US2274673A - Lubricating composition - Google Patents
Lubricating composition Download PDFInfo
- Publication number
- US2274673A US2274673A US328095A US32809540A US2274673A US 2274673 A US2274673 A US 2274673A US 328095 A US328095 A US 328095A US 32809540 A US32809540 A US 32809540A US 2274673 A US2274673 A US 2274673A
- Authority
- US
- United States
- Prior art keywords
- lubricating
- oil
- lubricating composition
- polymerized
- higher fatty
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M7/00—Solid or semi-solid compositions essentially based on lubricating components other than mineral lubricating oils or fatty oils and their use as lubricants; Use as lubricants of single solid or semi-solid substances
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/06—Mixtures of thickeners and additives
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- C10M5/00—Solid or semi-solid compositions containing as the essential lubricating ingredient mineral lubricating oils or fatty oils and their use
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- C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
- C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
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- C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
- C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
- C10M2203/102—Aliphatic fractions
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- C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
- C10M2203/104—Aromatic fractions
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- C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
- C10M2203/106—Naphthenic fractions
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- C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
- C10M2203/108—Residual fractions, e.g. bright stocks
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- C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
- C10M2205/026—Butene
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- C10M2205/17—Fisher Tropsch reaction products
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- C10M2207/022—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms containing at least two hydroxy groups
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- C10M2207/023—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings
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- C10M2207/023—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings
- C10M2207/026—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings with tertiary alkyl groups
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- C10M2207/10—Carboxylix acids; Neutral salts thereof
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- C10M2207/122—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms monocarboxylic
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Definitions
- compositions of mineral oil or vegetable oil, lithium soaps and a stabilizing agent such as polymerized esters of the acrylic series can be used in production of a lubricating grease.
- a mixture having the following formulation limits may be employed, the percentages depending upon the type of service for which it is intended:
- a preferred process of preparing the lubricating grease is as follows, for example: 85 parts of a mineral oil is heated up to C. to 250 C. at'which temperature 14 parts of lithium stearate is added and the temperature maintained for twenty to thirty minutes. soap becomes thoroughly mixed with the oil, the temperature is allowed to slowly recede. At about C. while the solution is still fluid one part of cetyl methacrylate is added and thoroughly stirred-into the solution. The solution is allowed to cool and jell after which it is ready for use.
- My invention includes the employment of polymerized esters of acrylic and methacrylic acids.
- a lubricating composition comprising a mineral oil, and a lithium soap of a higher fatty acid in quantity sufiicient substantially to thicken said oil.
- a lubricating composition comprising a vegetable oil and a lithium soap of a higher fatty acid in quantity sufllcient substantially to thicken said oil.
- a lubricating composition comprising a mineral oil, a lithium soap of a' higher fatty acid in quantity sufiicient substantially to thicken said oil and a polymerized ester of acrylic acid.
- a lubricating composition comprising a vegetable oil, a lithium soap of a higher fatty acid in quantity suflicient substantially to thicken and a polymerized ester of acrylic acid.
- a lubricating composition comprising oleaginous material selected from the group consisting of mineral oils and vegetable oils, a lithium soap of a higher fatty acid in quantity suflicient substantially to thicken and a polymerized ester of methacrylic acid.
- a lubricating composition comprising oleaginous material selected from the group consisting of mineral oils and vegetable oils, a lithium soap in quantity substantially to thicken, and a polymerized vinyl ester having a hydrocar- After the bon radical having an excess of 6 carbon atoms.
- a lubricating-composition comprising oleaginous material selected from the group con- 'sisting of mineral oils and vegetable oils, a V lithium soap in quantity substantially to thicken,-
- a lubricating grease comprising 54 to 90 parts of an oleaginous material selected from the group consisting of mineral and vegetable oils, 10 to 40 parts of a lithium soap of a higher fatty acid, and
Description
- Patented Mar. 3, 1942 UNITED STATES PATENT OFFICE- 2.214.673 wnmca'rmo COMPOSITION Clarence E. Earle, Washington, D. C.
No Drawing. Application April 5, 1940,
Serial No. 328,095
(Granted under the act of March 3, 1883, as amended April 30, 1928; 370 0. G. 757) Claims.
manufactured and produced by compounding mineral oil and'metallic salts such as sodium stearate, potassium stear'ate, or the oleates or other higher fatty acid salts of these two metals or alkaline earth salts of these acids such as those of calcium, barium, strontium, etc. It is significant to point out here that neither the literature nor the books on the art mention the use of lithium salts of the higher fatty acids, such as stearates, oleates, palmitates, etc., for producing greases.
I have found that the use of lithium soap or salts of soap forming higher fatty acids in the production of lubricating greases gives the greases entirely different properties from those obtained by the use of the other alkali metal salts. The greases produced by my method are water resistant, whereas the other alkali salts do not give such a property. My lithium soap greases withstand temperature greatly in excess of those containing other alkali metal salts. The properties of these improved lubricating greases are not only widely different from the other alkali metal soap types but also they are much more stable to temperature and pressure, both chemically and physically.
I have found that the addition of polymerized esters of the acrylic series materially improves the thixotropic properties of my lubricating compounds. Also I have found that the polymers of vinyl esters with long chains enhance the thixotropic properties of these improved lubricating compounds.
Various compositions of mineral oil or vegetable oil, lithium soaps and a stabilizing agent such as polymerized esters of the acrylic series can be used in production of a lubricating grease. As an example, a mixture having the following formulation limits may be employed, the percentages depending upon the type of service for which it is intended:
Percent by weight Mineral nil 90-54 Lithium soap or salt 10-40 Polymerized esters of methacrylic acid--- 0- 6 A preferred process of preparing the lubricating grease is as follows, for example: 85 parts of a mineral oil is heated up to C. to 250 C. at'which temperature 14 parts of lithium stearate is added and the temperature maintained for twenty to thirty minutes. soap becomes thoroughly mixed with the oil, the temperature is allowed to slowly recede. At about C. while the solution is still fluid one part of cetyl methacrylate is added and thoroughly stirred-into the solution. The solution is allowed to cool and jell after which it is ready for use. My invention includes the employment of polymerized esters of acrylic and methacrylic acids.
I have also found that the addition of small amounts of lithium soaps to lubricating oils improves their lubricating properties, thus lowering the power consumption and leakage from bear ing interfaces.
The grease made in accordance with my infor governmental purposes without the payment of any royalties thereon or therefor.
I claim:
1. A lubricating composition comprising a mineral oil, and a lithium soap of a higher fatty acid in quantity sufiicient substantially to thicken said oil.
2. A lubricating composition comprising a vegetable oil and a lithium soap of a higher fatty acid in quantity sufllcient substantially to thicken said oil.-
' 3. A lubricating composition comprising a mineral oil, a lithium soap of a' higher fatty acid in quantity sufiicient substantially to thicken said oil and a polymerized ester of acrylic acid.
4. A lubricating composition comprising a vegetable oil, a lithium soap of a higher fatty acid in quantity suflicient substantially to thicken and a polymerized ester of acrylic acid.
5. A lubricating composition comprising oleaginous material selected from the group consisting of mineral oils and vegetable oils, a lithium soap of a higher fatty acid in quantity suflicient substantially to thicken and a polymerized ester of methacrylic acid.
6. A lubricating composition comprising oleaginous material selected from the group consisting of mineral oils and vegetable oils, a lithium soap in quantity substantially to thicken, and a polymerized vinyl ester having a hydrocar- After the bon radical having an excess of 6 carbon atoms.
7. A lubricating-composition comprising oleaginous material selected from the group con- 'sisting of mineral oils and vegetable oils, a V lithium soap in quantity substantially to thicken,-
and a polymerized ester of acrylic acid.
8. As a new composition of matter, a lubricating grease comprising 54 to 90 parts of an oleaginous material selected from the group consisting of mineral and vegetable oils, 10 to 40 parts of a lithium soap of a higher fatty acid, and
not more than 6 parts of a polymerized lon'gchained ester of methacrylic acid.
1 ent in quantities suflicient substantially to thicken the oil.
CLARENCE E. EARLE.
Priority Applications (17)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
NL73006D NL73006C (en) | 1940-04-05 | ||
NL137009D NL137009C (en) | 1940-04-05 | ||
NL66982D NL66982C (en) | 1940-04-05 | ||
NL66799D NL66799C (en) | 1940-04-05 | ||
US259921A US2274613A (en) | 1939-03-04 | 1939-03-04 | Refrigeration apparatus |
US328095A US2274673A (en) | 1940-04-05 | 1940-04-05 | Lubricating composition |
US364248A US2274675A (en) | 1940-04-05 | 1940-11-04 | Lubricant containing lithium salts |
US364246A US2293052A (en) | 1940-04-05 | 1940-11-04 | Lubricant containing a lithium compound |
US364247A US2274674A (en) | 1940-04-05 | 1940-11-04 | Lubricant containing a lithium compound |
US364249A US2274676A (en) | 1940-04-05 | 1940-11-04 | Lubricant containing lithium salts |
FR1090381D FR1090381A (en) | 1940-04-05 | 1947-07-30 | Lubricants |
GB21283/47A GB637932A (en) | 1940-04-05 | 1947-08-05 | Improvements in or relating to lubricants |
CH269511D CH269511A (en) | 1940-04-05 | 1947-08-07 | Lubricant. |
GB722/48A GB643536A (en) | 1940-04-05 | 1948-01-09 | Lubricating compositions |
DEP14700D DE842108C (en) | 1940-04-05 | 1948-10-02 | lubricant |
DEN32A DE886948C (en) | 1940-04-05 | 1948-10-12 | lubricant |
US103164A US2566793A (en) | 1940-04-05 | 1949-07-05 | Grease compositions |
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US328095A US2274673A (en) | 1940-04-05 | 1940-04-05 | Lubricating composition |
US472509A US2397956A (en) | 1943-01-15 | 1943-01-15 | Production of lubricants |
GB2566793X | 1948-10-18 |
Publications (1)
Publication Number | Publication Date |
---|---|
US2274673A true US2274673A (en) | 1942-03-03 |
Family
ID=32233928
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US328095A Expired - Lifetime US2274673A (en) | 1939-03-04 | 1940-04-05 | Lubricating composition |
US103164A Expired - Lifetime US2566793A (en) | 1940-04-05 | 1949-07-05 | Grease compositions |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US103164A Expired - Lifetime US2566793A (en) | 1940-04-05 | 1949-07-05 | Grease compositions |
Country Status (6)
Country | Link |
---|---|
US (2) | US2274673A (en) |
CH (1) | CH269511A (en) |
DE (2) | DE842108C (en) |
FR (1) | FR1090381A (en) |
GB (2) | GB637932A (en) |
NL (4) | NL73006C (en) |
Cited By (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2417264A (en) * | 1944-01-01 | 1947-03-11 | Standard Oil Dev Co | Lubricant |
US2432577A (en) * | 1942-05-02 | 1947-12-16 | Patterson | Smoke screen composition |
US2443378A (en) * | 1944-07-08 | 1948-06-15 | Du Pont | Chemical process and product |
US2446177A (en) * | 1945-06-21 | 1948-08-03 | George M Hain | Silicone grease and method of preparation |
US2450219A (en) * | 1945-04-10 | 1948-09-28 | Texas Co | Texture-stable lithium base grease |
US2451039A (en) * | 1941-12-24 | 1948-10-12 | Standard Oil Dev Co | Lubricant |
US2451895A (en) * | 1946-06-08 | 1948-10-19 | Shell Dev | Synthetic grease |
US2468099A (en) * | 1947-10-01 | 1949-04-26 | Standard Oil Dev Co | High-temperature grease |
US2489281A (en) * | 1947-04-04 | 1949-11-29 | California Research Corp | Methacrylates in constant viscosity oils |
US2491028A (en) * | 1947-10-11 | 1949-12-13 | Standard Oil Dev Co | Lubricating grease compositions |
US2553568A (en) * | 1943-02-25 | 1951-05-22 | Finkelstein Leo | Incendiary filling for bombs |
US2577706A (en) * | 1948-11-26 | 1951-12-04 | California Research Corp | High melting-high water-resistant grease |
US2623017A (en) * | 1950-08-03 | 1952-12-23 | Phillips Petroleum Co | Gel-type grease |
US2681313A (en) * | 1950-02-20 | 1954-06-15 | California Research Corp | Alkyl orthosilicate and alkoxysiloxane base grease compositions |
US2696470A (en) * | 1951-03-01 | 1954-12-07 | Standard Oil Dev Co | Lubricating greases thickened with carbon black |
US2719124A (en) * | 1953-05-15 | 1955-09-27 | Exxon Research Engineering Co | Grease compositions containing oxonated acid soaps |
US2737494A (en) * | 1952-09-27 | 1956-03-06 | Socony Mobil Oil Co Inc | Stable greases containing synthetic gelling agents |
US4027070A (en) * | 1974-03-08 | 1977-05-31 | Nippon Steel Corporation | Steel plate for preparing cans by ironing |
Families Citing this family (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2755249A (en) * | 1956-07-17 | Halogenated hydrocarbon-treated | ||
US2651616A (en) * | 1948-01-13 | 1953-09-08 | Shell Dev | Lithium hydroxy stearate grease compositions |
BE510612A (en) * | 1951-04-13 | |||
US2606153A (en) * | 1951-04-25 | 1952-08-05 | Gen Electric | Silicone greases |
US2755247A (en) * | 1951-04-27 | 1956-07-17 | Texas Co | Wide temperature range alkali metal grease containing excess alkali metal hydroxides |
US2712527A (en) * | 1952-08-26 | 1955-07-05 | Exxon Research Engineering Co | Improved lubricating greases containing dihydroxy stearic acid soap |
NL91455C (en) * | 1952-10-16 | |||
FR1109884A (en) * | 1953-08-10 | 1956-02-02 | Bataafsche Petroleum | Fat compositions |
FR1113358A (en) * | 1953-10-05 | 1956-03-28 | Bataafsche Petroleum | Fat compositions |
US2905644A (en) * | 1956-07-24 | 1959-09-22 | Commercial Solvents Corp | Anticorrosion agent |
US2991247A (en) * | 1957-12-18 | 1961-07-04 | Kurt R Fisch | Process for forming a semifluid grease involving cooling to a subzero temperature |
NL110177C (en) * | 1958-03-05 | |||
FR1226563A (en) * | 1959-02-20 | 1960-07-13 | Exxon Standard Sa | Improved fats |
DE1271882B (en) * | 1960-07-01 | 1968-07-04 | Chem Fab Hoesch K G | Lithium soap grease |
US5595965A (en) * | 1996-05-08 | 1997-01-21 | The Lubrizol Corporation | Biodegradable vegetable oil grease |
US5858934A (en) * | 1996-05-08 | 1999-01-12 | The Lubrizol Corporation | Enhanced biodegradable vegetable oil grease |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2397956A (en) * | 1943-01-15 | 1946-04-09 | Internat Lubricant Corp | Production of lubricants |
US2403104A (en) * | 1942-10-17 | 1946-07-02 | Union Oil Co | Lithium greases |
US2450219A (en) * | 1945-04-10 | 1948-09-28 | Texas Co | Texture-stable lithium base grease |
US2450255A (en) * | 1945-04-17 | 1948-09-28 | Texas Co | Method of preparing lithium base greases |
US2450220A (en) * | 1945-05-03 | 1948-09-28 | Texas Co | Texture-stable lithium base grease |
US2475589A (en) * | 1947-04-18 | 1949-07-12 | Shell Dev | Lubricating grease composition |
-
0
- NL NL137009D patent/NL137009C/xx active
- NL NL66982D patent/NL66982C/xx active
- NL NL66799D patent/NL66799C/xx active
- NL NL73006D patent/NL73006C/xx active
-
1940
- 1940-04-05 US US328095A patent/US2274673A/en not_active Expired - Lifetime
-
1947
- 1947-07-30 FR FR1090381D patent/FR1090381A/en not_active Expired
- 1947-08-05 GB GB21283/47A patent/GB637932A/en not_active Expired
- 1947-08-07 CH CH269511D patent/CH269511A/en unknown
-
1948
- 1948-01-09 GB GB722/48A patent/GB643536A/en not_active Expired
- 1948-10-02 DE DEP14700D patent/DE842108C/en not_active Expired
- 1948-10-12 DE DEN32A patent/DE886948C/en not_active Expired
-
1949
- 1949-07-05 US US103164A patent/US2566793A/en not_active Expired - Lifetime
Cited By (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2451039A (en) * | 1941-12-24 | 1948-10-12 | Standard Oil Dev Co | Lubricant |
US2432577A (en) * | 1942-05-02 | 1947-12-16 | Patterson | Smoke screen composition |
US2553568A (en) * | 1943-02-25 | 1951-05-22 | Finkelstein Leo | Incendiary filling for bombs |
US2417264A (en) * | 1944-01-01 | 1947-03-11 | Standard Oil Dev Co | Lubricant |
US2443378A (en) * | 1944-07-08 | 1948-06-15 | Du Pont | Chemical process and product |
US2450219A (en) * | 1945-04-10 | 1948-09-28 | Texas Co | Texture-stable lithium base grease |
US2446177A (en) * | 1945-06-21 | 1948-08-03 | George M Hain | Silicone grease and method of preparation |
US2451895A (en) * | 1946-06-08 | 1948-10-19 | Shell Dev | Synthetic grease |
US2489281A (en) * | 1947-04-04 | 1949-11-29 | California Research Corp | Methacrylates in constant viscosity oils |
US2468099A (en) * | 1947-10-01 | 1949-04-26 | Standard Oil Dev Co | High-temperature grease |
US2491028A (en) * | 1947-10-11 | 1949-12-13 | Standard Oil Dev Co | Lubricating grease compositions |
US2577706A (en) * | 1948-11-26 | 1951-12-04 | California Research Corp | High melting-high water-resistant grease |
US2681313A (en) * | 1950-02-20 | 1954-06-15 | California Research Corp | Alkyl orthosilicate and alkoxysiloxane base grease compositions |
US2623017A (en) * | 1950-08-03 | 1952-12-23 | Phillips Petroleum Co | Gel-type grease |
US2696470A (en) * | 1951-03-01 | 1954-12-07 | Standard Oil Dev Co | Lubricating greases thickened with carbon black |
US2737494A (en) * | 1952-09-27 | 1956-03-06 | Socony Mobil Oil Co Inc | Stable greases containing synthetic gelling agents |
US2719124A (en) * | 1953-05-15 | 1955-09-27 | Exxon Research Engineering Co | Grease compositions containing oxonated acid soaps |
US4027070A (en) * | 1974-03-08 | 1977-05-31 | Nippon Steel Corporation | Steel plate for preparing cans by ironing |
Also Published As
Publication number | Publication date |
---|---|
GB637932A (en) | 1950-05-31 |
FR1090381A (en) | 1955-03-30 |
DE886948C (en) | 1953-08-20 |
GB643536A (en) | 1950-09-20 |
NL66799C (en) | |
DE842108C (en) | 1952-06-23 |
CH269511A (en) | 1950-07-15 |
NL73006C (en) | |
NL137009C (en) | |
NL66982C (en) | |
US2566793A (en) | 1951-09-04 |
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