TW414814B - Measure-device and measure-method for the orientation-degree of a fiber - Google Patents

Measure-device and measure-method for the orientation-degree of a fiber Download PDF

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TW414814B
TW414814B TW88119053A TW88119053A TW414814B TW 414814 B TW414814 B TW 414814B TW 88119053 A TW88119053 A TW 88119053A TW 88119053 A TW88119053 A TW 88119053A TW 414814 B TW414814 B TW 414814B
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Taiwan
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fiber
light
optical path
machine
path difference
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TW88119053A
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Chinese (zh)
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Akira Uragami
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Kanebo Ltd
Kanebo Eng Kk
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Abstract

The purpose of this invention is to provide a measure-device and a measure-method, which can measure easily and in wide range the orientation-degree of a synthesized-filament fiber. Said measure-device for the orientation-degree of a fiber is composed of: a light-source mechanism which can emit the white light; an observation mechanism which can observe said emitted light; a stage-compensation mechanism which is arranged between said light-source mechanism and said fiber, the four mechanisms of a continuous compensation mechanism which is arranged between the observation mechanism and said fiber.

Description

年q屬姜efi#良4灸正/補充 A7 五、發明說明U ) 用具1/4又光程差的、設置在上逑方位中之轉換機構(51) ,將其轉換為直線徧光。經如此轉換過的直線偏光之偏 光方向是從旋轉偏振Μ ( 5 2 >的基準點徧移0度。因而, 將旋轉偏振片(52)轉動0度,就與偏光方向成為正交, 而可補償殘留光程差。 其次,將使用具如上逑構成的測定裝置,以測定定向 度之方法予以說明。先說明對於圓形斷面的纖維之測定 方法,其後再説明任意斷面的纖維之測定方法。 首先,將合成纖維絲的定向度定義為纖維的長度方向 與粗細度方向的折射率之差(以下稱雙折射率)之後,再 將所定義的雙折射率變形為可由本測定裝置所測定的形 式之定義式之事,予以說明。Year q belongs to ginger efi # 良 4 moxibustion plus / supplement A7 V. Description of the invention U) A conversion mechanism (51) with a 1/4 light path difference and set in the upper position, converts it into a straight line of light. The polarization direction of the linearly polarized light thus converted is shifted by 0 degrees from the reference point of the rotation polarization M (5 2 >. Therefore, if the rotation polarization plate (52) is rotated by 0 degrees, it is orthogonal to the polarization direction, and Residual optical path difference can be compensated. Next, a method for measuring the degree of orientation will be described using a measuring device having the structure described above. The method for measuring a fiber with a circular cross section will be described first, and then the fiber with an arbitrary cross section will be described later. First, the orientation of synthetic fiber filaments is defined as the difference between the refractive index of the fiber in the length direction and the thickness direction (hereinafter referred to as the birefringence), and then the defined birefringence is deformed so that it can be measured by this method. The definition of the form measured by the device will be explained.

抝第4圖所示,在合成纖維絲(F)上,由於在紡絲、 拉伸等操作中,加至此種構成纖維的高分子鏈(Μ)之應 力,會産生基於分子鐽(Μ)的選擇定向而被凍結之定向 雙折射。因而,以定量性的測定所産生的雙折射,而以 纖維軸向(Υ軸方向)的折射率N y與垂直於纖維軸向(X ------------ _衣,’---一----訂------- (諳先閱讀背面之注意事項再填寫本頁) 經濟部智慧財產局員工消費合作社印製 向 定 維 纖 。 為者 χίΐ用 Ν使 Α 所 率般 射一 折是 雙> 的 差之; IS 義 率定 射1)? 折t " &式 N )6下--向由 N 方 ,Δ 軸度 1 /V 式 度 向 定 維 纖 II 率 IJ 折 雙 Ν Δ 率 Γ3 A3 折 之 向 軸 維 纖拗 As shown in Fig. 4, in the synthetic fiber filament (F), due to the stress added to the polymer chain (M) constituting the fiber during spinning, drawing and other operations, the molecular fiber (M) is generated. The selected orientation is frozen by the directional birefringence. Therefore, the birefringence produced is measured quantitatively, and the refractive index N y in the fiber axial direction (纤维 axis direction) is perpendicular to the fiber axial direction (X ------------ _ clothing , '--- 一 ---- Order ------- (谙 Please read the notes on the back before filling out this page) The Consumer Cooperatives of the Intellectual Property Bureau of the Ministry of Economy printed Xiang Dingwei Fiber. Ν makes Α to shoot like a fold is the difference between double > IS means definite to shoot 1)? Fold t " & formula N) 6 down-from N side, Δ axis degree 1 / V formula Degree-fixed-dimensional fiber II rate IJ folded double N Δ rate Γ3 A3 folded axis fiber

X 又X again

直 I 1?· 建 光 用 MU 禾 之 示 表 \)-2 /JV 式 下 率以 ί Ν 折 Δ 之將 向可 軸 t 維。 本紙張尺度適用中國國家標準(CNS)A4規格(210x 297公f ) A7 B7 414814 五、發明說明(〖) [産業上之利用領域1 本發明為有關一種繼維的分子定向度測定裝置及其測 定方法β [習知之技術] 以往的測定纖維分子定向度之方法,是有光衍射法 、红外二向色性法,及磁性各向導性法等,但其裝置都 很複雜而髙價,且,其測定方法也很複雜,並不實用。 比較實用的方法是有利用光學性手段之雙折射率測定法 。該雙折射率測定法中,有干涉條紋計數法、平行尼可 耳棱鏡Uicol)旋轉法,及分段補償器法等。干涉條紋 (請先閱讀背面之注意事項再填寫本頁) 經濟部智慧財產局員工消費合作社印製 照定平出度平式條 雒作要放 光出開取厚開段涉 纖備而其 色求特上勻特階干 的準,將 單以在路均在面定 細其上於 的,如光出如一測 極,朝難 長量有在求有 ,而 將斷要, 波數是,以是色, 須切須斜 準之法射,法涉紋 必的面傾 基紋轉照度器干條。 ,線斷會 用條旋光強值察涉者 中直切多 -涉鏡色的補觀干法 法地其維 斷干棱單光段面色方 數向,纖 切的耳用射分一黑之 計斜察 , 向出可 ,透。 ,現度 紋其觀時 斜顯尼佈該者佈呈向 條使方上 維所行公定法公其定I]涉先上鏡 缕面平所測方所使出51干預從徹 將斷。報,之報-求 U 述is)要顯 先切者公片度公長以 W 上 U 且在 預在法號F1向號程,㈣在 U 。置 是算方97波定89光隔㈣ ,|^_放 法計之26人的83«間 MtghEM 數,度-8放品-7補的I-B然Iffi很纖 ο ο 發 通 計射向 1 和樣 1 的紋ίξ(¾業將 本紙張尺度適用中國國家標準(CNS)A4規格(210x 297公釐) A7 B7 414814 五、發明說明(μ) 第5圖 傑光程差圖。 第6圖 傜觀察圖。 [參考符號說明] 1.....定向度測定裝置 光源機構 觀察機構 分段補償機構 迪續補償機構 合成纖維絲Straight I 1? · Jian Guang uses MU Hezhi's table \)-2 / JV below the rate in ί N fold Δ will be able to axis t dimension. This paper scale is applicable to Chinese National Standard (CNS) A4 specification (210x 297 male f) A7 B7 414814 V. Description of invention (〖) [Industrial application field 1 The present invention relates to a molecular dimension determination device for continuous dimension and its Measurement method β [Known technique] Conventional methods for measuring the molecular orientation of fibers include light diffraction method, infrared dichroism method, and magnetic anisotropy method. However, the devices are complex and expensive, and The measurement method is also complicated and not practical. A more practical method is the birefringence measurement method using optical means. Examples of the birefringence measurement method include an interference fringe counting method, a parallel Nicols Uicol rotation method, and a segment compensator method. Interference fringes (please read the notes on the back before filling this page) Printed by the Consumers' Cooperative of the Intellectual Property Bureau of the Ministry of Economy In order to achieve uniformity and order, we will narrow down the distance between the road and the surface. If the light comes out as a pole, the difficulty will be calculated. However, the wave number is It is a color, which must be cut obliquely, and the surface must be tilted to the base line to turn the illuminator dry. , The line break will use the optical rotation intensity value to detect the straight-cut multi-involved-related specular color method, the dimension of the single-segment surface of the dimensional cut-off edge is square, and the slicing ear is divided into black and black. Investigate obliquely. In the present time, the time of its observation was oblique, showing that Nibu ’s cloth was oriented toward the envoy Fang Shangwei ’s statutory law, which is based on the first intervention I ’ve done, and the 51 intervention made by Fang Nianping ’s measured side was completely cut off. The report, the report-seeking U is is to be displayed. The predecessor's public prince shall be above W and U in the pre-registration method F1, and then at U. Set is the calculation of 97 wave set 89 light interval |, ^ _ put the method of the 26 people of 83 «MtghEM number, the degree -8 put the product -7 complement the IB Ran Iffi is very fine ο ο pass meter shot to 1 The pattern of the sample 1 is the same as the standard of the Chinese paper (CNS) A4 (210x 297 mm) A7 B7 414814 V. Description of the invention (μ) Figure 5 Optical path difference chart. Figure 6傜 Observation diagram [Description of reference symbols] 1 ..... Orientation measuring device Light source mechanism Observation mechanism Segment compensation mechanism Di continued compensation mechanism Synthetic fiber filament

3 4 5 F Μ ....分子鏈 21 - . .光源透鏡 31 · - -光學顯微鏡 D…-照相機 ·* 6 圖像處理裝置 37· · . ·圖像顯示裝置 41 ....固定偏振片 42, 42a,42b · . ·.波阻片 42c · · 波阻片支承體 42cl · _切口部 i 42c2 . . 切口部 2 43 ..切口部 51 - . ·轉換機構 52 . . . ·旋轉偏振片 (請先闓讀背面之注意事項再填寫本頁) %----r----訂---------線 經濟部智慧財產局員工消費合作社印製 -16- 本紙張尺度適用中國國家標準(CNS)A4規格(210x 297公釐) 414814 A7 經濟部智慧財產局員工消費合作社印製 B7_五、發明說明(> ) 妥。且,纖維的光程差太大時,干涉條紋數亦多,高次 的干涉條紋會淡化,而會有計算錯誤之可能。潮定用的 補助措施是有塞拿蒙補償器 (Senaraont Compensator) 、及貝雷克補償器(Berek Compensator)等,但其光程 差的補償範圍太小,不適用於光程差大的纖維之測定。 又,測定用的補肋措施也另有巴皮内補償器(Babinet Conpensator)等,但其係只能潮出光程差的概值者,而 不適用於有高精度要求的纖維之定向度_定。 平行尼可耳棱鏡旋轉法是要求出具薄片狀之均勻厚度 樣品的定向度之方法,並不適用於具圓形斷面或任意斷 面的纖維之定向度測定。又,其僳尚需使偏振鏡和檢偏 鏡整體在光軸周圍旋轉所用之機構,和將單色光的波長 依次變更之濾光鏡裝卸機構,及將波阻片取出和放入於 光路上的波阻片位置控制機構,因而其構造會很複雜。 步级補償器法是光程差不同的多數痼波阻片(例如1/4 λ、 1/2凡、1A、 2又、3λ、 5λ>,以階段式的補償光 程差之方法,因而不適用於微小光程差(未滿1/4λ)之 補僂。又,其在任意斷面的纖維時,不會呈現一對的黑 色干涉條紋,因而不適用於任意斷面之纖維的定向測定 。且,未拉伸絲、極細絲等的光程差很小(1 / 1 Q 0又以下) ,因而,要以波阻Κ測定時,需準備具微小光程差的波 阻Η,其工作效率很低。因此,步级補償器法的澜定對 象只限定於圖形斷面的纖維,且光程差也要某程度大 (1/4;1以上)之纗雒。 一 4 - ------------l· ^---------訂---------線 (請先閱讀背面之注意事項再填寫本頁) 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) 經濟部智慧財產局員工消費合作社印製 414814 A7 _B7_ 五、發明說明(今) 本發明乃有鑑於上述問題,目的是在提供一種適用於 繼維定向度澜定之制定裝置及潮定方法者〇 [解決問題之手段] 為達成上述目的,本發明的定向度測定裝置僳包含: 對測定對象的繼維照射白色光所用之光源機構;觀察上 述照射光所用之觀察機構;設置在上述光源機構與缕維 之間的分段補傖機構;及配置在上述觀察機構與纖雒之 間的連績補償機構之4機構所構成,而上述分段補償機 構是由固定偏振片,和光程差補償值不同的多數艏波阻 片,及可使波阻片改變90°方向而放置的加減運算切口 部所構成,而上述連缠補償機構是由可將橢圓偏光轉換 為直線偏光所用的轉換機構,和正反轉自如的旋轉偏振 Η所構成者。又,本發明的定向度测定方法是以其折射 率是和測定對象之纖維的粗細度方向之折射率大致相同 之液體充填於纖維四周,而用光源機構對纖維照射白色 光,使其顯出由光程差所産生的干涉色,並將分段補償 機構的多數健波胆板放置於加減運算切口部,以將光程 差階段式的補償之後,使連縝補償機構的旋轉偏振片轉 動,以將光程差連鑲的補償,而由觀察機構來解析測定 對象的纖維所産生的干涉條紋,以求出雙折射率者。 [實施例】 以下參照圖面説明本發明的實施例 如第1圖及第3圖所示,本發明的定向度測定装置(1) 傺由朝向測定對象的合成纖維絲(F)照射白色光所用之 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) --------一----L·^---1-i---訂---------線 --r (請先閱讀背面之注意事項再填寫本頁) 414814 A7 經濟部智慧財產局員工消費合作社印製 B7_ 五、發明說明(& ) 光源機構(2);觀察合成纖維絲(F)的透射光所用之觀察 機構(3);配置在光源機構(2)與合成纖維絲(F)之間之 分段補償機構(4);及配置在觀察機構(3)與合成纖維絲 (F)之間之連籲補償機構(5)的4機構所構成,分段補值 機構(4)是由固定偏振H (4〇,和光程差補辑值不同的 多數個波阻Η (42),及可使波阻片(42)改變90°方向而 放置的加減運算切口部(43)所構成眉連缠補償機構(5) 是由可將橢圓偏光轉換為直線偏光所用的轉換機構(51) ,和正反轉自如的旋轉偏振片(52)所構成β 在此,將有關本發明的定向度測定裝置(1)中,以合 成纖維絲(F)為基準的各構成機構之位置關僳予以説明 。設平行於合成纖維絲(F)的粗細度方向為X軸方向, 平行於其長度方向為Υ軸方向。首先,使固定偏振片 (41)與旋轉偏振Η (52)的基準點之偏光方向成為正交 (90° ),形成正交尼可耳捷鏡。該固定偏振片(41)是配 置為與X軸方向成45° 。又,波胆Η (42)的相位提前方 向是配置為平行於X軸或Υ軸,此方向是在波阻Η (42) 要對合成纖維絲(F)的光程差進行加減運算之方位。轉 換機構(51)的相位提前方向是配置為與X軸成45° ^此 方向是轉換機構(51)要將透射過合成纖維絲(F)的橢圓 偏光轉換為直線偏光時之方位。 光源機構(2)是由眾所周知的鹵素燈和産生白色光的 濾先鏡所構成之光源裝置,而設置在觀察機構(3)中可 使合成纖維絲(F )的透射光入射之位置β -6- (請先閱讀背面之注意事項再填寫本頁) ^'丨 _ 訂---------線 --- 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) 經濟部智慧財產局員工消費合作社印製 414814 A7 B7 五、發明說明(f ) 钃察機_ ( 3 )是由光學顯撤鏑(3 1),連接在該光學顥微 鐮(31)中的照像機(33),連接在該照相梅(33)中的國像 處理裝置<36),及園像顯示裝置(37)所梅成β 分段補償機構(4)是由《光方向為一定的固定僱振Η (41)、光程差補黴值不同的多數健波阻Μ (42)、及可使 波阻Μ ( 4 2 )改變9 (Γ方向而放置的加滅竃算切口部(4 3 ) 所構成,而加減邇算切口部(43)是在固定鴒振片(41)上 部與其構成為整鼸構造。分段補值檐構(4>是具如此之 整釅構造,因而,可容易的放置在光學顧撖鏡(31)的光 灝透鏡(21)等之上來使用》又,波阻片(42a)、(42b)是 如第3園所示,是由波阻片支承髓(42c)所支承β支承 髏(42c)是由其内徑大致輿偏振Η直徑大致相等之中空 國柱或方柱,在箭頭X方向切掉波阻片(42b)寬度的切 口部1 (42cl)與在箭頭Y方向切掉波阻H (42a)寬度的 切口部2 (42c2)所_成。又切口部l(42cl>輿切口部2 (42e2)的切口是設計為不同的深度》又,切口部1 ,切 口部2的深度都設計為可插入多數镧波阻Μ之深度·如 第3圔所示,將波阻板(42a)放置在箭頭Υ方向時,其 光程差補僂值會被相加,而將波阻板(42b)放邃在箭頭 X方向時,其光程差補僂值會被相減〇 達鑛補償檐構(5)是由将椭圔傷光轉換為直線籲光用 的轉換櫬構(51)和正反轉自如的旋轉傾振Η (52)所構成 。連鑲補償檐構(5)是將上述分段補償機構(4)中所未能 完金補償的殘留光程差,缠鐮的、且完金的予以補償者 。具有殘留光程差的光一般上是成為檷國镐光,因而利 -7- 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) (請先閱讀背面之注意事項再填寫本頁) I--„--— I— I I I I---- 年q屬姜efi#良4灸正/補充 A7 五、發明說明U ) 用具1/4又光程差的、設置在上逑方位中之轉換機構(51) ,將其轉換為直線徧光。經如此轉換過的直線偏光之偏 光方向是從旋轉偏振Μ ( 5 2 >的基準點徧移0度。因而, 將旋轉偏振片(52)轉動0度,就與偏光方向成為正交, 而可補償殘留光程差。 其次,將使用具如上逑構成的測定裝置,以測定定向 度之方法予以說明。先說明對於圓形斷面的纖維之測定 方法,其後再説明任意斷面的纖維之測定方法。 首先,將合成纖維絲的定向度定義為纖維的長度方向 與粗細度方向的折射率之差(以下稱雙折射率)之後,再 將所定義的雙折射率變形為可由本測定裝置所測定的形 式之定義式之事,予以說明。3 4 5 F Μ .... molecular chain 21-.. Light source lens 31 ·--optical microscope D ...-camera · * 6 image processing device 37 · · · · image display device 41 .... fixed polarization Sheets 42, 42a, 42b ...... Wave blocking sheet 42c. Wave blocking sheet support 42cl. _Notch part i 42c2 .. Notch part 2 43 .. Notch part 51-.. Conversion mechanism 52 .. Polarizer (Please read the precautions on the back before filling this page)% ---- r ---- Order --------- Printed by the Consumer Cooperative of the Intellectual Property Bureau of the Ministry of Economic Affairs-16- This paper size applies the Chinese National Standard (CNS) A4 specification (210x 297 mm) 414814 A7 Printed by the Consumers ’Cooperative of the Intellectual Property Bureau of the Ministry of Economic Affairs B7_V. The invention description (>) is correct. In addition, when the optical path difference of the fiber is too large, the number of interference fringes is also large, and the high-order interference fringes will fade, and there may be a calculation error. The subsidy measures used by Tide are Senaraont Compensator and Berek Compensator, but the compensation range of the optical path difference is too small, and it is not suitable for fibers with large optical path difference. Its determination. In addition, the rib-reinforcing measures used for measurement are also Babinet Conpensator, etc., but it is only an approximate value of the difference in light path difference, and it is not suitable for the orientation of fibers with high accuracy requirements_ set. The parallel Nicols prism rotation method is a method that requires a sheet-like uniform thickness sample orientation. It is not suitable for measuring the orientation of fibers with circular or arbitrary cross-sections. In addition, it is still necessary to use a mechanism for rotating the polarizer and the analyzer as a whole around the optical axis, a filter attaching and detaching mechanism for sequentially changing the wavelength of monochromatic light, and removing and placing the wave blocking plate in the light. The wave barrier position control mechanism on the road will have a complicated structure. The step compensator method is a majority of chirped wave retarders with different optical path differences (such as 1 / 4λ, 1 / 2fan, 1A, 2A, 3λ, 5λ >). It is not suitable for the supplementation of small optical path difference (less than 1 / 4λ). Moreover, it does not show a pair of black interference fringes when the fiber is in any cross section, so it is not suitable for the orientation of the fiber in any cross section. And the optical path difference of unstretched filaments, ultra-fine filaments, etc. is very small (less than 1/1 Q 0 and below). Therefore, when measuring with wave resistance K, it is necessary to prepare a wave resistance with a small optical path difference. Its working efficiency is very low. Therefore, the target of the step compensator method is limited to the fiber of the graphic section, and the optical path difference must also be large (1/4; 1 or more). 4- ------------ l · ^ --------- Order --------- line (please read the precautions on the back before filling this page) Standards are applicable to China National Standard (CNS) A4 specifications (210 X 297 mm). Printed by the Consumers ’Cooperative of the Intellectual Property Bureau of the Ministry of Economic Affairs. 414814 A7 _B7_ V. Description of the invention (today) The present invention has been made in view of the above problems. A device and method for formulating a tide fixation method for in-plane orientation. [Means for solving problems] In order to achieve the above-mentioned object, the orientation measuring apparatus of the present invention includes: a light source for irradiating white light to the in-plane measurement object. An observation mechanism for observing the above-mentioned irradiated light; a segment compensation mechanism provided between the above-mentioned light source mechanism and the strands; and a mechanism for continuous performance compensation arranged between the above observation mechanism and the fiber, The segment compensation mechanism is composed of a fixed polarizer, most chirped wave retarders with different compensation values for the optical path difference, and an addition and subtraction operation cutout portion that can change the direction of the wave retarder by 90 °. The mechanism is composed of a conversion mechanism for converting elliptical polarized light into linear polarized light, and a rotating polarization chirp that can be reversed freely. The orientation measurement method of the present invention is based on the refractive index and the thickness of the fiber to be measured. Liquids with approximately the same refractive index in the degree direction are filled around the fiber, and the fiber is irradiated with white light by the light source mechanism, so that it is displayed by the difference in optical path The interference color generated, and the majority of the bipolar plate of the segmental compensation mechanism is placed in the addition and subtraction operation cutout portion to compensate the optical path difference stepwise, and then the rotating polarizer of the flail compensation mechanism is rotated to change the optical path. Compensation for the differential setting, and the observation mechanism analyzes the interference fringes generated by the fibers of the measurement object to obtain the birefringence. [Examples] Examples of the present invention will be described below with reference to the drawings. As shown in the figure, the orientation measuring device (1) of the present invention 傺 The size of the paper used for irradiating white light from the synthetic fiber filament (F) facing the measurement object is applicable to the Chinese National Standard (CNS) A4 specification (210 X 297 mm) -------- 一 ---- L · ^ --- 1-i --- order --------- line--r (Please read the notes on the back before filling in this Page) 414814 A7 Printed by the Consumers ’Cooperative of the Intellectual Property Bureau of the Ministry of Economic Affairs B7_ 5. Description of the invention (&) Light source mechanism (2); Observation mechanism (3) for observing transmitted light of synthetic fiber filament (F); The segment compensation mechanism (4) between the mechanism (2) and the synthetic fiber filament (F); and the observation mechanism (3) and The fibrous filaments (F) are composed of 4 mechanisms of the compensation mechanism (5), and the segmental compensation mechanism (4) is composed of a plurality of waves with different polarization H (40, and the optical path difference compensation value). The baffle (42), and the eyebrow entanglement compensation mechanism (5) formed by the addition and subtraction operation notch portion (43) which can change the 90 ° direction of the wave blocking plate (42), is used to convert elliptical polarization to linear polarization The conversion mechanism (51) and the forward and reverse rotation polarizing plate (52) are composed of β. Here, each of the components of the orientation measuring device (1) of the present invention, which is based on a synthetic fiber filament (F), is used as a reference. The location of the institution will be explained. The thickness direction parallel to the synthetic fiber filament (F) is assumed to be the X-axis direction, and the direction parallel to the length thereof is to be the Υ-axis direction. First, the polarization direction of the reference point of the fixed polarizer (41) and the rotating polarization chirp (52) is made orthogonal (90 °) to form a crossed Nicols lens. The fixed polarizer (41) is arranged at 45 ° with respect to the X-axis direction. In addition, the phase advance direction of the wave ridge Η (42) is arranged parallel to the X-axis or Υ axis, and this direction is the direction where the wave path Η (42) is to add or subtract the optical path difference of the synthetic fiber filament (F). . The phase advance direction of the conversion mechanism (51) is configured to be 45 ° from the X axis. ^ This direction is the orientation when the conversion mechanism (51) converts the elliptical polarized light transmitted through the synthetic fiber filament (F) into linearly polarized light. The light source mechanism (2) is a light source device composed of a well-known halogen lamp and a filter that generates white light, and is provided in the observation mechanism (3) at a position where the transmitted light of the synthetic fiber filament (F) can enter β- 6- (Please read the precautions on the back before filling this page) ^ '丨 _ Order --------- Line --- This paper size applies to China National Standard (CNS) A4 (210 X 297 mm) (B) Printed by the Consumer Cooperative of the Intellectual Property Bureau of the Ministry of Economic Affairs 414814 A7 B7 V. Description of the invention (f) The inspection machine _ (3) is removed by the optical display (3 1), which is connected to the optical microscope (31) The camera (33), the national image processing device < 36) and the garden image display device (37) connected to the photographic plum (33) are composed of the β segment compensation mechanism (4). A fixed employment vibration (41) with a certain light direction, a large number of healthy wave resistances M (42) with different optical path difference mold compensation values, and additions and deletions that can change the wave resistance M (4 2) by 9 (Γ direction) The calculation cut section (4 3) is constituted, and the addition and subtraction calculation cut section (43) is formed on the upper part of the fixed vibration plate (41) with its integral structure. The segmented value-added eaves structure (4 > It has a compact structure, so it can be easily placed and used on the optical lens (21), etc. of the optical mirror (31). Also, the wave blocking plates (42a) and (42b) are as shown in the third circle. Is supported by the baffle plate (42c), the β-supported bone (42c) is a hollow national or square pillar with its inner diameter approximately equal to the polarization, and the diameter is approximately equal, and the baffle plate (42b) is cut in the direction of the arrow X ) Width notch portion 1 (42cl) and notch portion 2 (42c2) with the width of wave impedance H (42a) cut in the direction of arrow Y. The notch portion 1 (42cl > notch portion 2 (42e2) is a notch It is designed to have different depths. Also, the depths of the notch 1 and the notch 2 are designed to be able to insert most of the lanthanum wave resistance M. As shown in Fig. 3, the wave resistance plate (42a) is placed in the direction of arrow Υ. , The optical path difference compensation value will be added, and when the wave blocking plate (42b) is placed in the direction of the arrow X, its optical path difference compensation value will be subtracted. 0 Mine compensation eaves structure (5) It is composed of a conversion structure (51) for converting ellipsoidal light into a linear light and a rotating tilting vibration (52) that can be reversed and reversed. (4) Residual optical path difference that cannot be compensated for gold compensation, who is sickling, and complete gold compensation. The light with residual optical path difference generally becomes the light of Guo Guohao. Paper size applies to China National Standard (CNS) A4 (210 X 297 mm) (Please read the precautions on the back before filling out this page) I-„--— I— III I ---- year is ginger efi # 良 4Moxibustion plus / supplement A7 V. Description of the invention U) A conversion mechanism (51) with a 1/4 optical path difference and set in the upper azimuth direction, converts it into a straight line of light. The polarization direction of the linearly polarized light thus converted is shifted by 0 degrees from the reference point of the rotation polarization M (5 2 >. Therefore, if the rotation polarization plate (52) is rotated by 0 degrees, it is orthogonal to the polarization direction, and Residual optical path difference can be compensated. Next, a method for measuring the degree of orientation will be described using a measuring device having the structure described above. The method for measuring a fiber with a circular cross section will be described first, and then the fiber with an arbitrary cross section will be described later. First, the orientation of synthetic fiber filaments is defined as the difference between the refractive index of the fiber in the length direction and the thickness direction (hereinafter referred to as the birefringence), and then the defined birefringence is deformed so that it can be measured by this method. The definition of the form measured by the device will be explained.

抝第4圖所示,在合成纖維絲(F)上,由於在紡絲、 拉伸等操作中,加至此種構成纖維的高分子鏈(Μ)之應 力,會産生基於分子鐽(Μ)的選擇定向而被凍結之定向 雙折射。因而,以定量性的測定所産生的雙折射,而以 纖維軸向(Υ軸方向)的折射率N y與垂直於纖維軸向(X ------------ _衣,’---一----訂------- (諳先閱讀背面之注意事項再填寫本頁) 經濟部智慧財產局員工消費合作社印製 向 定 維 纖 。 為者 χίΐ用 Ν使 Α 所 率般 射一 折是 雙> 的 差之; IS 義 率定 射1)? 折t " &式 N )6下--向由 N 方 ,Δ 軸度 1 /V 式 度 向 定 維 纖 II 率 IJ 折 雙 Ν Δ 率 Γ3 A3 折 之 向 軸 維 纖拗 As shown in Fig. 4, in the synthetic fiber filament (F), due to the stress added to the polymer chain (M) constituting the fiber during spinning, drawing and other operations, the molecular fiber (M) is generated. The selected orientation is frozen by the directional birefringence. Therefore, the birefringence produced is measured quantitatively, and the refractive index N y in the fiber axial direction (纤维 axis direction) is perpendicular to the fiber axial direction (X ------------ _ clothing , '--- 一 ---- Order ------- (谙 Please read the notes on the back before filling out this page) The Consumer Cooperatives of the Intellectual Property Bureau of the Ministry of Economy printed Xiang Dingwei Fiber. Ν makes Α to shoot like a fold is the difference between double > IS means definite to shoot 1)? Fold t " & formula N) 6 down-from N side, Δ axis degree 1 / V formula Degree-fixed-dimensional fiber II rate IJ folded double N Δ rate Γ3 A3 folded axis fiber

X 又X again

直 I 1?· 建 光 用 MU 禾 之 示 表 \)-2 /JV 式 下 率以 ί Ν 折 Δ 之將 向可 軸 t 維。 本紙張尺度適用中國國家標準(CNS)A4規格(210x 297公f ) A7 414814 B7_ 五、發明說明(7 ) Δ S = ( V 0 / V y ) - ( V 0 / v x ) .....(2) V ο :大氣中的光速 :物質中的X軸方向之光速 ν X :物質中的Υ軸方向之光速 又,若以搀質的通過距離為t。時,ΛΝ可由下式(3) 表示之。 Δ N = (v〇 /to )X (to /vy -to /νχ) .....(3) t。:物質的通過距離 又,若以Τχ、T/為物質内的通過時間時,AN可由 下式(4)表示之。 △ N= (l/t〇 )Xv〇 (Ty -Tx)=(l/t〇 )R .....(4) Τχ :物質内的X方向通過時間 T ^ :物質内的Y方向通過時間 R = v。(Ty -Tx):透射光的光程差 通常的纖維是Ty>Tx ,纖維的透射光係如第5(a)、 (b)圖所示,在Y方向的光會産生滞後,該滯後部分被 稱為光程差R (Retardation)。在具光程差R的合成纖 維絲(F)上照射白色光時,在合成纗維絲(F)的透射光之 影像上會顯出干涉色(多種顔色所構成的彩虹色)。一面 以觀察機構(3)觀察干涉色,一面調整分段補償機構(4) 的波阻Η (42)和連纊補償機構(5)的旋轉偏振Η (52), 使光程差補償值f逐漸增加時,干涉色會逐漸轉移到低 次倒(向黑暗方向)β光程差補償值β'具有將合成纖雒絲 (F)的Υ軸方向之滯後R部分導前IT之功能,如補償到 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) ^^1 ^^1 ^^1 ^^1 ^^1 ^^1 ι Γ— Bn - r Jt. ^^1 ^^1 ^^1 ^^1 ^^1 ^^1 p ^^1 ^^1 ^^1 ^^1 ^^1 ^^1 1 . 4^· (請先閱讀背面之注意事項再填寫本頁) 經濟部智慧財產局員工消費合作社印製 A7 414814 B7_ 五、發明說明(/ ) R= R1時,如第5(c)、 (d)圖所示,X軸方向的光和Y軸 方向的光會成為同相位。成為同相位的光是不能透射旋 轉偏振片(52),因而觀察此狀態的光時會成為黑暗狀態 ,而會顯出一對黑色干涉條紋。在此狀態下,利用纖維 的厚度t。就可求出雙折射率ΛΝ 。 也即,在合成餓維絲中,定義為纗維定向度的雙折射 率是可由透射光的光程差R除以厚度t。之值來表示 。在此,合成纗維絲並不是具有一定厚度的平板狀者, 而是近似於圓形斷面者,因而,其測定對象的厚度t。 並不能利用纖維直徑,而需求出可取代的代表厚度1; β 因此,在斷面形狀為近似於圓形的合成纖維絲中,如 能算出代表厚度t和透射光程差R的2傾值時,就可求 出定義為定向度的雙折射率ΛΝ 。 以上是對於定義式的變形先予説明,而以下是要說明 利用本發明的測定裝置,由此式(4)求出纖維定向度之 方法。 設平行於測定對象的合成纖維絲(F)的粗細度方向為 X軸方向,平行於其長度方向為Υ軸方向,而以如上述 的配置各構成機構之傾斜方位,經配置於如此之方位後 ,會呈現將橢圖镉光轉換為直線偏光而供應於旋轉偏振 片之作用。即,將各構成機構設定於所定之方位時,就 可使合成纖維絲(F)顯出干涉色,可達成由波阻片(42) 的階段式補償和由旋轉偏振片(52)的連缠性補償。而利 用此2階段補償以求出織維定向度。 -1 0 - 本紙張尺度適用中國囤家標準(CNS)A4規格(210 X 297公釐) --------ί 晒 — Γ I·---_----^---------線 -I f (請先閱讀背面之注意事項再填寫本頁) 經濟部智慧財產局員工消費合作社印製 經濟部智慧財產局員工消費合作社印製 414814 a7 _B7_ 五、發明說明(?) 接著,在要將纖維放置於顯微鏡之際,用其折射率是 和纖維的粗細度方向折射率大致相同之液體填於纖雒的 四周。由此可使織雒不會直接與大氣接觸,可避免光在 纖維的端頭産生複雜的折射,而可正確的測定定向度。 又,潘維的放置於顯撖鏡上的方向是使缕維的長度方向 (Υ軸方向)成為顯微鏡的前後方向較為理想。如此,可 使纖維在對物鏡下的對準位置及觀察干涉現象較為容易 ,且,可容易的在圖像處理裝置等上對準座標軸和方向 性。 接箸,由光源機構(2)對合成缕維絲(F)照射白色光。 由於使用白色光,而可在雜Μ的影像上顯出彩虹色的干 涉色。由於使其顯出彩虹色的干涉色,因而用波阻片以 補償光程差時,可明確的判斷是要將波阻Η相加或相減 β又,僅有在光程差被完全補償之位置是唯一會成為黑 暗之位置,因而,可明確的做出光程差的補償己完了之 判斷。 接著,使用光程差補償值不同的多數波阻片,以補償 纖維的光程差。波阻片的光程差補償值是用例如1几、 3又、9λ·.·等者。1Α是基準波長,雖並無恃別的限定 ,但從光程差所顯出的干涉色之周期性及生理學上的波 長敏感度上而言,是用5 4 6ηπι為理想。波阻片是在X軸 方向或Υ軸方向組合起來放置在加減運算切口部來使用 。Υ軸方向是相加,X軸方向是相減β例如在Υ軸方向 放置3λ、X軸方向放置1λ時,光程差補償值是成為 -1 1 - 本紙張又度適用中國國家標準(CNS)A4規格(210 X 297公釐) •^1 1^1 n I n n I n t I LI (請先閱讀背面之沒意事項再填寫本頁) A7 414814 B7_ 五、發明說明() (3λ-1Λ)β使用1;1、 3Λ、 9又時,可在1又〜13凡之 間構成1λ節距差。如再附加未滿1又的波阻片,例如 1/9λ、 1/3又時,可在1/9又〜(13 + 4/ 3Α)之間構成1/9 又節距差。 要使波阻片獲得最有效的組合時,使波阻片的光路差 補償值 e3m ΧΛ(βι = 0, ±1、 ±2、 .·)為理想。βι = -2 、-1、 0、 1、 2 時,是要準備 1 / 9 A、 1 / 3 A、 1 Λ、 3 λ 、9λ的波阻片。此乃可使波阻片的組合不致於重複, 而以所需最少限度的波阻片,就可實現廣範圍的補償值 者。 由觀察機構(3)觀察干涉色,逐漸增加波阻片的光程 差補償值時,干涉色會逐漸向低次倒(黑暗部分方向)轉 移〇波阻片具有將纖維的Υ軸方向的光之滞後R部分導 前R1之功能,如調整到ίί = ίί'時,Υ軸方向的光之滞後部 分會被補償(被抵消),而成為如第5 (c)、 (d)圖之狀 態。觀察此狀態的光時所看到的是黑暗^如為圓形斷面 的纖維時會顯出如第6(b)圖所示的一對黑色干涉條紋(S) 。將此影像由圖像處理裝置(36)來解析,而由下式求出 雙折射率。 ΔΝ = nA/SQR(Ds -W2 ) .....{5 ) △ N :纖維的雙折射酶 η :波阻Η之值 又:基準波長 D :圓形斷面纖維的直徑 -1 2 - 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) ------------l· 牧-----1----訂·-----— !線 .I f (請先閲讀背面之注意事項再填寫本頁) 經濟部智慧財產局員工消費合作社印製 經濟部智慧財產局員工消費合作社印製 414814 A7 __- * ._B7_ 五、發明說明() W :圓形斷面纖維的一對黑色干涉條紋之間隔 以這種方法時,只要調整波阻Η就可測定此種與通常 的圓形斷面纖維有關之定向度。然而,波阻片是以階段 式的補償光程差者,因而有其最小補償值之界限。而要 對某種其光程差極小(l/lfl〇;L以下)的缕雒(未拉伸絲或 棰細纖維),以波阻片測定時,必需準備多數個光程差 撤少之波阻片,非但效率低且不經濟。 又,如為任意斷面的纖雒時,不會顯出一對黑色干涉 條紋,因而式(4)不適用。在這種場合時,波阻片的補 僂僅止於粗調整,而由以下的操作來做光程度之補傖》 使旋轉辐振片(52)向正方向或反方向轉動,一面連缠 的補償光程差,一面做徹諝整,以完全的補償光程差, 使其呈現黑暗部。在波阻片不能完全補償而殘留撤小光 程差的光,一般是成為橢圓偏光。轉換機構(51)是具有 1/4 λ 的光程差,而配置在上述方位時,具有將橢圓偏 光轉換為直線偏光之作用β此原理可由記載在槭光相關 文獻等的波因卡勒球(Poincare Sphere)來說明,而在 此將詳細説明從略。從轉換機構透射的光會成為直線偏 光,但其偏光方向是徧移0角度。 殘留光程度ϋ與偏光方向0的關僳是ϋ=θ/18(Τ · λ 。因此,將旋轉偏振動0角度時,偏光方向成為正 交,而會呈現黑暗部。在圓形斷面纗維時,雖其光程差 徹少也會潁出如第S(b>圓所示的一對黑色干涉條紋。將 此影像由像處理裝置(36)來解析,而由下式就可求出雙折 -1 3- 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) H· n ^^1 ^^1 ^^1 ^^1 ^^1 ^^1 ^^1 ^^1 一·™ f (請先閱讀背面之注意事項再填寫本頁) 經濟部智慧財產局員工消費合作社印製 度通零或使 厚 Τ 為,以 的度約零轉 知厚大為反 周其是 0 Μ 所,差及振 眾等程 η 偏 ί 膜光使轉 段薄的可旋 度手的維,將 厚的狀纗時 ,。 部外 Η 些合值率 暗另薄某場負射 黑以,有此為折 的先又,在 0 雙 維預。又。使定 繼是之。者滅澜 面 Τ 出多負相可 斷度求為為的就 意厚丨者差 Η , 任的等知程阻值 :維器已光波負 Τ 纖定是或用為 測常,利 Θ 414814 A7 〆_B7__ 五、發明說明(^ ) 射率。 △ N = {η+(θ /180) } X /{SQR (D 2 -W 2 ) }.....(6) △ Ν :纖維的雙折射率 η :波阻Μ之值 Θ :從旋轉偏振片的基準點算起之轉動角度 又:基準波長 D :圓形斷面纖維的直徑 W :圓形斷面纖維的一對黑色干涉條紋之間隔 如為任意斷面纖維的情形時,將旋轉偏振Η轉動,以 便可在適當的位置(可容易測定纖維厚度的位置為理想)顯出黑 暗部。將此影像由圖像處理裝置(36)來解析,而由下式 就可求出雙折射率。 △ Ν = {η+(0/18Ο)}λ/Τ .....(7) Δ Ν :潘維的雙折射率 η :波阻片之值 0 :從旋轉偏振片的基準點算起之轉動角度 又:基準波長 本紙張足度適用中國國家標準(CNS)A4規格(210 X 297公釐) t n n I ^^1 I J (請先閱讀背面之注意事項再填寫本頁) 經濟部智慧財產局員工消費合作社印製 414814 A7 _ . ._B7_五、發明說明(Μ ) 又,有某些纖雒是具有折射率分散,而會在光程差被 補償之位置的黑暗部觀察到若干著色的情形。但是,這 種情形時,可由如下步驟來査証干涉色的次數K 。次數 K是表示光程差Κ= ηλ的η者。設第η條干涉條紋的位 置之纖維厚度為Τη ,第η+1條干涉條紋的位置之繼錐厚 度為Tn+i時,由式(8)可査証第η條干涉條紋的次數Κ 。Τη , Τη+1的測定方法是如為圓形斷面繼雒時,可在 圖像處理裝置描繪圖斷面的補助線以測定之。如為任意 斷面之潘維時,可由眾所周知的厚度測定器來求出。 Κ= Τη / (Tn+1 -Tn ) .....(8) [發明之效果] 如上所詳述,依據本發明時,可提供廉價的、其測定 準備作業及測定作業容易之定向度澜定裝置。又,在定 有含的 會包差 不於程 也對光 算可其 計,論 之又無 紋 。 * 條定又 涉潮 。 干之定 的度測 出確度 顯精向 所高定 於得之 對獲維 ,可纖 中而的 定,品 測誤樣 的錯狀 度數 Η 向計薄 大定之丨 小 定 測維 度織 向的 定值 之負 維現 缕呈 的或 樣維 各纖 種的 各零 於為 對差 可程 , 光 0 狀其定 形對测 面可行 斷也進 或 ,度 , 又向 明 說 單 簡 式 圖圖圖圖 12 3 4 B B 6 6 傑條fe像 圖 成 構 之 構 機 〇 償圖 補成 。差構 圖程之 成光構 構及機 置構傻 裝機補 定光段 測偏分 圖 向 定 維 m 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) ----—---ri — r 於-----—--訂 *----—-----l· (請先閱讀背面之注意事項再填寫本頁) A7 B7 414814 五、發明說明(μ) 第5圖 傑光程差圖。 第6圖 傜觀察圖。 [參考符號說明] 1.....定向度測定裝置 光源機構 觀察機構 分段補償機構 迪續補償機構 合成纖維絲Straight I 1? · Jian Guang uses MU Hezhi's table \)-2 / JV below the rate in ί N fold Δ will be able to axis t dimension. This paper size applies Chinese National Standard (CNS) A4 specification (210x 297 male f) A7 414814 B7_ V. Description of the invention (7) Δ S = (V 0 / V y)-(V 0 / vx) ..... (2) V ο: the speed of light in the atmosphere: the speed of light in the X-axis direction in the material ν X: the speed of light in the direction of the Υ-axis in the material. In this case, ΛN can be expressed by the following formula (3). Δ N = (v〇 / to) X (to / vy -to / νχ) ..... (3) t. : Passing distance of the substance. When T × and T / are the passing time in the substance, AN can be expressed by the following formula (4). △ N = (l / t〇) Xv〇 (Ty -Tx) = (l / t〇) R ..... (4) Τχ: X-direction passage time in the substance T ^: Y-direction passage in the substance Time R = v. (Ty -Tx): The optical path difference of the transmitted light is usually Ty> Tx. The transmitted light of the fiber is shown in Figures 5 (a) and (b). The light in the Y direction will lag. The lag portion is called the optical path difference R (Retardation). When white light is irradiated onto a synthetic fiber silk (F) with an optical path difference R, interference images (iridescent colors composed of multiple colors) appear on the image of the transmitted light of the synthetic ray fiber (F). While observing the interference color with the observation mechanism (3), adjust the wave impedance Η (42) of the segment compensation mechanism (4) and the rotation polarization Η (52) of the flail compensation mechanism (5) to make the optical path difference compensation value f When gradually increasing, the interference color will gradually shift to the low-order inversion (to the dark direction). The β optical path difference compensation value β 'has the function of leading the IT part of the hysteresis of the synthetic fiber reel (F) to the IT axis, such as Compensation to this paper size applies the Chinese National Standard (CNS) A4 (210 X 297 mm) ^^ 1 ^^ 1 ^^ 1 ^^ 1 ^^ 1 ^^ 1 ι— Bn-r Jt. ^^ 1 ^^ 1 ^^ 1 ^^ 1 ^^ 1 ^^ 1 p ^^ 1 ^^ 1 ^^ 1 ^^ 1 ^^ 1 ^^ 1 1. 4 ^ · (Please read the precautions on the back before filling in this Page) Printed by the Consumer Cooperatives of the Intellectual Property Bureau of the Ministry of Economic Affairs A7 414814 B7_ V. Description of Invention (/) When R = R1, as shown in Figures 5 (c) and (d), the light in the X-axis direction and the Y-axis direction The light will become in phase. The light in the same phase cannot transmit through the rotating polarizer (52), so when the light in this state is observed, it will become dark, and a pair of black interference fringes will appear. In this state, the thickness t of the fiber is used. The birefringence ΛN can be found. That is, the birefringence, which is defined as the degree of orientation of the unitary dimension in the synthetic star wire, is obtained by dividing the optical path difference R of the transmitted light by the thickness t. Value to represent. Here, the synthetic gauze silk is not a flat plate having a certain thickness, but a round cross-section. Therefore, the thickness t of the object to be measured. The fiber diameter cannot be used, but a representative thickness 1 that can be replaced is required. Β Therefore, in a synthetic fiber filament with a cross-sectional shape that is approximately circular, if the representative thickness t and the transmitted optical path difference R are calculated, the 2 inclination value can be calculated. Then, the birefringence ΛN defined as the degree of orientation can be obtained. The foregoing is a description of the deformation of the definition formula, and the following is a description of a method for determining the degree of fiber orientation from the formula (4) using the measuring device of the present invention. Assuming that the thickness direction of the synthetic fiber filament (F) parallel to the measurement object is the X-axis direction and the length direction parallel to the y-axis direction, the inclination orientation of each constituent mechanism is arranged in such an orientation as described above. Later, it will exhibit the function of converting ellipsoidal cadmium light into linear polarized light and supplying it to a rotating polarizer. That is, by setting each constituent mechanism at a predetermined orientation, the interference color of the synthetic fiber filament (F) can be displayed, and the stepwise compensation by the wave barrier (42) and the connection by the rotating polarizer (52) can be achieved. Compensation for tangling. And use this two-stage compensation to obtain the weaving dimension orientation. -1 0-The size of this paper applies to China Store Standard (CNS) A4 (210 X 297 mm) -------- ί Sun — Γ I · ---_---- ^ --- ------ Line-I f (Please read the notes on the back before filling out this page) Printed by the Consumer Cooperatives of the Intellectual Property Bureau of the Ministry of Economic Affairs Printed by the Employee Cooperatives of the Intellectual Property Bureau of the Ministry of Economic Affairs Printed by 414814 a7 _B7_ V. Description of the Invention (?) Next, when the fiber is to be placed under a microscope, a liquid having a refractive index approximately the same as the refractive index in the direction of the thickness of the fiber is used to fill the periphery of the fiber. This prevents the reed from directly contacting the atmosphere, avoids complicated refraction of light at the end of the fiber, and accurately determines the degree of orientation. Moreover, it is preferable that the direction in which Pan Wei is placed on the display mirror is such that the longitudinal direction of the strands (Z axis direction) becomes the front-back direction of the microscope. In this way, the alignment position of the fiber under the objective lens and the observation interference phenomenon can be made easier, and the coordinate axis and directivity can be easily aligned on an image processing device or the like. Then, the synthetic light wire (F) is irradiated with white light by the light source mechanism (2). Due to the use of white light, rainbow-colored interfering colors can be displayed on the image of the hybrid M. Because it shows a rainbow interference color, when using a wave retarder to compensate the optical path difference, it can be clearly determined that the wave impedance Η is to be added or subtracted β, and only when the optical path difference is completely compensated This position is the only one that will become dark. Therefore, the judgment that the compensation of the optical path difference has been completed can be made explicitly. Next, a majority of the wave retarders having different optical path difference compensation values are used to compensate the optical path difference of the fiber. The optical path difference compensation value of the wave barrier sheet is, for example, 1 to 3, 3, 9λ, ..., and the like. 1Α is a reference wavelength, and although there is no other limitation, it is ideal to use 5 4 6ηπ in terms of the periodicity and physiological wavelength sensitivity of the interference color displayed by the optical path difference. The wave retarder is used in combination with the X-axis direction or the Υ-axis direction and placed in the addition and subtraction operation notch. The Y-axis direction is additive, and the X-axis direction is subtracted. For example, when 3λ is placed in the Y-axis direction and 1λ is placed in the X-axis direction, the optical path difference compensation value becomes -1 1-This paper is also applicable to the Chinese National Standard (CNS ) A4 specification (210 X 297 mm) • ^ 1 1 ^ 1 n I nn I nt I LI (Please read the unintentional matter on the back before filling this page) A7 414814 B7_ V. Description of the invention () (3λ-1Λ ) β uses 1; 1, 3Λ, 9 and sometimes, it can form a 1λ pitch difference between 1 and 13. If you add a wave barrier that is less than 1, for example, 1 / 9λ, 1/3, and so on, you can form a 1/9 and a pitch difference between 1/9 and ~ (13 + 4 / 3Α). In order to obtain the most effective combination of wave barriers, the optical path difference compensation value of wave barriers e3m χΛ (βι = 0, ± 1, ± 2, ··) is ideal. When βι = -2, -1, 0, 1, 2 is to prepare 1/9 A, 1/3 A, 1 Λ, 3 λ, 9λ. This prevents the combination of wave barriers from repeating, and can achieve a wide range of compensation values with the minimum number of wave barriers required. When the interference color is observed by the observation mechanism (3), and the compensation value of the optical path difference of the wave blocking plate is gradually increased, the interference color will gradually shift to a low order (in the direction of the dark part). The function of the lagging R part leading R1, if adjusted to ίί = ί ′, the lagging part of the light in the direction of the y-axis will be compensated (canceled), and become as shown in Figure 5 (c), (d) Of the state. When you observe the light in this state, what you see is dark. If the fiber is a circular cross-section, a pair of black interference fringes (S) are shown in Figure 6 (b). This image is analyzed by an image processing device (36), and the birefringence is calculated by the following formula. ΔΝ = nA / SQR (Ds -W2) ..... {5) △ N: birefringence enzyme of the fiber η: value of wave resistance Η: reference wavelength D: diameter of circular cross-section fiber -1 2- This paper size applies to China National Standard (CNS) A4 (210 X 297 mm) ------------ l · Animal husbandry ----- 1 ---- Order · ---- -—! Line. I f (Please read the notes on the back before filling out this page) Printed by the Employees 'Cooperatives of the Intellectual Property Bureau of the Ministry of Economic Affairs Printed by the Employees' Cooperatives of the Intellectual Property Bureau of the Ministry of Economic Affairs Printed by 414814 A7 __- * ._B7_ V. Description of the Invention () W: The distance between a pair of black interference fringes of a circular cross-section fiber. In this method, the degree of orientation associated with a normal circular cross-section fiber can be determined by adjusting the wave impedance Η. However, the wave retarder is a step-wise compensation optical path difference, so there is a limit to its minimum compensation value. To measure a raylet (unstretched filament or thin fiber) with a very small optical path difference (l / lfl0; L or less), it is necessary to prepare a small number of optical path differences when measuring with a wave retarder. Wave barriers are not only inefficient and uneconomical. In the case of a fiber having an arbitrary cross-section, a pair of black interference fringes does not appear, so that the formula (4) is not applicable. In this case, the compensation of the wave-resistive sheet is only limited to the coarse adjustment, and the following operations are used to compensate for the light level. "Turn the rotating radial plate (52) in the forward or reverse direction, and entangle it on one side. The compensation of the optical path difference is completely rounded to completely compensate the optical path difference and make it appear in the dark part. The light with a small optical path difference that cannot be fully compensated in the wave barrier is generally elliptically polarized. The conversion mechanism (51) has an optical path difference of 1/4 λ. When disposed in the above orientation, it has the function of converting elliptical polarized light to linear polarized light. Β This principle can be described by the Poincare sphere described in the maple light related literature and the like. (Poincare Sphere) to explain, and here will be explained in detail. The light transmitted from the conversion mechanism becomes linearly polarized light, but its polarization direction is shifted by 0 degrees. The relationship between the degree of residual light ϋ and the direction of polarized light 0 is ϋ = θ / 18 (T · λ. Therefore, when the polarization is rotated by 0 degrees, the direction of polarized light becomes orthogonal and a dark part appears. In a circular cross section 纗In the case of dimensionality, a pair of black interference fringes as shown in the S (b > circle) will appear even though the optical path difference is small. This image is analyzed by the image processing device (36), and can be obtained by the following formula. Double fold-1 3- This paper size applies to China National Standard (CNS) A4 (210 X 297 mm) H · n ^^ 1 ^^ 1 ^^ 1 ^^ 1 ^^ 1 ^^ 1 ^^ 1 I. ™ f (Please read the notes on the back before filling out this page) The Intellectual Property Bureau of the Ministry of Economic Affairs ’employee consumer cooperatives’ seal system shall be zeroed or the thickness shall be zero. Zhou Qi is 0M, the difference is equal to Zhenzhong, etc. The film light makes the turning section thin and the dimensionality of the hand will be thick. When the outer part is thick, some combination ratios are darker and thinner in a certain field. Negative shooting is black, and this is the first one, and it is double-dimensioned at 0. Again, so that the fixed successor is the one. The negative side of the annihilation surface can be regarded as a good one. , Ren's iso-equipment resistance: dimension The optical fiber negative T fiber is determined or used as a measurement, which is beneficial to Θ 414814 A7 〆_B7__ V. Description of the Invention (^) Emissivity. △ N = {η + (θ / 180)} X / {SQR (D 2 -W 2)} ..... (6) △ Ν: birefringence of the fiber η: value of wave resistance M Θ: rotation angle from the reference point of the rotating polarizer and again: reference wavelength D: circular Cross-section fiber diameter W: If the interval between a pair of black interference fringes of a circular cross-section fiber is an arbitrary cross-section fiber, rotate the rotating polarization Η so that it can be placed at an appropriate position (a position where the fiber thickness can be easily measured) Ideally, the dark part is displayed. This image is analyzed by the image processing device (36), and the birefringence can be obtained by the following formula. △ Ν = {η + (0 / 18Ο)} λ / Τ. .... (7) Δ Ν: Pan Wei's birefringence η: value of wave barrier 0: rotation angle from the reference point of the rotating polarizer and again: reference wavelength This paper is fully compliant with Chinese national standards ( CNS) A4 specification (210 X 297 mm) tnn I ^^ 1 IJ (Please read the precautions on the back before filling this page) Printed by the Employees' Cooperatives of the Intellectual Property Bureau of the Ministry of Economic Affairs 414814 A7 _. ._B 7_V. Description of the Invention (M) In addition, some fibers have a refractive index dispersion, and some coloring is observed in the dark part where the optical path difference is compensated. However, in this case, it can be determined by The following steps are used to verify the number K of interference colors. The number K is the η representing the optical path difference K = ηλ. Let the fiber thickness at the position of the η interference fringe be τη, and the successor cone at the position of the η + 1 interference fringe. When the thickness is Tn + i, the number K of interference fringes η can be verified by the formula (8). The measurement methods for τη and τη + 1 are as follows: if a circular cross section is used, the auxiliary line of the cross section can be drawn on the image processing device for measurement. In the case of Panwei with an arbitrary cross section, it can be obtained by a well-known thickness measuring device. Κ = Τη / (Tn + 1 -Tn) ..... (8) [Effect of the invention] As described in detail above, according to the present invention, it is possible to provide a low-cost orientation that is easy to prepare for measurement and easy to perform measurement. Landing device. In addition, there is a difference between the set and the difference, and the calculation can be counted as light, and it is not streaked. * The rules are related to tide. The degree of dryness is determined by the degree of accuracy and accuracy. The accuracy is determined by the obtained pairs, which can be determined in the fiber. The degree of error in the product measurement is wrong. The value of the negative dimension of the fixed value or the zero of each fiber of the sample dimension is the difference between the two, and the shape of the light is 0, and its shape is also feasible for the measurement surface, and the degree, and the simple diagram Fig. 12 3 4 BB 6 6 The texture of the image of the image of the strip is composed by the compensation of the image. The difference between the optical structure and the mechanical structure of the difference patterning process. The deflection profile of the fixed beam segment is determined to the fixed dimension m. This paper size is applicable to the Chinese National Standard (CNS) A4 specification (210 X 297 mm) ------------ ri — R at -------- order * ---------- l · (Please read the notes on the back before filling this page) A7 B7 414814 V. Description of the Invention (μ) Section 5 Tujie optical path difference chart. Figure 6 傜 Observation diagram. [Description of reference symbols] 1 ..... Orientation measuring device Light source mechanism Observation mechanism Segment compensation mechanism Di continued compensation mechanism Synthetic fiber filament

3 4 5 F Μ ....分子鏈 21 - . .光源透鏡 31 · - -光學顯微鏡 D…-照相機 ·* 6 圖像處理裝置 37· · . ·圖像顯示裝置 41 ....固定偏振片 42, 42a,42b · . ·.波阻片 42c · · 波阻片支承體 42cl · _切口部 i 42c2 . . 切口部 2 43 ..切口部 51 - . ·轉換機構 52 . . . ·旋轉偏振片 (請先闓讀背面之注意事項再填寫本頁) %----r----訂---------線 經濟部智慧財產局員工消費合作社印製 -16- 本紙張尺度適用中國國家標準(CNS)A4規格(210x 297公釐)3 4 5 F Μ .... Molecular chain 21-.. Light source lens 31 ·--Optical microscope D ...-Camera · * 6 Image processing device 37 · · · · Image display device 41 .... Fixed polarization Sheets 42, 42a, 42b ...... Wave blocking sheet 42c. Wave blocking sheet support 42cl. _Notch part i 42c2 .. Notch part 2 43 .. Notch part 51-.. Conversion mechanism 52 .. Polarizer (Please read the precautions on the back before filling this page)% ---- r ---- Order --------- Printed by the Consumer Cooperative of the Intellectual Property Bureau of the Ministry of Economic Affairs-16- This paper size applies to China National Standard (CNS) A4 (210x 297 mm)

Claims (1)

414814 a* Be C8 _ D8 六、申請專利範圍 經濟部智慧財1局員工涓費合作社印製 : 之 傖向 線所 折 程 切的觀條 ·, 構 構 補方 直片 之 光 算構由涉 構 機 機 差。 為振 向 由 運機,干 機 償 償 程90換偏 方 出 減傻而之 源 補 補 光變 轉轉 度 顯 加補;生 光 段 績 和改 光旋 細 其 於鐮償産 :之 分 連 ,片,偏的 粗;使 置建補所 由用;的 的 片胆而形如 :的周; 放使的中 係所構間 間 振波.,圓自 括維四光 H,續維 其光機之 之 偏使成橢轉 包M雒色 阻後連纖 ,色察維 維 定可構將反 ,之鑛白 波之差的 置白觀纖 繼 固及所可正 法象於射 痼償程象 裝射的與 與 由,部由和 方對填照 數補光對。 定照用構 構 像片口 葆, 定定充維 多段將定者 測維所機 機,構阻切構構 测測體繼.,的分以测率 度鑛光源 察而機波算機機 度和液對色構差,在射 向的射光 觀.,償値蓮傖換 向是之構涉機程動種折 定象照述 述成補數減補轉 定率同機干償光轉此雙 的對述上 上構段多加缠的 的射相源的補將H析出 維定上在 在所分的的連用。維折致光生段以振解求 潘測察置 置構述同置述所者纖其大用産分,偏構以 種對觀配 配機上不放上光成種以率使所將部轉機 , 一 及 4 值而 偏構一 射 差 口 旋察紋 f ___________* , __;____T I m ^^^1 n ^^^1 ^ ί^ί. ^^1 · (II Ι^ϋ— — ^^^1 I 〆* ,i (請先閱讀背面之注意事項再填寫本s ) 本紙張尺度適用中國國家標準(CNS ) A4規格(210X297公釐)414814 a * Be C8 _ D8 VI. Application for Patent Scope Printed by the staff of the Ministry of Economic Affairs's Smart Finance 1 Bureau: Coordinated by the direction of the direction of the line. Machine is poor. In order to revitalize the aircraft, the machine pays 90 yuan for the remedy, reduces the silly source, and supplements the light, and the degree of rotation is significantly increased. , The film is too thick; the use of the built-in supplements is bold and shaped like: the week; the interoscillation between the structure of the middle system. The circle is enclosed by the four light H, continued The bias of the optical machine causes the fiber to be connected to the fiber after the elliptical subcontracting. The color inspection and maintenance can be reversed, and the difference between the white wave and the white fiber can be fixed and the normal method can be used to shoot. Like shooting with and by, part by and side pairs fill up the number of light pairs. The constellation image is used for fixed photos, and the fixed-filled multi-segments will be used to measure and fix the machine, and the structure will be cut and cut to measure the body. The contrast of the color structure is reflected in the direction of the light. The reversal of the lotus root is related to the mechanical movement of the fixed image, which is described as the complement minus the conversion rate. The complement of the multi-entangled radiographic source in the upper and upper segments will be used in conjunction with the H-precipitation dimension. The dimensional breakage photogenic section uses the solution to find Pan Jiancha's configuration and the same set of descriptions to use its large yield, and the partial configuration is to prevent the machine from turning on to the seeding machine to make the machine turn around. , And one and four values, and a constellation of an azimuthal fractal pattern, f ___________ *, __; ____T I m ^^^ 1 n ^^^ 1 ^ ί ^ ί. ^^ 1 · (II Ι ^ ϋ — — ^ ^^ 1 I 〆 *, i (Please read the notes on the back before filling in this s) This paper size applies to China National Standard (CNS) A4 (210X297 mm)
TW88119053A 1998-11-11 1999-11-02 Measure-device and measure-method for the orientation-degree of a fiber TW414814B (en)

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Publication number Priority date Publication date Assignee Title
CN110426379A (en) * 2019-08-08 2019-11-08 南京林业大学 A kind of rotary timber single fiber sectional area measuring device and method

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CN1910442B (en) * 2004-01-20 2011-04-13 联邦科学和工业研究组织 Method and apparatus for testing fibres

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110426379A (en) * 2019-08-08 2019-11-08 南京林业大学 A kind of rotary timber single fiber sectional area measuring device and method

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