UA83096C2 - Порошкоподібний діоксид титану та спосіб його одержання полуменевим гідролізом - Google Patents

Порошкоподібний діоксид титану та спосіб його одержання полуменевим гідролізом

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Publication number
UA83096C2
UA83096C2 UAA200607230A UAA200607230A UA83096C2 UA 83096 C2 UA83096 C2 UA 83096C2 UA A200607230 A UAA200607230 A UA A200607230A UA A200607230 A UAA200607230 A UA A200607230A UA 83096 C2 UA83096 C2 UA 83096C2
Authority
UA
Ukraine
Prior art keywords
titanium dioxide
steam
solid
primary
preparation
Prior art date
Application number
UAA200607230A
Other languages
English (en)
Russian (ru)
Inventor
Каі Шумахер
Андреас Шільд
Мартін Мьортерс
Original Assignee
Дегусса Аг
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE102004055165A external-priority patent/DE102004055165A1/de
Application filed by Дегусса Аг filed Critical Дегусса Аг
Publication of UA83096C2 publication Critical patent/UA83096C2/uk

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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/04—Oxides; Hydroxides
    • C01G23/047—Titanium dioxide
    • C01G23/07—Producing by vapour phase processes, e.g. halide oxidation
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/29—Titanium; Compounds thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/063—Titanium; Oxides or hydroxides thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
    • B01J35/39—Photocatalytic properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0238—Impregnation, coating or precipitation via the gaseous phase-sublimation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B01J37/10—Heat treatment in the presence of water, e.g. steam
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82B—NANOSTRUCTURES FORMED BY MANIPULATION OF INDIVIDUAL ATOMS, MOLECULES, OR LIMITED COLLECTIONS OF ATOMS OR MOLECULES AS DISCRETE UNITS; MANUFACTURE OR TREATMENT THEREOF
    • B82B1/00—Nanostructures formed by manipulation of individual atoms or molecules, or limited collections of atoms or molecules as discrete units
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20—Oxides; Hydroxides
    • C08K3/22—Oxides; Hydroxides of metals
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K3/00—Materials not provided for elsewhere
    • C09K3/14—Anti-slip materials; Abrasives
    • C09K3/1409—Abrasive particles per se
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/613—10-100 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/615—100-500 m2/g
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/10—Solid density
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Nanotechnology (AREA)
  • Inorganic Chemistry (AREA)
  • Public Health (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Geology (AREA)
  • Environmental & Geological Engineering (AREA)
  • Physics & Mathematics (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Birds (AREA)
  • Composite Materials (AREA)
  • Epidemiology (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Dermatology (AREA)
  • Thermal Sciences (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Catalysts (AREA)
  • Cosmetics (AREA)

Abstract

У заявці описаний одержаний полуменевим гідролізом порошкоподібний діоксид титану, який знаходиться у вигляді агрегатів первинних частинок і має площу поверхні БЕТ, що дорівнює від 20 до 200 м2/г, напівширину (НШ) [нм] розподілу первинних частинок, НШ [нм]=а EMBED Equation.3 БЕТf, де а=670 EMBED Equation.3 10-9м3/г та -1,3 EMBED Equation.3 f EMBED Equation.3 -1,0, і частку частинок, які мають діаметр, більший за 45 мкм, що знаходиться в діапазоні від 0,0001 до 0,05 мас.%. Порошок одержують способом, у якому галогенід титану випарюють при температурі нижче 200°С, пару подають у камеру змішування за допомогою газу-носія, який має задану вологість, і незалежно від цього водень, первинне повітря, яке необов’язково може бути збагачене киснем і/або попередньо підігріте, і пару подають у камеру змішування, потім реакційну суміш спалюють у реакційній камері, яка захищена від доступу повітря навколишнього середовища, у реакційну камеру додатково подають вторинне повітря, після чого тверду речовину відокремлюють від газоподібних речовин, і потім тверду речовину обробляють парою. Цей порошкоподібний діоксид титану можна застосовувати для термостабілізації полімерів.
UAA200607230A 2003-12-03 2004-11-24 Порошкоподібний діоксид титану та спосіб його одержання полуменевим гідролізом UA83096C2 (uk)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE10357508 2003-12-03
DE102004055165A DE102004055165A1 (de) 2003-12-03 2004-11-16 Flammenhydrolytisch hergestelltes Titandioxidpulver
PCT/EP2004/013317 WO2005054136A1 (en) 2003-12-03 2004-11-24 Flame-hydrolytically produced titanium dioxide powder

Publications (1)

Publication Number Publication Date
UA83096C2 true UA83096C2 (uk) 2008-06-10

Family

ID=34654860

Family Applications (1)

Application Number Title Priority Date Filing Date
UAA200607230A UA83096C2 (uk) 2003-12-03 2004-11-24 Порошкоподібний діоксид титану та спосіб його одержання полуменевим гідролізом

Country Status (7)

Country Link
US (1) US7686881B2 (uk)
EP (1) EP1697260B1 (uk)
JP (1) JP4445972B2 (uk)
KR (1) KR100712157B1 (uk)
RU (1) RU2344994C2 (uk)
UA (1) UA83096C2 (uk)
WO (1) WO2005054136A1 (uk)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5241994B2 (ja) * 2004-11-05 2013-07-17 戸田工業株式会社 酸化チタン粒子粉末及び光触媒
US20070141320A1 (en) * 2005-12-21 2007-06-21 Shulong Li Substrate having photocatalytic and activated carbon constituents and process for producing
TWI405610B (zh) * 2006-12-13 2013-08-21 Worthington Technologies Llc 高光敏性二氧化鈦及其形成方法
US7468175B2 (en) * 2006-12-13 2008-12-23 Worthington Technologies, Llc Highly photosensitive titanium dioxide and process for forming the same
DE102007010212A1 (de) * 2007-02-28 2008-09-04 Evonik Degussa Gmbh Polymere
ATE465976T1 (de) * 2007-05-22 2010-05-15 Evonik Degussa Gmbh Titandioxid mit erhöhter sinteraktivität
EP1997781B1 (de) 2007-05-22 2014-07-16 Evonik Degussa GmbH Verfahren zur Herstellung von Titandioxid mit variabler Sinteraktivität
TWI487668B (zh) * 2009-02-19 2015-06-11 Sakai Chemical Industry Co 金紅石型氧化鈦粒子之分散體，其製造方法，及其用途
GB0922552D0 (en) * 2009-12-23 2010-02-10 Croda Int Plc Particulate titanium dioxide
WO2015003871A1 (de) * 2013-07-11 2015-01-15 Evonik Industries Ag Verfahren zur herstellung von metalloxiden
EP3019269B1 (de) * 2013-07-11 2018-08-08 Evonik Degussa GmbH Verfahren zur herstellung von kieselsäure mit variabler verdickung
RU2539582C1 (ru) * 2013-12-23 2015-01-20 Федеральное Государственное Автономное Образовательное Учреждение Высшего Профессионального Образования "Дальневосточный Федеральный Университет" (Двфу) Способ получения диоксида титана
EP4064386A1 (en) 2021-03-24 2022-09-28 Evonik Operations GmbH Core-shell particles based on red lead for lead-acid batteries

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US4048290A (en) * 1976-01-28 1977-09-13 Cabot Corporation Process for the production of finely-divided metal and metalloid oxides
DE3840196C1 (uk) * 1988-11-29 1990-04-12 Bayer Ag, 5090 Leverkusen, De
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Also Published As

Publication number Publication date
EP1697260B1 (en) 2012-07-11
RU2344994C2 (ru) 2009-01-27
JP2007515368A (ja) 2007-06-14
US7686881B2 (en) 2010-03-30
WO2005054136A1 (en) 2005-06-16
RU2006123435A (ru) 2008-01-20
KR20060086451A (ko) 2006-07-31
KR100712157B1 (ko) 2007-05-02
EP1697260A1 (en) 2006-09-06
JP4445972B2 (ja) 2010-04-07
US20070144076A1 (en) 2007-06-28

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