US1036282A - Process of finishing, filling, loading, or dressing textile fabrics and spun goods. - Google Patents
Process of finishing, filling, loading, or dressing textile fabrics and spun goods. Download PDFInfo
- Publication number
- US1036282A US1036282A US65959411A US1911659594A US1036282A US 1036282 A US1036282 A US 1036282A US 65959411 A US65959411 A US 65959411A US 1911659594 A US1911659594 A US 1911659594A US 1036282 A US1036282 A US 1036282A
- Authority
- US
- United States
- Prior art keywords
- viscose
- cellulose
- finishing
- fabric
- loading
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000004744 fabric Substances 0.000 title description 21
- 238000000034 method Methods 0.000 title description 11
- 239000004753 textile Substances 0.000 title description 5
- 229920000297 Rayon Polymers 0.000 description 22
- 229920002678 cellulose Polymers 0.000 description 19
- 239000001913 cellulose Substances 0.000 description 19
- 239000003513 alkali Substances 0.000 description 10
- 239000002253 acid Substances 0.000 description 9
- 150000003839 salts Chemical class 0.000 description 7
- HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Inorganic materials [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 7
- 239000003518 caustics Substances 0.000 description 6
- 239000003795 chemical substances by application Substances 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 4
- 150000007513 acids Chemical class 0.000 description 4
- 239000000835 fiber Substances 0.000 description 4
- 238000005406 washing Methods 0.000 description 4
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- 150000001298 alcohols Chemical class 0.000 description 3
- 238000004040 coloring Methods 0.000 description 3
- 239000000470 constituent Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 235000011121 sodium hydroxide Nutrition 0.000 description 3
- 229920000742 Cotton Polymers 0.000 description 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 2
- 235000011187 glycerol Nutrition 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 2
- 239000000049 pigment Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 235000000346 sugar Nutrition 0.000 description 2
- 229910052725 zinc Inorganic materials 0.000 description 2
- 239000011701 zinc Substances 0.000 description 2
- 239000005995 Aluminium silicate Substances 0.000 description 1
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
- 241000651994 Curio Species 0.000 description 1
- DWAQJAXMDSEUJJ-UHFFFAOYSA-M Sodium bisulfite Chemical compound [Na+].OS([O-])=O DWAQJAXMDSEUJJ-UHFFFAOYSA-M 0.000 description 1
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
- 239000004902 Softening Agent Substances 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical compound OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 description 1
- RGCKGOZRHPZPFP-UHFFFAOYSA-N alizarin Chemical compound C1=CC=C2C(=O)C3=C(O)C(O)=CC=C3C(=O)C2=C1 RGCKGOZRHPZPFP-UHFFFAOYSA-N 0.000 description 1
- 235000012211 aluminium silicate Nutrition 0.000 description 1
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 description 1
- 229910052921 ammonium sulfate Inorganic materials 0.000 description 1
- 235000011130 ammonium sulphate Nutrition 0.000 description 1
- 239000010425 asbestos Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- IKCOOALACZVGLI-GNOQXXQHSA-K bis[[(z)-octadec-9-enoyl]oxy]alumanyl (z)-octadec-9-enoate Chemical compound [Al+3].CCCCCCCC\C=C/CCCCCCCC([O-])=O.CCCCCCCC\C=C/CCCCCCCC([O-])=O.CCCCCCCC\C=C/CCCCCCCC([O-])=O IKCOOALACZVGLI-GNOQXXQHSA-K 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 1
- 239000004359 castor oil Substances 0.000 description 1
- 235000019438 castor oil Nutrition 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 150000004677 hydrates Chemical class 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000001023 inorganic pigment Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000005517 mercerization Methods 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 150000007522 mineralic acids Chemical class 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- -1 or dressed threads Substances 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 239000012860 organic pigment Substances 0.000 description 1
- 235000011118 potassium hydroxide Nutrition 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 238000009877 rendering Methods 0.000 description 1
- 229910052895 riebeckite Inorganic materials 0.000 description 1
- 235000010267 sodium hydrogen sulphite Nutrition 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 229910052854 staurolite Inorganic materials 0.000 description 1
- 235000020357 syrup Nutrition 0.000 description 1
- 239000006188 syrup Substances 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
- D06M15/05—Cellulose or derivatives thereof
- D06M15/09—Cellulose ethers
Definitions
- a primary object of my invention is to remedy this defect.
- the viscose to be employed for finishing or dressing is made so rich in caustic alkalis that its percentage of caustic alkali is at least as great as its percentage of cellulose or cellulose hydrate.
- viscose very rich in alkali penetrates very deep into the textile fiber so that fabrics, or dressed threads, or fabrics made of such dressed threads finished with it by itself or mixed with other finishing or dressing agents, or with inorganic or organic loading materials or pigments or coloring matters by themselves .or mixed one with another, gain' exceedingly in touch, strength and Weight, and are not far removed in appearance from, or are equal in appearance Specification of Letters Patent.
- Viscose or viscose purified according to one of the well-known processes e. 9. those using salts, weak acids and salts, alcohols, weak acids and alcohols, other agents which withdraw water, bisulfite lye, sulfurous acid, carbonic acid and other weak acidsand the like, and possessing a percentage of alkali amounting at least to as much as its percentage of cellulose or cellulose hydrate, is applied by hand or by means of suitable -machines onto the fabric or spun goods to be finished or is incorporated therein. In order that the fibers may be penetrated still deeper this impregnation may take place in rarefied chambers or under an increased pressure.
- the viscose' may have added to it other finishing or dressing agents or loading materials, such as kaolin, oxid of zinc, asbestos, staurolite (Taufstein) and the like, or inorganic or organic pigments, e. g. lax, mineral colors and the like, or coloring mat ter, either by themselves or mixed one with another.
- finishing or dressing agents or loading materials such as kaolin, oxid of zinc, asbestos, staurolite (Taufstein) and the like, or inorganic or organic pigments, e. g. lax, mineral colors and the like, or coloring mat ter, either by themselves or mixed one with another.
- the abundance of caustic alkalis can be produced by providing therefor either when manufacturing the viscose, for example by converting the cellulose with the aid of suitably concentrated caustic potash solutions into alkali cellulose and adapting the pressure to which the same is subjected to the percentage of alkali which is finally desired and the like, or byadding to the finished viscose as much caustic alkali in a solid form or in solution as is desired for the purpose in view.
- the viscose is preferably rendered insoluble (regeneration of the cellulose or hydrocellulose) in known manner, that is to say by exposing the finished or dressed fabric or spun goods to actions which are capable of decomposin the viscose, cellulose or hydrocellulose beingformed.
- the following agents may be used: steam, dry
- the material may be, washed with only cold or hot water alone or subjected in addition to the washing process to a neutralizing process or one which removes the acid, to which end solutions of inorganic or organic acids or acid salts can be employed.
- This treatment with an acid or an acid salt can take place either before or after the washing process or between two washing operations.
- a softening agent such as glycerin, Turkey red oil, aluminium oleate, polyricinol acid, castor oil, sugar, syrup and thelike, are added to the mass described above in Example 1 or 2.
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Artificial Filaments (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Description
PROCESS OF FINISHING, FILLING,
\ tiuirnn smrns PATENT curios."
LEON LILIENFELD, OF VIENNA, AUSTRIA-HUNGARY.
No Drawing.
To all whom it may concern:
Be it known that I, LEON LILIENFELD,
' doctor, chemist, a subject of the Emperor of or pigments or coloring matter the difficulty is met with that the'cellulose or hydrocellulose which is regenerated from the viscose during its decomposition does notpenetrate sufliciently into the fibers themselves and consequently is too visible on the surface of the fabric and fills up the meshes of the fabric. The same holds good of threads dressed with viscose in the manner known heretofore, when the cellulose was also regenerated more on the surfacethan in the interior. The consequence is that the fabric or dressed threads or fabric made of dressed threads finished in the manner known heretofore with viscose alone or with viscose mixed with the above-mentioned substances partially or entirely loses or lose the appearance and touch of the natural, not finished fabric.
A primary object of my invention is to remedy this defect. Tothisend, the viscose to be employed for finishing or dressing is made so rich in caustic alkalis that its percentage of caustic alkali is at least as great as its percentage of cellulose or cellulose hydrate. I have found that viscose very rich in alkali penetrates very deep into the textile fiber so that fabrics, or dressed threads, or fabrics made of such dressed threads finished with it by itself or mixed with other finishing or dressing agents, or with inorganic or organic loading materials or pigments or coloring matters by themselves .or mixed one with another, gain' exceedingly in touch, strength and Weight, and are not far removed in appearance from, or are equal in appearance Specification of Letters Patent.
LOADING, OR DRESSING. TEXTILE FABRICS AND SPUN GOODS.
Patented Aug. 20, 1912.
Application filed November 10, 1911. Serial No. 659,594.
to, natural fabric or threads. According to my process it is possible to precipitate very large quantities of cellulose or cellulose hydrates in or on the fiber without considerable formation of superficial layers or layers filling up the meshes and impairing the fabric.
For carrying my process into practice crude Viscose or viscose purified according to one of the well-known processes, e. 9. those using salts, weak acids and salts, alcohols, weak acids and alcohols, other agents which withdraw water, bisulfite lye, sulfurous acid, carbonic acid and other weak acidsand the like, and possessing a percentage of alkali amounting at least to as much as its percentage of cellulose or cellulose hydrate, is applied by hand or by means of suitable -machines onto the fabric or spun goods to be finished or is incorporated therein. In order that the fibers may be penetrated still deeper this impregnation may take place in rarefied chambers or under an increased pressure. The viscose'may have added to it other finishing or dressing agents or loading materials, such as kaolin, oxid of zinc, asbestos, staurolite (Taufstein) and the like, or inorganic or organic pigments, e. g. lax, mineral colors and the like, or coloring mat ter, either by themselves or mixed one with another. The abundance of caustic alkalis can be produced by providing therefor either when manufacturing the viscose, for example by converting the cellulose with the aid of suitably concentrated caustic potash solutions into alkali cellulose and adapting the pressure to which the same is subjected to the percentage of alkali which is finally desired and the like, or byadding to the finished viscose as much caustic alkali in a solid form or in solution as is desired for the purpose in view.
If it is wished to avoid the shrinking of the fabric or spun goods occasioned by the percentage of alkali or to diminish the same, it is preferable to finish or dress the fabric or spun goods or to render the viscose insoluble, 2'. e. to regenerate the cellulose or hydrocellulose, or to liberate the same from impurities by lixiviation or to dry the fabric or spun goods while stretching the same.
The viscose is preferably rendered insoluble (regeneration of the cellulose or hydrocellulose) in known manner, that is to say by exposing the finished or dressed fabric or spun goods to actions which are capable of decomposin the viscose, cellulose or hydrocellulose beingformed. To this end the following agents may be used: steam, dry
heat, hot water; acids by themselves or mixed with glycerin, sugar and the like; acids and salts; salts alone, 6. g. ammonium sulfate, ammonium chlorid, sodium chlorid, sodium bisulfite and the like; salts of heavy metals; agents which withdraw-water, such as alcohols and the like. The goods which have been finished or dressed and in which the viscose has been rendered insoluble must then be liberated from the impurities due to the viscose. This is preferably done by a thorough washing process. The material may be, washed with only cold or hot water alone or subjected in addition to the washing process to a neutralizing process or one which removes the acid, to which end solutions of inorganic or organic acids or acid salts can be employed. This treatment with an acid or an acid salt can take place either before or after the washing process or between two washing operations. The
' alkali which passes into the water can be recovered by any process known in the art of mercerization or otherwise.
Examples.
1. 100 partsjby weight of a crude viscose containing 1015% cellulose and 3.54% caustic soda are mixed with 30 to 150 parts by weight of a soda lye of B. (50%), and a cotton fabric is finished with this mass on a suitable finishing-machine or a cotton thread is dressed on a suitable dressing-niachine. The treatment is completed according to one of the processes described above.
2. 10 to 20 parts by weight of china clay or oxid of zinc are added to the mass described in Example 1.
3. 10 to 20 parts by weight of a softening agent, such as glycerin, Turkey red oil, aluminium oleate, polyricinol acid, castor oil, sugar, syrup and thelike, are added to the mass described above in Example 1 or 2.
4. 10 to 20 parts by weight of'starch or this process is ,to use a viscose having a percentage ofcaustic alkali at least equal to the percentage of its cellulose constituent. I use the term cellulose as a generic term to include the substance which is .known by this name, and also for hydrocellulose.
What I claim as my invention and desire tosecure by Letters Patent is:
1. The herein described process of treat.-'
ing textile fabrics and spun goods, which consists in applying to the fabric a viscose possessing a percentage of caustic alkall at .least equal to the percentage of its cellulose constituent, and subsequently rendering the viscose insoluble.
2. The herein described process of treating textile fabrics and spun goods, which consists in applying to the fabric a viscose possessing a percentage of caustic alkali at least equal to the percentage of its cellulose constituent, and subsequently decomposing the viscose into cellulose, respectively hydrocellulose.
In testlmony whereof I have aflixed my signature in presence of two witnesses.
LEON LILIENFELD.
Witnesses:
FRANZ REITER, AUeUs'r FUGGER.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US65959411A US1036282A (en) | 1911-11-10 | 1911-11-10 | Process of finishing, filling, loading, or dressing textile fabrics and spun goods. |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US65959411A US1036282A (en) | 1911-11-10 | 1911-11-10 | Process of finishing, filling, loading, or dressing textile fabrics and spun goods. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US1036282A true US1036282A (en) | 1912-08-20 |
Family
ID=3104561
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US65959411A Expired - Lifetime US1036282A (en) | 1911-11-10 | 1911-11-10 | Process of finishing, filling, loading, or dressing textile fabrics and spun goods. |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US1036282A (en) |
Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2432091A (en) * | 1947-12-09 | Method of making cleansing pads | ||
| US2482042A (en) * | 1945-03-21 | 1949-09-13 | Montclair Res Corp | Oxycellulose products, their manufacture and utilization |
| US2689194A (en) * | 1952-02-18 | 1954-09-14 | Sayles Finishing Plants Inc | Finishing process and fabric |
| US2910380A (en) * | 1955-10-13 | 1959-10-27 | Union Carbide Corp | Method of making seamless viscoseregenerated cellulose tubing |
| WO1998002366A1 (en) | 1996-07-17 | 1998-01-22 | Alfacel S.A. | Packaging of shirred food casing |
| WO1998004140A1 (en) | 1996-07-31 | 1998-02-05 | Alfacel S.A. | Adjustable reaction tubs for cellulose |
| WO1998008393A1 (en) | 1996-08-27 | 1998-03-05 | Alfacel S.A. | Method to slowly regenerate cellulosic sausage casing |
| US5736087A (en) * | 1996-10-30 | 1998-04-07 | Alfacel S.A. | Method for finishing of sausage casings |
| WO1998016114A2 (en) | 1996-10-15 | 1998-04-23 | Alfacel S.A. | Shirred food casing end system |
| US5773035A (en) * | 1996-07-01 | 1998-06-30 | Alfacel S.A. | Tubular cellulosic casing die |
| US5776398A (en) * | 1997-01-15 | 1998-07-07 | Alfacel S.A. | Method of regenerating sausage casing |
| US5782683A (en) * | 1996-08-27 | 1998-07-21 | Alfacel S.A. | Cold temperature shirring |
| US5795523A (en) * | 1996-10-30 | 1998-08-18 | Alfacel S.A. | Method for treatment of CS2 and H2 S emissions during viscose regeneration |
| US5914141A (en) * | 1997-03-11 | 1999-06-22 | Alfacel S.A. | Easy peeling wiener casings via use of enzymes |
-
1911
- 1911-11-10 US US65959411A patent/US1036282A/en not_active Expired - Lifetime
Cited By (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2432091A (en) * | 1947-12-09 | Method of making cleansing pads | ||
| US2482042A (en) * | 1945-03-21 | 1949-09-13 | Montclair Res Corp | Oxycellulose products, their manufacture and utilization |
| US2689194A (en) * | 1952-02-18 | 1954-09-14 | Sayles Finishing Plants Inc | Finishing process and fabric |
| US2910380A (en) * | 1955-10-13 | 1959-10-27 | Union Carbide Corp | Method of making seamless viscoseregenerated cellulose tubing |
| US5773035A (en) * | 1996-07-01 | 1998-06-30 | Alfacel S.A. | Tubular cellulosic casing die |
| WO1998002366A1 (en) | 1996-07-17 | 1998-01-22 | Alfacel S.A. | Packaging of shirred food casing |
| US5865312A (en) * | 1996-07-17 | 1999-02-02 | Alfacel S.A | Packaging of shirred food casing |
| US5741529A (en) * | 1996-07-31 | 1998-04-21 | Alfacel S.A. | Adjustable reaction tubs for cellulose |
| WO1998004140A1 (en) | 1996-07-31 | 1998-02-05 | Alfacel S.A. | Adjustable reaction tubs for cellulose |
| WO1998008393A1 (en) | 1996-08-27 | 1998-03-05 | Alfacel S.A. | Method to slowly regenerate cellulosic sausage casing |
| US5782683A (en) * | 1996-08-27 | 1998-07-21 | Alfacel S.A. | Cold temperature shirring |
| US5783131A (en) * | 1996-08-27 | 1998-07-21 | Alfacel S.A. | Method to slowly regenerate cellulosic sausage casing |
| WO1998016114A2 (en) | 1996-10-15 | 1998-04-23 | Alfacel S.A. | Shirred food casing end system |
| US5897432A (en) * | 1996-10-15 | 1999-04-27 | Alfacel S.A. | Shirred food casing end system |
| US5736087A (en) * | 1996-10-30 | 1998-04-07 | Alfacel S.A. | Method for finishing of sausage casings |
| US5795523A (en) * | 1996-10-30 | 1998-08-18 | Alfacel S.A. | Method for treatment of CS2 and H2 S emissions during viscose regeneration |
| US5776398A (en) * | 1997-01-15 | 1998-07-07 | Alfacel S.A. | Method of regenerating sausage casing |
| US5914141A (en) * | 1997-03-11 | 1999-06-22 | Alfacel S.A. | Easy peeling wiener casings via use of enzymes |
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