US131312A - Improvement in processes and apparatus for producing oils - Google Patents

Improvement in processes and apparatus for producing oils Download PDF

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US131312A
US131312A US131312DA US131312A US 131312 A US131312 A US 131312A US 131312D A US131312D A US 131312DA US 131312 A US131312 A US 131312A
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water
pipe
condenser
improvement
oil
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/06Flash distillation

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  • My invention relates, first, to a process in which a vapor caused to issue from pine wood is introduced into condensing water, to the surface'of which it, as a condensed body, by
  • Figure 1 is a vertical longitudinal section of the apparatus above named.
  • Fig. 2 is a sectional front view.
  • Fig. 3 is a top view of the condenser.
  • A is a cylindrical retort of any suitable contents, constructed of sheet or cast iron, and provided with a grate, a, front-hinged door b, and free discharge-openings and pipes c.
  • the retort is set in masonry A having an ordinary furnace or grate, A.
  • the pipes 0 leading from the retort enter the upper head of a condenser, B, extending downward some distance therein.
  • An open inflowing pipe is shown at d, attaching to a pump, hydrant, or other point from which cold water may enter the condenser under pressure.
  • An open outflowing pipe, d, leads from the condenser B to a separatingchamber and gasometer, G, the upper portion of this receptacle being the gasometer, and the lower the separating-chamber.
  • a pipe, f, rises from the gasometer leading to any desired point.
  • Two free discharge-pipes leading from the separating-chamber are represented by e e.
  • the condenser 13 having the pipes at and cl, combined with the separating-chamber and gasoineter 0 having the pipes e e and f, substantially as set forth, for the purposes specified.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Fats And Perfumes (AREA)

Description

J. D. STANLEY. Improvement in Process and Apparatus for P'rodycing Oils, &c. No, 131,312, Patented Sep.10,1872.
UNITE STATES" PAIN FFICE.
IMPROVEMENT IN PROCESSES AND APPARATUS FOR PRODUCING OILS, &:.
Specification forming part of Letters Patent No. 131,312, dated September 10, 1872.
To all whom it may concern:
Be it known that I, JAMES D. STANLEY, of the city of Baltimore and State of Maryland, have invented certain improvements in process and apparatus whereby oil is distilled from pine wood, and purified inflammable gas produced for purposes of illumination or otherwise, of which improvements the following is a specification; and I do hereby declare that in the same is contained a full, clear, and exact description of my said invention, reference being had to the accompanying drawing and to the letters of reference marked thereon.
My invention relates, first, to a process in which a vapor caused to issue from pine wood is introduced into condensing water, to the surface'of which it, as a condensed body, by
reason of its inferior specific gravity, arises in the form of oil the portion of the vapor not undergoing condensation "rising as an inflammable gas, purified by its passage through the condensing water. The process is completed by the separation of the floating oil and gas from the water and united acids, the oil passing into a separating-chamber, the gas into a gasometer, and the condensing water and acids passing or flowing off as waste. My invention relates, secondly, to certain improved apparatus hereinafter described, used in the above-named process.
In the accompanying drawing, forming a part of this specification, Figure 1 is a vertical longitudinal section of the apparatus above named. Fig. 2 is a sectional front view. Fig. 3 is a top view of the condenser.
Similar letters of reference indicate similar parts of the invention in all the figures.
A is a cylindrical retort of any suitable contents, constructed of sheet or cast iron, and provided with a grate, a, front-hinged door b, and free discharge-openings and pipes c. The retort is set in masonry A having an ordinary furnace or grate, A. The pipes 0 leading from the retort enter the upper head of a condenser, B, extending downward some distance therein. An open inflowing pipe is shown at d, attaching to a pump, hydrant, or other point from which cold water may enter the condenser under pressure. An open outflowing pipe, d, leads from the condenser B to a separatingchamber and gasometer, G, the upper portion of this receptacle being the gasometer, and the lower the separating-chamber. A pipe, f, rises from the gasometer leading to any desired point. Two free discharge-pipes leading from the separating-chamber are represented by e e.
The process of distilling and producing oil and purified inflammable gas by means of the apparatus herein described is as follows: Pinewood sticks are placed lengthwise upon the grate a of the retort. The door b is then closed and fire applied to the furnace A. Cold water is injected through the pipe d into the condenser B, overflowing through that 01 into the separating chamber 0, in turn issuing from it through the pipe 6. The pipes c are designed to extend below the level to which the water is allowed to rise within the condenser,
reaching a short distance below the overflowpipe 01. The vapor and acids generated and distilled from the heated wood enter the condenser B through the submerged pipes c, a portion of the vapor being condensed.- This condensed body rises as an oil to the surface of the water. The Watergby reason of its contact with the vapor, becomes heated, the heated water occupying with the oil the upper surface of the liquid, because specifically lighter than the cooler portion thereof. The warm water and floating oil flow together through the pipe (1 into the separating-chamber 0, when, again, because of the difierences in specific gravity existing between the oil and water, the former flows oif from the pipe 0, and the latter through that e. The necessity of providing a separating-chamber, G, is apparent. Otherwise condensation would soon cease by reason of the condensing water becoming warm. By the use of the pipe d and chamber 0 the warmed wateris continually displaced by cool water forced into the condenser B through the pipe d. The oil as it departs from the pipe e is entirely separated from the water. The acids from the wood unite with the water in the condenser and pass off with it as waste. That portion of the vapor not condensed issues with the oil and warm water from the condenser B through the pipe 01 into the gasometer formed of the upper portion of the separatingchamber O. This vapor is conveyed thence as an inflammable gas by means of the pipe fto any desired locality. The wood at the end of the process is removed from the retort in good condition as charcoal.
3. The condenser 13 having the pipes at and cl, combined with the separating-chamber and gasoineter 0 having the pipes e e and f, substantially as set forth, for the purposes specified.
In testimony whereof I have hereto subscribed my name in the city of Washington, this sixth day of August, in the year of our Lord eighteen hundred and seventy-two.
JAMES D. STANLEY.
Witnesses:
GEo. H. HOWARD, EDM. F. BROWN.
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