US125009A - Improvement in compounds for hardening bar-iron - Google Patents
Improvement in compounds for hardening bar-iron Download PDFInfo
- Publication number
- US125009A US125009A US125009DA US125009A US 125009 A US125009 A US 125009A US 125009D A US125009D A US 125009DA US 125009 A US125009 A US 125009A
- Authority
- US
- United States
- Prior art keywords
- iron
- compounds
- improvement
- hardening
- bar
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 150000001875 compounds Chemical class 0.000 title description 5
- 229910000754 Wrought iron Inorganic materials 0.000 title description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 12
- 229910052742 iron Inorganic materials 0.000 description 6
- 229910000831 Steel Inorganic materials 0.000 description 5
- 239000010959 steel Substances 0.000 description 5
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 2
- ZCCIPPOKBCJFDN-UHFFFAOYSA-N calcium nitrate Chemical compound [Ca+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ZCCIPPOKBCJFDN-UHFFFAOYSA-N 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Inorganic materials [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 2
- 235000010333 potassium nitrate Nutrition 0.000 description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 229910002651 NO3 Inorganic materials 0.000 description 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
- 235000008331 Pinus X rigitaeda Nutrition 0.000 description 1
- 235000011613 Pinus brutia Nutrition 0.000 description 1
- 241000018646 Pinus brutia Species 0.000 description 1
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 229910000366 copper(II) sulfate Inorganic materials 0.000 description 1
- JZCCFEFSEZPSOG-UHFFFAOYSA-L copper(II) sulfate pentahydrate Chemical compound O.O.O.O.O.[Cu+2].[O-]S([O-])(=O)=O JZCCFEFSEZPSOG-UHFFFAOYSA-L 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 235000006408 oxalic acid Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D1/00—General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
- C21D1/56—General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering characterised by the quenching agents
- C21D1/60—Aqueous agents
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M1/00—Liquid compositions essentially based on mineral lubricating oils or fatty oils; Their use as lubricants
- C10M1/08—Liquid compositions essentially based on mineral lubricating oils or fatty oils; Their use as lubricants with additives
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Thermal Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Mechanical Engineering (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Physics & Mathematics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Plural Heterocyclic Compounds (AREA)
Description
UNITED STATES PATENT OFFICE.
FRANKLIN E. BLAKE, OF MA'TTOON, ILLINOIS.
Specification forming part of Letters Patent No. 125,009, dated March 26, 1872.
' inyimprovement: Blue vitriol, oxalic acid, carbonate of ammonia, pure saltpeter, muriate of tin, (crystals,) equal parts.
Mode of Preparation.
Dissolve the chemicals in a (q. s.) suflicient quantity of ninety-six per cent. alcohol. After all is dissolved, put in pine sawdust, as much'as the solution will hold without dripping. Then pack the iron to be steelified with the compound in an iron case made perfectly air-tight by luting with fire-clay. Then put the case into a furnace and keep it at a cherry-red about thirty minutes, for steelifying the iron, after which let it cool gradually. This compound can be used a number of times and produce good results.
For case-hardening bar-iron, use the same material and process; and while red hot plunge the iron into the following compound, as follows: Three gallons of strong alkali; one pound saltpeter (nitrate of potassa); and muria-te of tin, one-quarter pound.
The sample of one-half-inch square ironth at accompanies this specification and drawing was broken before it was converted into steel, and shows the fibrous grain at the end; and
after going through the steelifying process it was broken off at the other end, and shows that the fibrous nature has been changed to crystal, and the whole piece converted into steel, that can be worked the same as any other steel.
The sample piece of iron one-half inch thick and one and one-quarter inch wide shows the case-hardening; and we claim that bar-iron case-hardened by this process can be heated and worked the same as steel, and has this advantage over all other case-hardening with which we are acquainted-of being tempered in water the same as English or bar-steel, without the trouble of re-case-hardening. This is a great advantage over other modes of casehardening, as other case-hardened work will spring and get out of shape. Again, iron casehardened by this process will not have any blisters, and will be strengthened considerable, thus making my invention of vast public utility.
Claim.
1 claim The compound herein described, with the privilege of varying the proportions of the ingredients named, so as always to produce the same results, substantially as or for the purpose herein set forth.
In testimony whereof I have signed myname to this specification in the presence of two subscribing witnesses.
FBAN KLIN E. BLAKE.
W'itn esses J. P. SoU'rHARD, E. O. FRINK.
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US125009A true US125009A (en) | 1872-03-26 |
Family
ID=2194438
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US125009D Expired - Lifetime US125009A (en) | Improvement in compounds for hardening bar-iron |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US125009A (en) |
-
0
- US US125009D patent/US125009A/en not_active Expired - Lifetime
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