US3098294A - Lubricant for metal forming process - Google Patents

Lubricant for metal forming process Download PDF

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Publication number
US3098294A
US3098294A US72809A US7280960A US3098294A US 3098294 A US3098294 A US 3098294A US 72809 A US72809 A US 72809A US 7280960 A US7280960 A US 7280960A US 3098294 A US3098294 A US 3098294A
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metal
solution
brass
heated solution
cold drawing
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US72809A
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Arthur M Shapiro
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21DWORKING OR PROCESSING OF SHEET METAL OR METAL TUBES, RODS OR PROFILES WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21D51/00Making hollow objects
    • B21D51/16Making hollow objects characterised by the use of the objects
    • B21D51/54Making hollow objects characterised by the use of the objects cartridge cases, e.g. for ammunition, for letter carriers in pneumatic-tube plants
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S72/00Metal deforming
    • Y10S72/70Deforming specified alloys or uncommon metal or bimetallic work

Definitions

  • This invention relates to metal forming lubricants. Its purpose is to provide an improved lubricant whereby the force of the metal shaping operation, such as cold drawing and stamping, is materially reduced.
  • the results of these tests are shown in the following tabulation.
  • the first column of this tabulation lists a series of single acid sodium soaps.
  • the second column indicates the number of carbon atoms in the fatty acid while the third column shows the number of double bonds in the acid.
  • the fourth column indicates the percent difference in the forces required to cold draw a 70-30 lbrass draw piece into a 30 caliber cartridge casing using typical commercially available multiple fatty acid soaps containing between about 20 to 40% sodium oleate and about 60 to 80% sodium stearate and the sodium soaps of my invention.
  • the minus signs in column 4 indicate that the single acid soaps of the invention required less force to form the cartridge case than when multiple acid soaps were employed.
  • the positive signs indicate the opposite.
  • the last column presents data similar to those of column 4, but with a mild steel such as 1020.
  • the percentages above represent averages of five individual runs.
  • the multiple fatty acid soaps used to obtain the comparison data above i.e., the 20-40% sodium oleate and 60-80% sodium stearate, were considered the 3,098,294 Patented July 23, 1963 most satisfactory to date as revealed by exhaustive laboratory experimentation with cold drawing -30 and -20 brass and mild steels.
  • Other multiple fatty acid soaps containing a mixture of ingredients such as lard oil, soy bean oil, and tallow fatty acid soaps (40 titre) yielded results inferior to the multiple fatty acid soaps used.
  • the data above are also representative of those obtained when cold drawing 50 caliber 70-30 brass, and 30 and 50 caliber mild steel, into cartridge casings.
  • the metal is cleaned if required and immersed in a 1 to 2% solution of sodium behenate in water which is maintained at a temperature of about F. to 200 F. for about 3 to 5 minutes. Thereafter, one of several procedures is followed. According to one procedure, the metal is removed from the solution and immediately cold drawn while flooding it with the heated solution. Another procedure involves removing the metal from the heated solution and allowing it to dry over night, and then dipping it in the heated solution before cold drawing. Still another procedure is to remove the metal from the heated solution, dry over night, and cold draw in that condition.
  • the tabulated data were obtained using the second procedure outlined above, but generally comparable data were obtained when using any of the three methods outlined above.
  • the sodium behenate may be increased upwardly to about 20% of the aqueous solution.
  • the improved lubrication made possible by the present invention has the important advantage that it decreases power consumption, prolongs the life of the dies used, and permits the forming of heavier gauge metal.
  • a process of cold drawing a small article from a draw piece made of a metal selected from the group consisting of 70-30 brass, 80-20 brass, and mild steel comprising immersing the metal to be cold drawn in an aqueous solution of about 1 to 2% sodium behenate soap, said solution being maintained at a temperature between about 150 to 200 F., permitting said immersed metal to remain submerged in said heated solution for a period ranging between about 3 to 5 minutes, removing said immersed metal from the heated solution and cold drawing said removed metal into a small article while flooding with said heated solution.
  • a process of cold drawing a small cartridge case from a draw piece made of a metal selected from the group consisting of 70-30 brass, 80-20 brass, and mild steel comprising immersing the metal to be cold drawn in an aqueous solution of about 1 to 2% sodium behenate soap, said solution being maintained at a temperature between about 150 to 200 F., permitting said immersed metal to remain submerged in said heated solution for a period ranging between about 3 to 5 minutes, removing said immersed metal from the heated solution, allowing said removed metal to dry over night and cold drawing said dried metal into a small caliber cartridge case.
  • a process of cold drawing a small cartridge case from a draw piece made of a metal selected from the group consisting of 70-30 brass, 80-20 brass, and mild steel comprising immersing the metal to be cold drawn in an aqueous solution of about 1 to 2% sodium behenate soap, said solution being maintained at a temperature between about 150 to 200 F., permitting said immersed metal to remain submerged in said heated solution for a period ranging between about 3 to 5 minutes, removing said immersed metal from the heated solution, allowing said removed metal to dry over night, dipping said removed metal into said heated solution and immediately cold drawing said dipped metal into a small cartridge case.

Description

LUERIQANT FOR METAL FOG PRGCESS Arthur M. Shapiro, Philadeiphia, Pa., assignor to the United States of America as represented by the Secretary of the Army No Drawing. Filed Nov. 30, 1960, Ser. No. 72,309
3 Claims. (Cl. 29-523) (Granted under Title 35, US. Code (1952), sec. 266) The invention described herein may be manufactured and used by or for the Government for governmental purposes without the payment to me of any royalty thereon.
This application is a continuation-in-part of my application Serial No. 4,825, filed January 26, 1960, entitled Lubricant for Metal Forming Process, now abandoned.
This invention relates to metal forming lubricants. Its purpose is to provide an improved lubricant whereby the force of the metal shaping operation, such as cold drawing and stamping, is materially reduced.
Heretofore various aqueous soap solutions have been utilized in the formation of metal objects. These solutions have generally included sodium soaps which contain a plurality of fatty acids. As a result of comparative tests, it has been found that certain sodium soaps containing a single acid will function to reduce the required metal forming force to an extent not realized with sodium soaps containing a plurality of fatty acids.
The results of these tests are shown in the following tabulation. The first column of this tabulation lists a series of single acid sodium soaps. The second column indicates the number of carbon atoms in the fatty acid while the third column shows the number of double bonds in the acid. The fourth column indicates the percent difference in the forces required to cold draw a 70-30 lbrass draw piece into a 30 caliber cartridge casing using typical commercially available multiple fatty acid soaps containing between about 20 to 40% sodium oleate and about 60 to 80% sodium stearate and the sodium soaps of my invention. The minus signs in column 4 indicate that the single acid soaps of the invention required less force to form the cartridge case than when multiple acid soaps were employed. The positive signs indicate the opposite. The last column presents data similar to those of column 4, but with a mild steel such as 1020.
The percentages above represent averages of five individual runs. The multiple fatty acid soaps used to obtain the comparison data above, i.e., the 20-40% sodium oleate and 60-80% sodium stearate, were considered the 3,098,294 Patented July 23, 1963 most satisfactory to date as revealed by exhaustive laboratory experimentation with cold drawing -30 and -20 brass and mild steels. Other multiple fatty acid soaps containing a mixture of ingredients such as lard oil, soy bean oil, and tallow fatty acid soaps (40 titre) yielded results inferior to the multiple fatty acid soaps used. The data above are also representative of those obtained when cold drawing 50 caliber 70-30 brass, and 30 and 50 caliber mild steel, into cartridge casings.
In utilizing sodium behenate soap as a lubricant in cold drawing operations, the metal is cleaned if required and immersed in a 1 to 2% solution of sodium behenate in water which is maintained at a temperature of about F. to 200 F. for about 3 to 5 minutes. Thereafter, one of several procedures is followed. According to one procedure, the metal is removed from the solution and immediately cold drawn while flooding it with the heated solution. Another procedure involves removing the metal from the heated solution and allowing it to dry over night, and then dipping it in the heated solution before cold drawing. Still another procedure is to remove the metal from the heated solution, dry over night, and cold draw in that condition. The tabulated data were obtained using the second procedure outlined above, but generally comparable data were obtained when using any of the three methods outlined above.
For larger caliber cases or heavier gauge metals, the sodium behenate may be increased upwardly to about 20% of the aqueous solution.
As will be understood by those skilled in the art, the improved lubrication made possible by the present invention has the important advantage that it decreases power consumption, prolongs the life of the dies used, and permits the forming of heavier gauge metal.
-I claim:
1. In a process of cold drawing a small article from a draw piece made of a metal selected from the group consisting of 70-30 brass, 80-20 brass, and mild steel, the steps comprising immersing the metal to be cold drawn in an aqueous solution of about 1 to 2% sodium behenate soap, said solution being maintained at a temperature between about 150 to 200 F., permitting said immersed metal to remain submerged in said heated solution for a period ranging between about 3 to 5 minutes, removing said immersed metal from the heated solution and cold drawing said removed metal into a small article while flooding with said heated solution.
2. In a process of cold drawing a small cartridge case from a draw piece made of a metal selected from the group consisting of 70-30 brass, 80-20 brass, and mild steel, the steps comprising immersing the metal to be cold drawn in an aqueous solution of about 1 to 2% sodium behenate soap, said solution being maintained at a temperature between about 150 to 200 F., permitting said immersed metal to remain submerged in said heated solution for a period ranging between about 3 to 5 minutes, removing said immersed metal from the heated solution, allowing said removed metal to dry over night and cold drawing said dried metal into a small caliber cartridge case.
3. In a process of cold drawing a small cartridge case from a draw piece made of a metal selected from the group consisting of 70-30 brass, 80-20 brass, and mild steel, the steps comprising immersing the metal to be cold drawn in an aqueous solution of about 1 to 2% sodium behenate soap, said solution being maintained at a temperature between about 150 to 200 F., permitting said immersed metal to remain submerged in said heated solution for a period ranging between about 3 to 5 minutes, removing said immersed metal from the heated solution, allowing said removed metal to dry over night, dipping said removed metal into said heated solution and immediately cold drawing said dipped metal into a small cartridge case.
UNITED STATES PATENTS Salender Apr. 13, 1937 Spring Sept. 21, 1943 Whitney Oct. 14, 1952 Leduc Jan. 27, 1959 Fucinari Dec. 27, 1960

Claims (1)

1. IN A PROCESS OF COLD DRAWING A SMALL ARTICLE FROM A DRAW PIECE MADE OF A METAL SELECTED FROM THE GROUP CONSISTING OF 70-30 BRASS, 80-20 BRASS, AND MILD STEEL, THE STEPS COMPRISING IMMERSING THE METAL TO BE COLD DRAWN IN AN AQUEOUS SOLUTION OF ABOUT 1 TO 2% SODIUM BEHENATE SOAP, SAID SOLUTION BEING MAINTAINED AT A TEMPERATURE BETWEEN ABOUT 150 TO 200*F., PERMITTING SAID IMMERSED METAL TO REMAIN SUBMERGED IN SAID HEATED SOLUTION FOR A PERIOD RANGING BETWEEN ABOUT 3 TO 5 MINUTES, REMOVING SAID IMMERSED METAL FROM THE HEATED SOLUTION AND COLD DRAWING SAID REMOVED METAL INTO A SMALL ARTICLE WHILE FLOODING WITH SAID HEATED SOLUTION.
US72809A 1960-11-30 1960-11-30 Lubricant for metal forming process Expired - Lifetime US3098294A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3372117A (en) * 1965-11-26 1968-03-05 Hooker Chemical Corp Cold forming lubricant
US4099989A (en) * 1975-09-08 1978-07-11 Kaiser Aluminum & Chemical Corporation Protective coating for aluminum products
US6277795B1 (en) 1996-09-10 2001-08-21 Kanthal Ab Metal wire or a metal strip having a lubricating surface layer, and a method for its preparation
WO2007132851A1 (en) * 2006-05-15 2007-11-22 Sumitomo Metal Industries, Ltd. Lubricant for steel pipe cold working and relevant method of cold working

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2076793A (en) * 1935-06-05 1937-04-13 American Rolling Mill Co Process to prevent sticking during annealing
US2329731A (en) * 1942-02-12 1943-09-21 Spring Samuel Drawing lubricant
US2613626A (en) * 1948-07-21 1952-10-14 Heintz Mfg Co Method of cold drawing sheet metal
US2870903A (en) * 1955-04-08 1959-01-27 Diamond Alkali Co Metal drawing lubricant
US2966425A (en) * 1959-02-18 1960-12-27 Montgomery H A Co Drawing lubricant coating methods and compositions

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2076793A (en) * 1935-06-05 1937-04-13 American Rolling Mill Co Process to prevent sticking during annealing
US2329731A (en) * 1942-02-12 1943-09-21 Spring Samuel Drawing lubricant
US2613626A (en) * 1948-07-21 1952-10-14 Heintz Mfg Co Method of cold drawing sheet metal
US2870903A (en) * 1955-04-08 1959-01-27 Diamond Alkali Co Metal drawing lubricant
US2966425A (en) * 1959-02-18 1960-12-27 Montgomery H A Co Drawing lubricant coating methods and compositions

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3372117A (en) * 1965-11-26 1968-03-05 Hooker Chemical Corp Cold forming lubricant
US4099989A (en) * 1975-09-08 1978-07-11 Kaiser Aluminum & Chemical Corporation Protective coating for aluminum products
US6277795B1 (en) 1996-09-10 2001-08-21 Kanthal Ab Metal wire or a metal strip having a lubricating surface layer, and a method for its preparation
WO2007132851A1 (en) * 2006-05-15 2007-11-22 Sumitomo Metal Industries, Ltd. Lubricant for steel pipe cold working and relevant method of cold working
US20090090439A1 (en) * 2006-05-15 2009-04-09 Sumitomo Metal Industries, Ltd. Cold working lubricant and cold working method for steel pipe
JPWO2007132851A1 (en) * 2006-05-15 2009-09-24 住友金属工業株式会社 Lubricant for cold working of steel pipe and cold working method
US20100132427A1 (en) * 2006-05-15 2010-06-03 Sumitomo Metal Industries, Ltd. Cold Working Lubricant and Cold Working Method for Steel Pipe

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