US320821A - Half to henby w - Google Patents
Half to henby w Download PDFInfo
- Publication number
- US320821A US320821A US320821DA US320821A US 320821 A US320821 A US 320821A US 320821D A US320821D A US 320821DA US 320821 A US320821 A US 320821A
- Authority
- US
- United States
- Prior art keywords
- solution
- mordant
- baum
- chromium
- pints
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- MUBZPKHOEPUJKR-UHFFFAOYSA-N oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 12
- HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 12
- VYZAMTAEIAYCRO-UHFFFAOYSA-N chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 8
- 229910052804 chromium Inorganic materials 0.000 description 8
- 239000011651 chromium Substances 0.000 description 8
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 6
- 238000009835 boiling Methods 0.000 description 6
- 239000004744 fabric Substances 0.000 description 6
- 239000000203 mixture Substances 0.000 description 6
- FGIUAXJPYTZDNR-UHFFFAOYSA-N Potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 4
- 239000003086 colorant Substances 0.000 description 4
- 238000004043 dyeing Methods 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- 235000011121 sodium hydroxide Nutrition 0.000 description 4
- 229920000742 Cotton Polymers 0.000 description 2
- KMUONIBRACKNSN-UHFFFAOYSA-N Potassium dichromate Chemical compound [K+].[K+].[O-][Cr](=O)(=O)O[Cr]([O-])(=O)=O KMUONIBRACKNSN-UHFFFAOYSA-N 0.000 description 2
- 229910000423 chromium oxide Inorganic materials 0.000 description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- 235000011187 glycerol Nutrition 0.000 description 2
- GRYLNZFGIOXLOG-UHFFFAOYSA-N nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 2
- 235000006408 oxalic acid Nutrition 0.000 description 2
- 235000010333 potassium nitrate Nutrition 0.000 description 2
- WGLPBDUCMAPZCE-UHFFFAOYSA-N trioxochromium Chemical compound O=[Cr](=O)=O WGLPBDUCMAPZCE-UHFFFAOYSA-N 0.000 description 2
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/653—Nitrogen-free carboxylic acids or their salts
- D06P1/6533—Aliphatic, araliphatic or cycloaliphatic
Definitions
- My invention is an improved mordant of a character to deposit chromium oxide upon cotton and other fabrics in order to adapt the same to be dyed fast-colors by the use of aniline dyes.
- I use 0xalate 'of chromium, which I prepare in the following manner: I first dissolve sixty-six pounds of bichromate of potash in ninetythree pints of boiling Water, and add to the solution fifty-five pints of nitric acid of a strength of 36 Baum. I then prepare a second solution of twenty-nine pounds of oxalic acid in sixty pints of water, and add sixteen pints of glycerine of a strength of 28 Baum.
- the mordant mixture thus produced eonstitutes a salable preparation.
- the mordant is to be used for mordanting fabrics, a portion thereof is diluted 0 with double its volume of cold water, and the goods,after being soaked in boiling water,are soaked in the mordant-liquor for ten hours, and then removed, thoroughly washed, and dyed in the ordinary manner.
- I claim- A mordant for preparing fabrics for dyeing with aniline dyes, consisting of a mixture of a solution of oxalate of chromium and a solution of caustic soda, substantially as described.
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Coloring (AREA)
Description
UNITED STATES PATENT OFFICE RUDOLF SILBERBERG, OF JERSEY CITY, NEW JERSEY, ASSIGNOR OF ONE- HALF TO HENRY W. HOOPS, JR, OF SAME PLACE.
MO RDANT.
SPECIFICATION forming part of Letters Patent No. 320,821, dated June 23, 1885. Application filed May 8, 1885. (No specimens.) Patented in Canada April 20, 1885, No. 21,458.
To all whom it may concern.-
Be it known that I, RUDoLE SILBERBERG, a citizen of the United States, residing at J ersey City, in the county of Hudson and State of New Jersey, have invented certain new and useful Improvements in Mordants, of which the following is a specification.
My invention is an improved mordant of a character to deposit chromium oxide upon cotton and other fabrics in order to adapt the same to be dyed fast-colors by the use of aniline dyes.
In the preparation of my mordant I use 0xalate 'of chromium, which I prepare in the following manner: I first dissolve sixty-six pounds of bichromate of potash in ninetythree pints of boiling Water, and add to the solution fifty-five pints of nitric acid of a strength of 36 Baum. I then prepare a second solution of twenty-nine pounds of oxalic acid in sixty pints of water, and add sixteen pints of glycerine of a strength of 28 Baum. The two solutions are added together and boiled until a diluted solution appears of a clear green color, after which the solution is allowed to stand until nitrate of potash is deposited as crystals, when the oxalate of chromium will be in solution in the liquor of a strength of to 88 Baum.
In making the mordant I take twenty quarts of the abovementioned liquor diluted with water to 8 Baum, and mix therewith seventeen and a half quarts of a solution of caustic soda of a strength of 20 Baum, and after the two are well mixed I add five quarts of 5 water.
The mordant mixture thus produced eonstitutes a salable preparation.
\Vhen the mordant is to be used for mordanting fabrics, a portion thereof is diluted 0 with double its volume of cold water, and the goods,after being soaked in boiling water,are soaked in the mordant-liquor for ten hours, and then removed, thoroughly washed, and dyed in the ordinary manner.
I do not here claim the mode of making an oxalate of chromium or the mode of dyeing aniline colors therewith, as the same constitutes the subject of separate applications for Letters Patent Nos. 160,074 and 160,075.
I claim- A mordant for preparing fabrics for dyeing with aniline dyes, consisting of a mixture of a solution of oxalate of chromium and a solution of caustic soda, substantially as described.
I11 testimony whereof I have signed my name to this specification in the presence of two subscribing witnesses.
RUDOLF SILBERBERG.
Witnesses:
FRANK J. MATnEws, HENRY W. HOOPS, Jr.
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US320821A true US320821A (en) | 1885-06-23 |
Family
ID=2389962
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US320821D Expired - Lifetime US320821A (en) | Half to henby w |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US320821A (en) |
-
0
- US US320821D patent/US320821A/en not_active Expired - Lifetime
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