1 Candidus 1 V. YJMAYEWSKY, Assistant Examiner.
3,040,112 6/ 1962 Smith 1331
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
AT554162 | 1962-07-10 |
Publications (1)
Publication Number | Publication Date |
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US3270118A true US3270118A (en) | 1966-08-30 |
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US293355A Expired - Lifetime US3270118A (en) | 1962-07-10 | 1963-07-08 | Process for the vacuum melting of metals by means of electron beam |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3390222A (en) * | 1965-08-17 | 1968-06-25 | Air Reduction | Electron beam apparatus with variable orientation of transverse deflecting field |
US3409729A (en) * | 1966-12-16 | 1968-11-05 | Air Reduction | Electron beam furnace and method for heating a target therein |
US5064989A (en) * | 1957-06-27 | 1991-11-12 | Lemelson Jerome H | Surface shaping and finishing apparatus and method |
US5263044A (en) * | 1989-09-05 | 1993-11-16 | Bremer Siegfried M K | Remelting method for recognition and recovery of noble metals and rare metals |
Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1100835B (en) * | 1952-03-01 | 1961-03-02 | Zeiss Carl Fa | Device for milling profiles, for cutting templates or for drilling nozzle channels by means of a charge carrier beam |
US3005859A (en) * | 1958-04-24 | 1961-10-24 | Nat Res Corp | Production of metals |
FR1274810A (en) * | 1960-07-12 | 1961-10-27 | Vakutronik Veb | Furnace focusing and deflecting an electron beam |
US3040112A (en) * | 1960-06-03 | 1962-06-19 | Stauffer Chemical Co | Electron-beam furnace with beam emission suppressors |
US3068309A (en) * | 1960-06-22 | 1962-12-11 | Stauffer Chemical Co | Electron beam furnace with multiple field guidance of electrons |
FR1334547A (en) * | 1962-06-29 | 1963-08-09 | Alsacienne D Electronique Et D | Improvements in electron bombardment fusion |
US3105275A (en) * | 1960-05-27 | 1963-10-01 | Stauffer Chemical Co | Electron-beam furnace with double-coil magnetic beam guidance |
GB972908A (en) * | 1962-07-20 | 1964-10-21 | Balzers Patent Beteilig Ag | Improvements in and relating to the zone-wise melting of metals and of semi-conductors |
-
1963
- 1963-07-08 US US293355A patent/US3270118A/en not_active Expired - Lifetime
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1100835B (en) * | 1952-03-01 | 1961-03-02 | Zeiss Carl Fa | Device for milling profiles, for cutting templates or for drilling nozzle channels by means of a charge carrier beam |
US3005859A (en) * | 1958-04-24 | 1961-10-24 | Nat Res Corp | Production of metals |
US3105275A (en) * | 1960-05-27 | 1963-10-01 | Stauffer Chemical Co | Electron-beam furnace with double-coil magnetic beam guidance |
US3040112A (en) * | 1960-06-03 | 1962-06-19 | Stauffer Chemical Co | Electron-beam furnace with beam emission suppressors |
US3068309A (en) * | 1960-06-22 | 1962-12-11 | Stauffer Chemical Co | Electron beam furnace with multiple field guidance of electrons |
FR1274810A (en) * | 1960-07-12 | 1961-10-27 | Vakutronik Veb | Furnace focusing and deflecting an electron beam |
FR1334547A (en) * | 1962-06-29 | 1963-08-09 | Alsacienne D Electronique Et D | Improvements in electron bombardment fusion |
GB972908A (en) * | 1962-07-20 | 1964-10-21 | Balzers Patent Beteilig Ag | Improvements in and relating to the zone-wise melting of metals and of semi-conductors |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5064989A (en) * | 1957-06-27 | 1991-11-12 | Lemelson Jerome H | Surface shaping and finishing apparatus and method |
US3390222A (en) * | 1965-08-17 | 1968-06-25 | Air Reduction | Electron beam apparatus with variable orientation of transverse deflecting field |
US3409729A (en) * | 1966-12-16 | 1968-11-05 | Air Reduction | Electron beam furnace and method for heating a target therein |
US5263044A (en) * | 1989-09-05 | 1993-11-16 | Bremer Siegfried M K | Remelting method for recognition and recovery of noble metals and rare metals |
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