US1902922A - Apparatus for dry-spinning artificial textile fibers with recovery of the volatile solvents - Google Patents
Apparatus for dry-spinning artificial textile fibers with recovery of the volatile solvents Download PDFInfo
- Publication number
- US1902922A US1902922A US306940A US30694028A US1902922A US 1902922 A US1902922 A US 1902922A US 306940 A US306940 A US 306940A US 30694028 A US30694028 A US 30694028A US 1902922 A US1902922 A US 1902922A
- Authority
- US
- United States
- Prior art keywords
- cell
- spinning
- solvent
- dry
- recovery
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000002904 solvent Substances 0.000 title description 40
- 238000000578 dry spinning Methods 0.000 title description 15
- 238000011084 recovery Methods 0.000 title description 14
- 239000004753 textile Substances 0.000 title description 13
- 239000000835 fiber Substances 0.000 title description 12
- 210000004027 cell Anatomy 0.000 description 44
- 238000009987 spinning Methods 0.000 description 32
- 239000000243 solution Substances 0.000 description 16
- 238000001816 cooling Methods 0.000 description 9
- 238000009833 condensation Methods 0.000 description 8
- 230000005494 condensation Effects 0.000 description 8
- 238000010438 heat treatment Methods 0.000 description 6
- 238000000034 method Methods 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 239000008246 gaseous mixture Substances 0.000 description 4
- 239000007788 liquid Substances 0.000 description 3
- 239000012267 brine Substances 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 2
- 229920002955 Art silk Polymers 0.000 description 1
- 210000000712 G cell Anatomy 0.000 description 1
- 239000000020 Nitrocellulose Substances 0.000 description 1
- SMEGJBVQLJJKKX-HOTMZDKISA-N [(2R,3S,4S,5R,6R)-5-acetyloxy-3,4,6-trihydroxyoxan-2-yl]methyl acetate Chemical compound CC(=O)OC[C@@H]1[C@H]([C@@H]([C@H]([C@@H](O1)O)OC(=O)C)O)O SMEGJBVQLJJKKX-HOTMZDKISA-N 0.000 description 1
- 229940081735 acetylcellulose Drugs 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 229920002301 cellulose acetate Polymers 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 230000006854 communication Effects 0.000 description 1
- 235000019628 coolness Nutrition 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229920001220 nitrocellulos Polymers 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
- 238000004804 winding Methods 0.000 description 1
Images
Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/04—Dry spinning methods
Definitions
- the object of the present invention is to obviate the aforesaid drawbacks, or at least to restrict the cooling and'subsequent heating of the gaseous mixture present in the cell to I a'small. quantity thereof.
- the invention which enables the spinning to be conducted in closed cells, renders it unnecessary to remove and cool the gaseous mixture which fills the spinningjcell, byproviding a limited surface wvhich is cooled to an adequate degree, in the spinning cell itself. This temperature should be so calculated that it does not exceed 40 the temperature of the spinning cell (measured in the immediate vicinity of the filament) and is, in any event, below'the boiling pointrof the solvent or solvents;
- Fig.1 is a diagrammatic vertical section.
- the jackets'p'ace B enables thespinning cell A to be warmed by means of hot air, hot; Water or steam.
- the cell are disposed one or more tubes C through which cold water orbrine is circa lated for cooling purposes.
- V 'As' already mentioned the vaportension of the s'olvent'vapors formed during the spin ni'ng process tends to attain the value cor- I
- Fig. 3 is a similar view bf anothermodifi'caso I responding to thetemperature of the cooling 'device. fThe cooling, water or brine enters the. tube Czat C" and issuestherefrom atE.
- the a paratu's may, of course, vary in de-- signs T us,in Fig; 2 thecooler consist'sof a'* plain tube C through which water or brine fis circulating.
- the condensed solvents collect in p the lowermost part "of the spinning cell, and are drawn oil through the the invention as cla ms- I V I I heating coils, electrical resistance and so forth, without departing fromthe scope of the invention;
- Fig. 3 represents still another embodiment.
- the cooler is confined to the lowermost part of the cell.
- the upper part is heated by the liquid circulating in the heating acket B, which it enters at T and leaves at
- the lower part is cooled by the cooling jacket B through'which water or brineat a suitable temperature is circulated.
- This latter arrangement insures a quiescent filament during the spinning process, since the gentle currents resulting from the sinking of the vapors from the hot to the coldlzone of the cell facilitate the spinning process itself.
- the solvents recovered in this manner are in a high state of purity, and can be used again without intermediate distillation.
- a spining cell for use in dry-spinning 'artificial textile fibers with recovery of the solvent .cont-ained in the spinning solution having, in combination, means for heating the cell, and meansin thecell for condensingsolvent vapors.
- solvent containedfin the spinning solution having, in combinatiom'means torheating V the upper portion "of the .cell,means for cooling the lower portion of the cell to'the temperature I of condensation of the solvent artificial textile fibers with solvent contained in the spinning solution,
- vapors within the cell and means including a siphon for collecting and withdrawing the condensate from the cell.
- V i I 15 A process of dry spinning artificial silk including continuous extrusion of a spinning solution into a cell, continuously passing over the filament thus formed a heated gas in which the solvent evaporates, and;
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Textile Engineering (AREA)
- Spinning Methods And Devices For Manufacturing Artificial Fibers (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
IT309158X | 1928-04-07 |
Publications (1)
Publication Number | Publication Date |
---|---|
US1902922A true US1902922A (en) | 1933-03-28 |
Family
ID=11232770
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US306940A Expired - Lifetime US1902922A (en) | 1928-04-07 | 1928-09-19 | Apparatus for dry-spinning artificial textile fibers with recovery of the volatile solvents |
Country Status (5)
Country | Link |
---|---|
US (1) | US1902922A (en(2012)) |
BE (1) | BE353940A (en(2012)) |
DE (1) | DE489964C (en(2012)) |
FR (1) | FR658700A (en(2012)) |
GB (1) | GB309158A (en(2012)) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2451854A (en) * | 1944-06-15 | 1948-10-19 | Du Pont | Dry spinning apparatus |
US2472842A (en) * | 1942-08-25 | 1949-06-14 | Rhodiaceta | Apparatus and method of dry spinning vinyl compounds |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
NL105057C (en(2012)) * | 1957-04-30 |
-
0
- BE BE353940D patent/BE353940A/xx unknown
-
1928
- 1928-05-03 DE DES85354D patent/DE489964C/de not_active Expired
- 1928-08-08 FR FR658700D patent/FR658700A/fr not_active Expired
- 1928-09-17 GB GB26607/28A patent/GB309158A/en not_active Expired
- 1928-09-19 US US306940A patent/US1902922A/en not_active Expired - Lifetime
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2472842A (en) * | 1942-08-25 | 1949-06-14 | Rhodiaceta | Apparatus and method of dry spinning vinyl compounds |
US2451854A (en) * | 1944-06-15 | 1948-10-19 | Du Pont | Dry spinning apparatus |
Also Published As
Publication number | Publication date |
---|---|
BE353940A (en(2012)) | |
FR658700A (fr) | 1929-06-07 |
DE489964C (de) | 1930-01-23 |
GB309158A (en) | 1930-01-29 |
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