US6242A - Improvement in dyeing - Google Patents
Improvement in dyeing Download PDFInfo
- Publication number
- US6242A US6242A US6242DA US6242A US 6242 A US6242 A US 6242A US 6242D A US6242D A US 6242DA US 6242 A US6242 A US 6242A
- Authority
- US
- United States
- Prior art keywords
- dyeing
- goods
- dye
- potash
- soda
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000004043 dyeing Methods 0.000 title description 8
- FGIUAXJPYTZDNR-UHFFFAOYSA-N Potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 12
- 239000000975 dye Substances 0.000 description 12
- 239000004744 fabric Substances 0.000 description 12
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 10
- 239000003086 colorant Substances 0.000 description 10
- 235000011149 sulphuric acid Nutrition 0.000 description 10
- 239000001117 sulphuric acid Substances 0.000 description 10
- BVKZGUZCCUSVTD-UHFFFAOYSA-N Carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 8
- 210000002268 Wool Anatomy 0.000 description 8
- 239000000463 material Substances 0.000 description 6
- 229940072033 potash Drugs 0.000 description 6
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 6
- 235000015320 potassium carbonate Nutrition 0.000 description 6
- KWYUFKZDYYNOTN-UHFFFAOYSA-M potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 6
- 235000010333 potassium nitrate Nutrition 0.000 description 6
- 150000003839 salts Chemical class 0.000 description 6
- 239000011780 sodium chloride Substances 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 235000002687 Caesalpinia echinata Nutrition 0.000 description 4
- 229920000742 Cotton Polymers 0.000 description 4
- 241001424361 Haematoxylum brasiletto Species 0.000 description 4
- 229960003351 Prussian blue Drugs 0.000 description 4
- 239000002253 acid Substances 0.000 description 4
- 239000001045 blue dye Substances 0.000 description 4
- DCYOBGZUOMKFPA-UHFFFAOYSA-N iron(2+);iron(3+);octadecacyanide Chemical compound [Fe+2].[Fe+2].[Fe+2].[Fe+3].[Fe+3].[Fe+3].[Fe+3].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-] DCYOBGZUOMKFPA-UHFFFAOYSA-N 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- ATJFFYVFTNAWJD-UHFFFAOYSA-N tin hydride Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 4
- 241000349750 Baphia nitida Species 0.000 description 2
- 241001271907 Baphia racemosa Species 0.000 description 2
- 208000006558 Dental Calculus Diseases 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N HCl Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 240000007829 Haematoxylum campechianum Species 0.000 description 2
- 235000010701 Lavanda vera Nutrition 0.000 description 2
- 240000002809 Lavandula angustifolia Species 0.000 description 2
- 235000003515 Lavandula officinalis Nutrition 0.000 description 2
- 241001124569 Lycaenidae Species 0.000 description 2
- 241000658540 Ora Species 0.000 description 2
- VWDWKYIASSYTQR-UHFFFAOYSA-N Sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- XFXPMWWXUTWYJX-UHFFFAOYSA-N cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 description 2
- 230000003247 decreasing Effects 0.000 description 2
- 230000001066 destructive Effects 0.000 description 2
- 238000010790 dilution Methods 0.000 description 2
- 235000021384 green leafy vegetables Nutrition 0.000 description 2
- 235000011167 hydrochloric acid Nutrition 0.000 description 2
- 239000001102 lavandula vera Substances 0.000 description 2
- 235000018219 lavender Nutrition 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L na2so4 Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
- NHNBFGGVMKEFGY-UHFFFAOYSA-N nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 2
- 235000021018 plums Nutrition 0.000 description 2
- 239000000344 soap Substances 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-L sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/0076—Dyeing with mineral dye
Definitions
- my invention consists in preparing and using dyes for the purpose of dyeingfabrics in a raw ora manufactured state, the same being intended to produce what is termed prussian-blue dye, including the various shades of blue, green, lavender, purple, plum, brown, 853. This will dye wool and woolen goods, cotton and cotton goods, silk and silk goods, linen and linen goods, as well as all other fabrics, particularly animal productions.
- My jetamallar or prussian-blue dye is prepared as follows: For a middle shade of color take a wooden vessel, and having prepared one hundred parts (100 lbs.) of wool, cloth, or goods made from wool, and a sufficiency of water, the water is to be heated by steam to 125 Fahrenheit, at which heat put in one and onefourth part (1 lb.) of nitrate of potash, or nitrate ofsoda as a substitute. To this add one and one-fourth part (1 lb.) muriate of soda, or as substitute muriatic acid. Next add five parts (5lbs.) of sulphuric acid, these being thoroughly mixed and at Fahrenheit.
- the wool, cloth, or goods may beentcred and remain ten minutes.
- the goods should then be removed from the liquid, after which it should be cooled down to Fahrenheit, and at that degree of heat add one and a half part (1, ⁇ lb.) sulphuric muriate of tin, or as substitutes nitro-muriate'of tin or other salt of like character. Mix the liquor well together, and again materials should be increased; if the contrary, they should be decreased.
- Log-wood should be used to deepen the color, ahd gives a rich blooming color, and should be used in quantity to suit the judgment and produce the desired shade, while cam-wood, bar-wood, Brazilwood, peach-wood, &c., can be used so as to give the desired shade of color to the full variety, as before stated; but a fine dark green is produced when bichromite of potash is used.
- the salts may be mixed'with the sulphuric acid and afterward put in the dye-vessel; but it is far preferable to operate as hereinbefore described, for be it understood that the sulphate of potash and sulphate of soda that are formed when the sulphuric acid and salts come in contact with each other form a mordant for the coloring-matter and answer the purpose of salmixon or red tartar.
Description
UNITED STATES PATENT OFFICE.
SAMUEL MALLARD, OF STATEN ISLAND, NEW roan.
IMPROVEMENT IN DYEING.
Specification forming part of Letters Patent No- 6,242, dated March 527, 1849.
To all whom it may concern:
Be it known that I, SAMUEL MALLAED, of Staten Island, in the county of Richmond and State of New York, have invented a new and useful Process and Composition of Materials for Dyeing Fabrics; and I do hereby declare the following to be a full, clear, and exact description of the same.
The nature of my invention consists in preparing and using dyes for the purpose of dyeingfabrics in a raw ora manufactured state, the same being intended to produce what is termed prussian-blue dye, including the various shades of blue, green, lavender, purple, plum, brown, 853. This will dye wool and woolen goods, cotton and cotton goods, silk and silk goods, linen and linen goods, as well as all other fabrics, particularly animal productions.
My jetamallar or prussian-blue dye isprepared as follows: For a middle shade of color take a wooden vessel, and having prepared one hundred parts (100 lbs.) of wool, cloth, or goods made from wool, and a sufficiency of water, the water is to be heated by steam to 125 Fahrenheit, at which heat put in one and onefourth part (1 lb.) of nitrate of potash, or nitrate ofsoda as a substitute. To this add one and one-fourth part (1 lb.) muriate of soda, or as substitute muriatic acid. Next add five parts (5lbs.) of sulphuric acid, these being thoroughly mixed and at Fahrenheit. The wool, cloth, or goods may beentcred and remain ten minutes. At this time put in five parts (5 lbs.) of prussia-te of potash, or prussiate of soda as a substitute, without taking out the goods, and increase the heat to Fahrenheit, and run or contiuueit forty minutes more, or one hour in all, the heat being constantly increased until it arrives at a spring heat-thatis, near a boil-and thus continued as long as the color improves, or, say, twenty or thirty minutes. The goods should then be removed from the liquid, after which it should be cooled down to Fahrenheit, and at that degree of heat add one and a half part (1,} lb.) sulphuric muriate of tin, or as substitutes nitro-muriate'of tin or other salt of like character. Mix the liquor well together, and again materials should be increased; if the contrary, they should be decreased. Log-wood should be used to deepen the color, ahd gives a rich blooming color, and should be used in quantity to suit the judgment and produce the desired shade, while cam-wood, bar-wood, Brazilwood, peach-wood, &c., can be used so as to give the desired shade of color to the full variety, as before stated; but a fine dark green is produced when bichromite of potash is used.
It will be understood that when the nitrate of potash and muriate of soda come in contact with the sulphuric acid and water they produce a dilution ofmuriatic acid ofa mild type, which is advantageous for its lack of destructive qualities, as it will fail to weaken the cloth, as such acid does when distilled previous to its application.
The salts may be mixed'with the sulphuric acid and afterward put in the dye-vessel; but it is far preferable to operate as hereinbefore described, for be it understood that the sulphate of potash and sulphate of soda that are formed when the sulphuric acid and salts come in contact with each other form a mordant for the coloring-matter and answer the purpose of salmixon or red tartar.
The advantages of this method of making a dye are very great as regards two material facts: First, the colors thus produced will not crock, will stand washing with soap, and are very fast though not permanent colors to a positive degree, yet they are far more permanent than most any of the other dyes-that is, dyes prepared and 'used as heretofore; second, it is very much cheaper than dye, for these colors now known and in use for dyeing blues, greens, browns, plums, and such like shades and colors in full variety and of very bright and beautiful tints.
What I claim as my discovery, and desire to secure by Letters Patent, is-
The peculiar compound of nitrate of potash or nitrate of soda and muriate of soda with the sulphuric acid and coloring-matter, in manner and for the purpose herein described, by which I. make a superior and much cheaper dye than has before been made to produce such colors in fabrics when dyed, in manner and,
for the purposes herein described and set forth.
SAMUEL MALLARD. Witnesses:
J L. KINGSLEY, J. P. PIRSSON.
Publications (1)
Publication Number | Publication Date |
---|---|
US6242A true US6242A (en) | 1849-03-27 |
Family
ID=2066543
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US6242D Expired - Lifetime US6242A (en) | Improvement in dyeing |
Country Status (1)
Country | Link |
---|---|
US (1) | US6242A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2020229699A1 (en) | 2019-05-16 | 2020-11-19 | Ceva Sante Animale | Compositions and methods for increasing reproduction performance in non human mammals using recombinant luteinizing hormone |
-
0
- US US6242D patent/US6242A/en not_active Expired - Lifetime
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2020229699A1 (en) | 2019-05-16 | 2020-11-19 | Ceva Sante Animale | Compositions and methods for increasing reproduction performance in non human mammals using recombinant luteinizing hormone |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
US6242A (en) | Improvement in dyeing | |
US1273293A (en) | Vegetable dye and process of making same. | |
US2368690A (en) | Process for the improvement of the properties of artificial masses and fibers manufactured from proteinlike substances | |
US1635628A (en) | Dye solution | |
DE2638236C3 (en) | Process for dyeing leather by the simultaneous use of acidic and basic dyes | |
US1486353A (en) | George j | |
Parnell | Dyeing and Calico-printing | |
US46200A (en) | Improvement in the dyeing, printing, and manufacture of water-proof flocked cloth | |
US266825A (en) | Abmand mtiller j | |
US120393A (en) | Improvement in dyeing and printing madder colors | |
US8494A (en) | Improvement in processes for dyeing blue | |
US129753A (en) | Improvement in dyeing with indigo | |
DE466810C (en) | Process for producing real yellow tints | |
DE448909C (en) | Process for the production of dyes or colored bases | |
US647684A (en) | Fabric-renovating compound. | |
US9890A (en) | Teecke | |
US499690A (en) | Zinc res ist-mordant | |
US491951A (en) | Frank p | |
US1271067A (en) | Dyeing process. | |
US1026574A (en) | Process of dyeing and the product thereof. | |
US1485790A (en) | Dye solution and process for making and utilizing same | |
US60546A (en) | Alfred paraf | |
US1379175A (en) | Solvent for dyestuffs | |
DE1419551C (en) | Process for coloring nitrogen-containing fibers | |
US1755658A (en) | Textile paint |