US1901007A - Process of treating artificial fibers - Google Patents

Process of treating artificial fibers Download PDF

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Publication number
US1901007A
US1901007A US408547A US40854729A US1901007A US 1901007 A US1901007 A US 1901007A US 408547 A US408547 A US 408547A US 40854729 A US40854729 A US 40854729A US 1901007 A US1901007 A US 1901007A
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US
United States
Prior art keywords
bunch
fibers
bath
artificial fibers
fiber
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US408547A
Inventor
Stuhlmann Hans Caesar
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
IG Farbenindustrie AG
Original Assignee
IG Farbenindustrie AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by IG Farbenindustrie AG filed Critical IG Farbenindustrie AG
Application granted granted Critical
Publication of US1901007A publication Critical patent/US1901007A/en
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Expired - Lifetime legal-status Critical Current

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Classifications

    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F2/00Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof
    • D01F2/06Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof from viscose
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D10/00Physical treatment of artificial filaments or the like during manufacture, i.e. during a continuous production process before the filaments have been collected
    • D01D10/04Supporting filaments or the like during their treatment
    • D01D10/0418Supporting filaments or the like during their treatment as cakes or similar coreless thread packages
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D10/00Physical treatment of artificial filaments or the like during manufacture, i.e. during a continuous production process before the filaments have been collected
    • D01D10/04Supporting filaments or the like during their treatment
    • D01D10/0436Supporting filaments or the like during their treatment while in continuous movement
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D5/00Formation of filaments, threads, or the like
    • D01D5/12Stretch-spinning methods
    • D01D5/16Stretch-spinning methods using rollers, or like mechanical devices, e.g. snubbing pins
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/70Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment combined with mechanical treatment

Definitions

  • the present invention relates to a process of treating bunches of artificial fibers in a continuous manner in the course of their manufacture and more particularly to an after-treatment of artificial fiber imnches of high total titer on their way from. the precipitating bath to the collecting device.
  • bunches of artificial fibers of high total titer and astonishingly good physical properties are obtainable in the viscose spinning process by subjecting the freshly produced fibers collected to form a bunch in the acid moist state, that is, when leaving the precipitating bath, to a tension as high as possible, and by passing them simultaneously through a hot water bath before the usual washing operations and after-treatments take place.
  • My new operation may be performed in the following manner:
  • a fiber bunch having a total titer of, for instance, 10,000 to 100,000 deniers is formed by collecting the fibers which are produced by a correspondent plurality of spinning nozzles in a viscose spinning process.
  • the freshly produced and consequently acidmoist fiber bunch is passed through a trough having a len th of about 2 to 12 meters, but preferably of 5 meters and being filled with water kept at-a temperature of about 70 to 100 (1, care being taken that the fiber bunch is completely beneath the surface of the hot water.
  • the speed with which the fiber bunch is guided through the bath may vary between 40 to 60 meters per minute.
  • the speed is dependent from the length of the water bath.
  • the stretching of the bunches in the water bath may be performed in any known manner, for instance by causing them to run over rods or rolls so that they form an angle on their way or by (guiding them over a lurality of rollers of i eral velocity.
  • the single fibers of the bunch have for instance a titer of 1.4 denier-s and a dry tenacity of about 1 grams and a wet tenacity of about 2 grams, while fibers treated in a hot waterbath without tension show a dry tenacity of 2.9 grams and a wet tenacity of 1.2 grams. Furthermore, the material obtained according to my process shows an extremely good luster,
  • the process which comprises treat' in a continuous manner bunches of artificia fibers obtainable by precipitating a viscose solution in an acid precipitating bath in an acid-moist state with hot water, and simultaneously stretching the fibers.
  • the recess which comprises collecting artificial bers made from a viscose solution leayin the precipitating bath to fo a bunch o a total titer of about 40,000 to 100,000 deniers, passing the bunch through a water bath of a-length of-about 2 to 12 meters bei lrept at a temperature of about 7 0 to 100 40 to 60' meters r minute, and subj the bunch sim taneously to a tension 0 about 0.5 to 0.8 hlograms r square meter.

Description

Patented Mar. 14, 1933 UNITED STATES OFFICE HANS CAESAR STUHLHANN, OF FREHNITZ, GIEHZHANY, ASEIGNOE "1'0 1., G. FWENDT- DUSTBIE AKTIENGESELLSCHAFT, 0F FRANKFOBT-OH-THE-MH, GERMANY PROCESS OF TREzlflJENG ARTH'KCIAL WWW Ho Drawing. Application filed October 05,, 1000,, {Serial 1%. 013,547, and infiermany November 16, 1928.
The present invention relates to a process of treating bunches of artificial fibers in a continuous manner in the course of their manufacture and more particularly to an after-treatment of artificial fiber imnches of high total titer on their way from. the precipitating bath to the collecting device.
According to my invention bunches of artificial fibers of high total titer and astonishingly good physical properties are obtainable in the viscose spinning process by subjecting the freshly produced fibers collected to form a bunch in the acid moist state, that is, when leaving the precipitating bath, to a tension as high as possible, and by passing them simultaneously through a hot water bath before the usual washing operations and after-treatments take place.
My new operation may be performed in the following manner:
A fiber bunch having a total titer of, for instance, 10,000 to 100,000 deniers is formed by collecting the fibers which are produced by a correspondent plurality of spinning nozzles in a viscose spinning process. The freshly produced and consequently acidmoist fiber bunch is passed through a trough having a len th of about 2 to 12 meters, but preferably of 5 meters and being filled with water kept at-a temperature of about 70 to 100 (1, care being taken that the fiber bunch is completely beneath the surface of the hot water. Simultaneously I stretch the fiber by subjecting them to a high tension of, for instance, 0.5 to'0.8 kilograms per square millimeter The speed with which the fiber bunch is guided through the bath may vary between 40 to 60 meters per minute. Obviously, the speed is dependent from the length of the water bath. The stretching of the bunches in the water bath may be performed in any known manner, for instance by causing them to run over rods or rolls so that they form an angle on their way or by (guiding them over a lurality of rollers of i eral velocity.
bunch in a water bath of a fierent and adjusts le periphing a temperature of 70 to 100 (3,, and under the action of the high tension the fiber bunch soaked with the acid liquid of the precipitating bath is very quickly complete ly coagulated. The bunch of fibers then is desulfurized, bleached and finished in the usual manner. Thus very valuable products are obtainable. The single fibers of the bunch have for instance a titer of 1.4 denier-s and a dry tenacity of about 1 grams and a wet tenacity of about 2 grams, while fibers treated in a hot waterbath without tension show a dry tenacity of 2.9 grams and a wet tenacity of 1.2 grams. Furthermore, the material obtained according to my process shows an extremely good luster,
What I claim is:
1. The process which comprises treat' in a continuous manner bunches of artificia fibers obtainable by precipitating a viscose solution in an acid precipitating bath in an acid-moist state with hot water, and simultaneously stretching the fibers.
2. The
ing artificial fibers made from a viscose sola bunch of a total titer of a out $0,000 to 100,000 deniers, and treatin the acid-moist at 70 to 100 (1., and simultaneously stretching the fibers. 3. The recess which comprises collecting artificial bers made from a viscose solution leayin the precipitating bath to fo a bunch o a total titer of about 40,000 to 100,000 deniers, passing the bunch through a water bath of a-length of-about 2 to 12 meters bei lrept at a temperature of about 7 0 to 100 40 to 60' meters r minute, and subj the bunch sim taneously to a tension 0 about 0.5 to 0.8 hlograms r square meter.
ture.
The fiber bunch coming from the pre 0 cipitating bath is not coa lated through? out. Under the action of t e hot liquid havrocess which comprises collectwlth a drawing speed of about u In testimony whereof, afix my signaution leaving the precipitatin bath to form
US408547A 1928-11-16 1929-10-25 Process of treating artificial fibers Expired - Lifetime US1901007A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DEI0036103 1928-11-16

Publications (1)

Publication Number Publication Date
US1901007A true US1901007A (en) 1933-03-14

Family

ID=25821711

Family Applications (1)

Application Number Title Priority Date Filing Date
US408547A Expired - Lifetime US1901007A (en) 1928-11-16 1929-10-25 Process of treating artificial fibers

Country Status (7)

Country Link
US (1) US1901007A (en)
AT (1) AT123384B (en)
CH (1) CH142976A (en)
DE (1) DE507351C (en)
FR (1) FR684965A (en)
GB (1) GB342027A (en)
NL (1) NL26404C (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE743851C (en) * 1940-04-12 1944-01-04 Deutsches Forschungsinstitut F Process for the production of cellulose threads from well-ripened viscose
DE749338C (en) * 1940-11-20 1944-12-19 Glanzstoff Ag Process for the production of artificial threads or fibers with increased strength from low-alkali viscose
DE851995C (en) * 1941-07-14 1952-10-09 Onderzoekings Inst Res Device for wet treatment of rayon threads in a continuous operation in barges
DE846147C (en) * 1943-01-21 1952-08-11 Glanzstoff Ag Process for the degassing of a freshly spun viscose thread cable intended for the production of rayon

Also Published As

Publication number Publication date
NL26404C (en) 1932-03-15
DE507351C (en) 1930-09-15
CH142976A (en) 1930-10-31
FR684965A (en) 1930-07-03
GB342027A (en) 1931-01-29
AT123384B (en) 1931-06-25

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