US3200068A - Recovering fines in a mechanical dehydrator - Google Patents

Recovering fines in a mechanical dehydrator Download PDF

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US3200068A
US3200068A US247709A US24770962A US3200068A US 3200068 A US3200068 A US 3200068A US 247709 A US247709 A US 247709A US 24770962 A US24770962 A US 24770962A US 3200068 A US3200068 A US 3200068A
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fines
coal
drum
layer
water
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US247709A
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Jonakin James
Robert P Hensel
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Combustion Engineering Inc
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Combustion Engineering Inc
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Priority to US247709A priority Critical patent/US3200068A/en
Priority to GB49101/63A priority patent/GB1055278A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B04CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
    • B04BCENTRIFUGES
    • B04B1/00Centrifuges with rotary bowls provided with solid jackets for separating predominantly liquid mixtures with or without solid particles
    • B04B1/20Centrifuges with rotary bowls provided with solid jackets for separating predominantly liquid mixtures with or without solid particles discharging solid particles from the bowl by a conveying screw coaxial with the bowl axis and rotating relatively to the bowl
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B04CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
    • B04BCENTRIFUGES
    • B04B5/00Other centrifuges
    • B04B5/10Centrifuges combined with other apparatus, e.g. electrostatic separators; Sets or systems of several centrifuges

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  • This invention relates to an improvement in the method of separating solids and liquids.
  • An object of this invention is a method for recovering fines from the effiuent of a mechanical separator.
  • a further object is a method utilizing the layer of separated solids in a mechanical separator as a filter bed for fiocculated fines in the liquid discharge of said separator.
  • a more specific object is a method depositing a mixture of fiocculated fines and liquid, from the liquid discharged from a centrifuge, onto the solids on the beach of said centrifuge to filter said mixture and recover said fines.
  • a centrifugal separator indicated generally at 19 is supported for rotation inside of a casing 12 on bearings 14.
  • the drum 16 of the centrifuge may be rotated by any suitable means such as a pulley 18.
  • a second drum 20 mounted concentric with drum 16 is supported in any suitable manner such as by bearings, not shown, inside of the bearings 14 for rotation inside of the centrifuge drum 16.
  • a gear box 22 connecting the drums 16 and 26 will rotate the drum 2% ⁇ with the drum 16 but at a slightly diiferent rate.
  • a screw conveyor 24 mounted on the exterior of drum 20 extends between drum 20 and drum 16 and will force coal separated from a pipeline coal slurry, fed through pipe 26 and the stationary shaft 23 into the interior of drum 20 and 3,2fifi,68 Patented Aug.
  • the drum 16 is provided with a tapered portion 36, connecting the larger diameter portion with the smaller portion, to provide a beach supporting a layer of coal removed from the pool of liquid 38 that collects in the larger diameter of the drum 16. Liquid separated from the coal is discharged through openings 40, which openings will determine the depth of the pool.
  • the separated coal is forced along the beach by the screw impeller 24 and is discharged through the opening 42 into the coal discharge chute 44 and fed to a pulverizer, not shown, as indicated in my above identified co-pending application.
  • the efi luent discharged from the orifice 49 contains an appreciable amount of very fine coal which is carried along with the efiluent.
  • a flocculant such as Separan sold by Dow Chemical Company of Midland, Michigan, is mixed with the eflluent discharge through conduit 48 and fed to the flocculator 5% where the fines are fiocculated or coagulated and settle to the bottom of the flocculator.
  • the drum 20 is divided by a partition 58 into a compartment 6t) and a compartment 62.
  • the conduit 28 terminates in compartment s0 and delivers the pipeline slurry from conduit 26 into compartment 69 from which it is discharged through orifices 30 into the larger diameter portion of the drum 1a.
  • Conduit 56 extends completely through compartment 643 and through the center partition 58 into compartment 62 and discharges the mixture of fiocculated fines and water into the compartment 62 from which compartment they are discharged through orifices 64 under centrifugal force onto the layer of coal on the beach 36.
  • This coal layer which is removed from and separate from the liquid pool 3% acts as a filter or screen for this mixture of Water and flocculated fines, the water passing or filtering through the layer or bed of coal and along the beach to the pool 38.
  • the fines after being fiocculated are then fiocs large enough so that they will not pass readily through the compacted layer of coal on the beach 36 and hence are quite readily filtered or screened out to provide substantially a recovery of the fines.
  • the filtered or screened fine fiocs are fed along with the separated coal by the screw conveyor 22 along the beach and are discharged through the solids discharge orifice 42 and fed along with the separated coal through conduit 44 to the furnace.
  • a method of recovering fines from the efiiuent of a centrifuge dividing a coal slurry into a partially dewatered coal layer in the centrifuge and an elfiuent containing Water and coal fines comprising, the steps of forming materially larger particle units of the fines in said effluent by passing said effluent including said fines through a hoe- 3 4 culator and fiecculating said fines into enlarged flees of 2,596,616 5/52 Strezynski 233-7 X fines, feeding a slurry of said enlarged flees and Water onto 2,600,372 6/52 Milliken et a1.

Description

g- 1965 J. JONAKIN ETAL RECOVERING FINES IN A MECHANICAL DEHYDRATOR Filed Dec. 27, 1962 I I l Nw wh Mb mh wk NTOR ONAK
- HEN ATTORNEY United States Patent 3,200,068 RECOVERING FINES IN A MECHANICAL DEHYDRATOR James Jonakin and Robert P. Hensel, Simsbury, Conn,
assignors to Combustion Engineering, 1116., Windsor,
Conn., a corporation of Delaware Filed Dec. 27, 1962, Ser. No. 247,709 1 Claim. (Cl. 210-54) This invention relates to an improvement in the method of separating solids and liquids.
An object of this invention is a method for recovering fines from the effiuent of a mechanical separator.
A further object is a method utilizing the layer of separated solids in a mechanical separator as a filter bed for fiocculated fines in the liquid discharge of said separator.
A more specific object is a method depositing a mixture of fiocculated fines and liquid, from the liquid discharged from a centrifuge, onto the solids on the beach of said centrifuge to filter said mixture and recover said fines.
Other features and advantages will be apparent from the following specification and claim and from the attached drawing which illustrates a now preferred embodiment of the invention and in which the single figure is a side elevation, partly in section of a centrifuge and flocculator embodying the invention.
In mechanically separating water from the coal in a pipeline slurry an appreciable portion of the coal is discharged as fines with the liquid effluent from the mechanical separator. These fines must be recovered from the effluent as completely as possible and fed to the furnace in order to avoid a direct loss in, and a reduction in the overall efficiency of, the system of dewatering a pipeline coal slurry and feeding the dewatered, or partially dewatered, slurry to, and burning the same in, a furnace of a vapor generator.
As shown in my co-pending application Serial No. 159,600 filed December 15, 1961, entitled Drying and Burning of Pipeline Coal, on which the structure or" this application is an improvement and which may be referred to for further details of the system, previously the eflluent has been passed through a flocculator to fiocculate the fines and the mixture of the water and flocculated fines has been pumped back to the inlet of the mechanical de waterer and mixed with the incoming slurry and then fed to the mechanical dewaterer with the slurry. While this will produce a generally satisfactory removal of the fines We have found that by feeding this mixture of flocculated fines and water separately to the mechanical dewaterer, instead of mixing it with the incoming slurry, and then feeding this separate stream of flocculated fines and water onto the layer of coal on the beach of the mechanical separator, where the layer of coal is supported independent of the pool of separated liquid in the mechanical separator, that the coal layer will act as a filter bed to efiiciently filter the flocculated fines from the water in a single pass and improve and speed up the recovery of the fines.
As shown in the figure, a centrifugal separator indicated generally at 19 is supported for rotation inside of a casing 12 on bearings 14. The drum 16 of the centrifuge may be rotated by any suitable means such as a pulley 18. A second drum 20 mounted concentric with drum 16 is supported in any suitable manner such as by bearings, not shown, inside of the bearings 14 for rotation inside of the centrifuge drum 16. A gear box 22 connecting the drums 16 and 26 will rotate the drum 2%} with the drum 16 but at a slightly diiferent rate. A screw conveyor 24 mounted on the exterior of drum 20 extends between drum 20 and drum 16 and will force coal separated from a pipeline coal slurry, fed through pipe 26 and the stationary shaft 23 into the interior of drum 20 and 3,2fifi,68 Patented Aug. 10, 1965 through openings 3%) into the interior of the drum 16, lengthwise of the drum from the larger diameter 32 of the drum 16 toward the smaller diameter 34 of the drum 16. The drum 16 is provided with a tapered portion 36, connecting the larger diameter portion with the smaller portion, to provide a beach supporting a layer of coal removed from the pool of liquid 38 that collects in the larger diameter of the drum 16. Liquid separated from the coal is discharged through openings 40, which openings will determine the depth of the pool.
The separated coal is forced along the beach by the screw impeller 24 and is discharged through the opening 42 into the coal discharge chute 44 and fed to a pulverizer, not shown, as indicated in my above identified co-pending application.
The efi luent discharged from the orifice 49 contains an appreciable amount of very fine coal which is carried along with the efiluent. A flocculant such as Separan sold by Dow Chemical Company of Midland, Michigan, is mixed with the eflluent discharge through conduit 48 and fed to the flocculator 5% where the fines are fiocculated or coagulated and settle to the bottom of the flocculator. These fiocculated fines along with sufiicient water to provide a pumpable mixture, such as 30% fines and 70% water, is pumped by a pump 52, such as a gear or screw pump, through a conduit 54 and into a stationary conduit 56 supported inside of conduit .28.
The drum 20 is divided by a partition 58 into a compartment 6t) and a compartment 62. The conduit 28 terminates in compartment s0 and delivers the pipeline slurry from conduit 26 into compartment 69 from which it is discharged through orifices 30 into the larger diameter portion of the drum 1a. Conduit 56 extends completely through compartment 643 and through the center partition 58 into compartment 62 and discharges the mixture of fiocculated fines and water into the compartment 62 from which compartment they are discharged through orifices 64 under centrifugal force onto the layer of coal on the beach 36. This coal layer which is removed from and separate from the liquid pool 3% acts as a filter or screen for this mixture of Water and flocculated fines, the water passing or filtering through the layer or bed of coal and along the beach to the pool 38. The fines after being fiocculated are then fiocs large enough so that they will not pass readily through the compacted layer of coal on the beach 36 and hence are quite readily filtered or screened out to provide substantially a recovery of the fines. The filtered or screened fine fiocs are fed along with the separated coal by the screw conveyor 22 along the beach and are discharged through the solids discharge orifice 42 and fed along with the separated coal through conduit 44 to the furnace.
This combination of flocculating or coagulating fines in the effluent and then utilizing the layer or bed of coal as a filter in the mechanical separator gives an improved recovery of the fines both in time and in quantity without any additional equipment or any additional operating expense.
It is to be understood that the invention is not limited to the specific embodiment herein illustrated and described, but may be used in other ways Without departure from its spirit and that various changes can be made which would come within the scope of the invention which is limited only by the appended claim.
We claim:
A method of recovering fines from the efiiuent of a centrifuge dividing a coal slurry into a partially dewatered coal layer in the centrifuge and an elfiuent containing Water and coal fines, comprising, the steps of forming materially larger particle units of the fines in said effluent by passing said effluent including said fines through a hoe- 3 4 culator and fiecculating said fines into enlarged flees of 2,596,616 5/52 Strezynski 233-7 X fines, feeding a slurry of said enlarged flees and Water onto 2,600,372 6/52 Milliken et a1. 2337 the layer of partially dewatered coal in said centrifuge 2,685,369 8/54 Crossley 233-14 X and utilizing said coal layer as a screen and filter, screen- OTHER REFERENCES ing said enlarged fiocs by said coal layer and filtering the water from said slurry of enlarged fiocs through said layer. 5 DOW Diamond: Vol-V 18, published'by The DOW Chemical Co., Midland, Michigan, 1955, pages 1-4. References Cited by the Examiner UNITED STATES PATENTS 2,069,024 1/37 Vohrnann et a1. 210-54 10 REUBEN FRIEDMAN, Primary Examiner.
HARRY B. THORNTON, Examiner.
US247709A 1962-12-27 1962-12-27 Recovering fines in a mechanical dehydrator Expired - Lifetime US3200068A (en)

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GB49101/63A GB1055278A (en) 1962-12-27 1963-12-12 Method and apparatus for mechanically separating coal and water from a coal slurry

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Cited By (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3407934A (en) * 1965-04-22 1968-10-29 Karl Goran Henrik Ejefors Method and apparatus for separating particles from suspensions such as sludge and the like
US3430850A (en) * 1967-11-13 1969-03-04 Perfection Eng Co Inc Centrifugal separator
DE1632270B1 (en) * 1966-11-09 1971-06-16 Bird Machine Co centrifuge
DE1757369B1 (en) * 1967-05-26 1971-12-23 Alfa Laval Ab centrifuge
US3696923A (en) * 1970-07-28 1972-10-10 Bethlehem Steel Corp Method for recovering fine coal and coal-containing particles in a coal recovery circuit
US3854658A (en) * 1973-05-07 1974-12-17 Dorr Oliver Inc Solid bowl conveyer type centrifuge
US4209128A (en) * 1979-04-06 1980-06-24 Yara Engineering Corporation Methods and apparatus for classifying fine particle solids
US4216082A (en) * 1977-01-07 1980-08-05 Shell Oil Company Method for processing a slurry of coal particles in water
US4257879A (en) * 1976-10-21 1981-03-24 Bergwerksverband Gmbh Process for dewatering coal slurries
US4298160A (en) * 1977-05-24 1981-11-03 Thomas Broadbent & Sons Limited Solid bowl decanter centrifuges
US4661243A (en) * 1984-02-22 1987-04-28 Hoesch Aktiengesellschaft Method and apparatus for treating moist dust and mud in the steel industry
US4761157A (en) * 1983-05-18 1988-08-02 Pennwalt Corporation Centrifuge apparatus
US5176616A (en) * 1989-06-29 1993-01-05 Kloeckner-Humboldt-Deutz Aktiengesellschaft Method and apparatus for the after-treatment of the thick material in the thick material discharge region of a solid bowl worm centrifuge
US5509882A (en) * 1994-09-12 1996-04-23 Tetra Laval Holdings & Finance S.A. Decanter centrifuge having an offset conveyor flight to aid rinsing
US5899844A (en) * 1997-06-23 1999-05-04 Eberle, Sr.; Louis C. Method of controlling the density of the solids separated from a feed slurry in a separator
US20110105292A1 (en) * 2008-06-06 2011-05-05 M-I L.L.C. Dual feed centrifuge

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116328457B (en) * 2023-03-16 2023-12-19 浙江伊诺环保集团股份有限公司 Fly ash pulping water washing process and pulping water washing equipment

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2069024A (en) * 1933-01-05 1937-01-26 Forderanlagen Ernst Heckel Mit Process and apparatus for clarifying coal slurry and the like
US2596616A (en) * 1951-04-09 1952-05-13 Laval Separator Co De Method and system for separating solids from liquids
US2600372A (en) * 1949-12-16 1952-06-10 Bird Machine Co Centrifugal separator
US2685369A (en) * 1951-06-27 1954-08-03 Allied Chem & Dye Corp Coagulation of finely divided suspended solids

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2069024A (en) * 1933-01-05 1937-01-26 Forderanlagen Ernst Heckel Mit Process and apparatus for clarifying coal slurry and the like
US2600372A (en) * 1949-12-16 1952-06-10 Bird Machine Co Centrifugal separator
US2596616A (en) * 1951-04-09 1952-05-13 Laval Separator Co De Method and system for separating solids from liquids
US2685369A (en) * 1951-06-27 1954-08-03 Allied Chem & Dye Corp Coagulation of finely divided suspended solids

Cited By (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3407934A (en) * 1965-04-22 1968-10-29 Karl Goran Henrik Ejefors Method and apparatus for separating particles from suspensions such as sludge and the like
DE1632270B1 (en) * 1966-11-09 1971-06-16 Bird Machine Co centrifuge
DE1757369B1 (en) * 1967-05-26 1971-12-23 Alfa Laval Ab centrifuge
US3430850A (en) * 1967-11-13 1969-03-04 Perfection Eng Co Inc Centrifugal separator
US3696923A (en) * 1970-07-28 1972-10-10 Bethlehem Steel Corp Method for recovering fine coal and coal-containing particles in a coal recovery circuit
US3854658A (en) * 1973-05-07 1974-12-17 Dorr Oliver Inc Solid bowl conveyer type centrifuge
US4257879A (en) * 1976-10-21 1981-03-24 Bergwerksverband Gmbh Process for dewatering coal slurries
US4216082A (en) * 1977-01-07 1980-08-05 Shell Oil Company Method for processing a slurry of coal particles in water
US4298160A (en) * 1977-05-24 1981-11-03 Thomas Broadbent & Sons Limited Solid bowl decanter centrifuges
US4209128A (en) * 1979-04-06 1980-06-24 Yara Engineering Corporation Methods and apparatus for classifying fine particle solids
US4761157A (en) * 1983-05-18 1988-08-02 Pennwalt Corporation Centrifuge apparatus
US4661243A (en) * 1984-02-22 1987-04-28 Hoesch Aktiengesellschaft Method and apparatus for treating moist dust and mud in the steel industry
US5176616A (en) * 1989-06-29 1993-01-05 Kloeckner-Humboldt-Deutz Aktiengesellschaft Method and apparatus for the after-treatment of the thick material in the thick material discharge region of a solid bowl worm centrifuge
US5509882A (en) * 1994-09-12 1996-04-23 Tetra Laval Holdings & Finance S.A. Decanter centrifuge having an offset conveyor flight to aid rinsing
US5899844A (en) * 1997-06-23 1999-05-04 Eberle, Sr.; Louis C. Method of controlling the density of the solids separated from a feed slurry in a separator
US20110105292A1 (en) * 2008-06-06 2011-05-05 M-I L.L.C. Dual feed centrifuge
US8961381B2 (en) * 2008-06-06 2015-02-24 M-I L.L.C. Dual feed centrifuge

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