201206562 六、發明說明： 【發明所屬之技術領域】 本發明係有關一 種增點劑造粒物&其製造方法 0 【先前技術】 質’在食 賦*予黏稠 增黏多醋類係具有少 品用途中係廣泛用於調節 性等。 量即可顯現高黏性之性 口感、質地之安定化、 食品用途中廣泛使用之掸 臂黏夕醣類可舉例如：三仙 膠、瓜爾膠、鹿角菜膠、刺槐 判栀旦膠、褐藻酸鈉、聚三葡萄 糖專水溶性高分子，作兮·望 該專増黏多_體當將其粉末本身添 加於液體中時，因分散性不良 K rtq谷易產生結塊，而有在使 結塊完全溶解時會相當費時費力之問題。 為了解決上述問題，而U 丁、+、+ 4 ^ 而以下述方式進行：將增黏多醣 類進行造粒’使分散性提高，而抑制結塊產生。 增黏多酿類之造粒方法已知有下述方法：將作為黏合 劑液體之特定約鹽之溶液進行喷霧來造粒之方法(參照專 利文獻1);將作為黏合劑液體之轉檬酸及/或鱗酸之溶液進 行喷霧來造粒之方法(參照專利文獻2);將作為黏合劑液體 之鉀鹽之溶液進行喷霧來造粒之方法（參照專利文獻3) 等，但依所使用之鹽之種類，有時亦具有苦味和刺鼻味， 而不適於食品用途。 [先前技術文獻] 201206562 (專利文獻） 專利文獻1 :曰本特開2008_68194號公報 專利文獻2 : W02007/13 6083號公報 專利文獻3 : W02006/095756號公報 【發明内容】 [發明所欲解決之問題] 另-方面，在用於以口且嚼、吞噪困難者為對象之飲食 品之用途中，正尋求一種增點劑造粒物，纟分散性良好、 不會產生結塊、黏度會快速上升’並且平衡黏度高，除此 之外亦不會損害飲食品之風味。 、然而，上述之·習知之增#έ多醋類之造粒方法無法充分 滿足該等特性，而尋求更良好之造粒方法。 因此，本發明之目的在於提供一種增黏劑造粒物及其 氣艳方法、以及飲食物，該增黏劑造粒物分散性良好、不 會產生結塊、黏度會快速上升，並且平衡黏度高，除此之 2亦不會損害飲食品之風味，該飲食物係使用前述增黏劑 造粒物，且係以咀嚼、吞嚥困難者為對象。 [解決問題之技術手段] 本發明係為了達成上述目的而提供下述[丨]。 [U—種增黏劑造粒物之製造方法，其係具有下述步驟：將 黏合劑液體喷霧在包含增黏多醣類之初級原料中而獲得初 ' k粒物之步驟；以及使相對於前述增黏多醣類丨〇〇質量 201206562 份為85質量份以上之糊精被覆在前述初級造粒物上之步 驟。 7 此外，本發明係為了達成上述目的而提供下述[2]〜[12] 的發明。 [2]如前述Π]所述之增黏劑造粒物之製造方法，其 ^則述被覆之步驟係包括：將黏合劑液體喷霧在次級原 料中而獲得次級造粒物之步驟，該次級原料係於前述初級 造粒物中添加糊精並混合而得。 P]如前述[1]或前述[2]所述之增黏劑造粒物之製造 法其中，則述被覆之步驟，係使相對於前述增黏多醣 類100質量份為90〜130皙詈价夕她杜、 貨里伤之糊精被覆在前述初級造 粒物上之步驟。 生]如月J述[1 ]至[3 ]中任一項所述之增黏劑造粒物之 製造方法，其中，前述初級原料係包含：相對於前述增黏 多聽類100質量份為(M〜45質量份之糊精。 [5]如别述[1]至[3]中任—項所述之增黏劑造粒物之 1方法’其中’前述初級原料係包含：相對於前述增黏 多酿類100質量份為15〜40質量份之糊精。201206562 VI. Description of the Invention: [Technical Field of the Invention] The present invention relates to a granulating agent granule & Manufacture method 0 [Prior Art] Qualitative 'in the food * viscous thickening vinegar type has less The product is widely used for adjustability and the like. The amount of the high-viscosity taste, the stability of the texture, and the widely used 食品 黏 黏 食品 食品 食品 食品 可 可 可 可 可 可 可 可 可 可 可 可 可 可 可 可 可 可 可 可 可 可 可 可 可 可 可 可 可 可 可 可 可 可 可 可Sodium alginate, polytriglyceride water-soluble polymer, for the purpose of this special 増 _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ It can be quite time consuming and labor intensive to completely dissolve the agglomerates. In order to solve the above problem, U, +, + 4 ^ are carried out in the following manner: granulation of the polysaccharide-promoting polysaccharide is carried out to improve the dispersibility and suppress the occurrence of agglomeration. A method of granulating a viscous multi-flavored granule is known as a method of granulating a solution of a specific salt as a binder liquid (refer to Patent Document 1); A method in which a solution of an acid and/or a scaly acid is sprayed and granulated (see Patent Document 2); a method of spraying a solution of a potassium salt as a binder liquid to granulate (see Patent Document 3), etc. Depending on the type of salt used, it sometimes has a bitter and pungent taste and is not suitable for food use. [Prior Art Document] 201206562 (Patent Document) Patent Document 1: JP-A-2008-68194 Patent Document 2: W02007/13 6083 Patent Document 3: WO2006/095756 [Invention] [The present invention is to be solved In addition, in the use of foods and beverages for people who have difficulty in chewing and swallowing, it is seeking a granulating agent, which has good dispersibility, no caking, and no stickiness. It rises quickly and has a high equilibrium viscosity, which in addition does not damage the flavor of food and beverage. However, the granulation method of the above-mentioned cultivar is not sufficient to satisfy these characteristics, and a better granulation method is sought. Accordingly, it is an object of the present invention to provide a tackifier granule, a glazing method thereof, and a food or drink, which have good dispersibility, no agglomeration, a rapid increase in viscosity, and an equilibrium viscosity. High, in addition to this, it does not impair the flavor of foods and drinks. The foods are made of the above-mentioned tackifier granules, and are intended for those who have difficulty in chewing or swallowing. [Technical means for solving the problem] The present invention provides the following [丨] in order to achieve the above object. [U- a method for producing a viscous granule, which comprises the steps of: spraying a binder liquid into a primary material containing a viscosifying polysaccharide to obtain an initial 'k granule; The step of coating the dextrin of the above-mentioned primary granules with respect to the above-mentioned primary granules in which the mass of the viscous polysaccharides is 201206562 parts is 85 parts by mass or more. Further, the present invention provides the following inventions [2] to [12] in order to achieve the above object. [2] The method for producing a tackifier granule according to the above, wherein the step of coating comprises the step of: spraying a binder liquid into the secondary raw material to obtain secondary granules. The secondary raw material is obtained by adding dextrin to the primary granules and mixing them. The method for producing a thickener granule according to the above [1] or [2], wherein the coating step is 90 to 130 parts by mass based on 100 parts by mass of the polysaccharide of the polysaccharide. At the price of her, the dextrin in the cargo was covered with the above-mentioned primary granules. The method for producing a thickener granule according to any one of the above [1], wherein the primary raw material comprises: 100 parts by mass relative to the thickened polyphonic type ( [1] The method of the viscous granule according to any one of [1] to [3], wherein the aforementioned primary raw material comprises: relative to the foregoing 100 parts by mass of the viscous multi-flavored product is 15 to 40 parts by mass of dextrin.
[6]如前述⑴至[5]中任—項所述之増黏劑造粒物: 1方法’其中，前述增黏多醣類係從三仙膠、來爾膠 H菜膠'刺槐豆膠、褐藻酸納、聚三葡萄U C(carboxymethylcenul〇se^f^ 之種或兩種以上。 [7] 如前述[1]至[6]中任一 項所述之増黏劑造粒物之 201206562 製造方法’其中，前述初級原料中之糊精為與前述用以被 覆之糊精相同種類之糊精。 [8] 如前述[1]至[7]中任一項所述之增黏劑造粒物之 製造方法，其中，前述黏合劑液體為水、或包含2〇質量％ 以下之糊精之水溶液。 [9] 一種增黏劑造粒物，其係藉由前述[1 ]至[8]中任 一項所述之增黏劑造粒物之製造方法所製造。 [10] 如前述[9]所述之增黏劑造粒物，其中，前述增 黏劑造粒物係用於以咀嚼、吞嚥困難者為對象之飲食品。 [U] 一種飲食品，其係包含前述[9]或[1〇]所述之增黏 劑造粒物。 [12] 一種提高增黏多醣類之分散性之方法，其係使 用藉由前述[1]至[8]中任一項所述之增黏劑造粒物之製造 方法所製造之增黏劑造粒物。 [功效] 根據本發明，可提供一種增黏劑造粒物及其製造方 法、以及飲食物，該增黏劑造粒物分散性良好、不會產生 結塊、黏度會快速上升，並且平衡黏度高，除此之外亦不 會損害飲食品之風味，該飲食物係使用前述増黏劑造粒 物，且係以咀嚼、吞嚥困難者為對象。 【實施方式】 [實施發明的較佳形態] 201206562 [本發明之實施形態之增黏劑造粒物之製造方法] 本發明之實施形態之增黏劑造粒物之製造方法，其係 具有下述步驟：將黏合劑液體喷霧在包含增黏多醣類之初 級原料中而獲得初級造粒物之步驟；以及使相對於前述增[6] The viscous granule according to any one of the above-mentioned items (1) to (5), wherein: the method of the above-mentioned viscosifying polysaccharide is from the three sacred gum, the lyre gum, the vegetable gum, the locust bean The granules of the granules of the granules of the granules of the granules of the granules of the granules of the glutenic acid granules 201206562 The method of the present invention, wherein the dextrin in the above-mentioned primary raw material is the same type of dextrin as the above-mentioned dextrin to be coated. [8] The tackifier according to any one of the above [1] to [7] The method for producing a granulated material, wherein the binder liquid is water or an aqueous solution containing 2% by mass or less of dextrin. [9] A tackifier granule by the above [1] to [ (8) The tackifier granule according to the above [9], wherein the tackifier granule is used A food or drink for those who have difficulty in chewing or swallowing. [U] A food or drink comprising the tackifier granule according to the above [9] or [1〇]. [12] An increase in viscosity increase Dispersion of sugar The viscosifier of the tackifier produced by the method for producing a viscous granule according to any one of the above [1] to [8]. [Effect] According to the present invention, A tackifier granule, a method for producing the same, and a food or drink, wherein the tackifier granule has good dispersibility, does not cause agglomeration, has a rapid increase in viscosity, and has high equilibrium viscosity, and does not The flavor of the food or drink is impaired by using the above-mentioned sputum granules, and it is intended to be chewable or swallowed. [Embodiment] [Preferred Embodiment of the Invention] 201206562 [Embodiment of the Invention] Method for producing tackifier granules] A method for producing a tackifier granule according to an embodiment of the present invention, which comprises the steps of: spraying a binder liquid into a primary raw material containing a polysaccharide-promoting polysaccharide And obtaining the steps of primary granulation; and making the increase relative to the foregoing
黏多醣類100質量份為85暫县L 貝里r刀马μ質量伤以上之糊精被覆在前述初 級造粒物上之步驟。 <獲得初級造粒物之步驟> 在本實施形態之獲得初級造粒物之步驟中，係將黏合 劑液體喷霧在包含增黏多醣類之初級原料中。 (初級原料） : 刀級原料係包含增黏多醣類。以包含增黏多醣類及糊 初級原料中之糊精，以包含相對於增黏多聽類⑽ 多ο.1〜45質量份之糊精為佳。以包含相對於增黏 =類⑽質量份為15〜則量份之糊精較佳。以包含相 =黏多酿類⑽質量份為18〜29質量份之糊精更佳。 U相對於增黏多Μ⑽質量份為2G〜24f量份 精最佳。若增黏多醣類及糊精為上述範圍之含量比 將增黏劑造粒物添加於水等中並混合1在 上升，讦n 才貧决逮顯現黏度 並且造粒效率亦優異。在快速顯現黏度上升之觀點 ^包含相對於增黏多聽類⑽f量份為2q〜M^ ^精特佳。若糊精含量相對於增黏多釀類: 使用之IT則在隨後之使糊精被覆之步驟中，被覆時可 a減少’故將增黏劑造粒物添加於水等中時之分 心化’而會產生結塊。 201206562 初級原料中之糊精’以與在隨後之使糊精被覆之步驟 中所被覆之糊精相同種類之糊精為佳，其原因為： 之混亂和操作錯誤較少。 (增黏多醣類） 在本實施形態令，增黏多醣類係無特別限定，從容解 後之黏度上升性優異等之觀點來看，以從三仙膠、瓜爾膠、 鹿角菜膠、刺槐豆膠、褐藻酸鈉、聚三葡萄糖、及c 鹽之中選出之-種或兩種以上為佳。特別是，以從三仙勝' 瓜爾膠、刺槐豆膠、及CMC鈉鹽 / ,.+ 乂115;種或兩種以 為佳。以使用三仙膠、瓜爾膠、及CMC鈉鹽最佳。 三仙膠以在初級原料中包含使增黏劑造粒物中之三仙 膠之含量成為30〜45質量％之量為佳。以33〜43質： 較佳，以35〜40質量％更佳。 〇 瓜爾膠以在初級原料中包含使增黏劑造粒物中 膠之含量成為〇5〜3晳暑〇/夕旦 巧，5 3質量叙篁為佳。以1〜3質量％較 佳，U 1〜2.5質量％更佳。 CMC鈉鹽以在初級原料中包含使増黏劑造粒物中 CMC鈉鹽之含量成為卜4質量％之量為佳。以μ〜 置％較佳，以1>5〜2 5 f量％更佳。 (黏合劑液體） 噴霧在初級原料中之黏合劑液體，以水、或包含2〇質 里/6以下之糊精之水溶液為佳。以包含糊精丄〜汕質量％ 之水溶液為佳，以包含5〜2G質量％之水溶液較佳，以^ 含5〜15質量％之水溶液更佳。 201206562 關於在隨後之使糊精被覆之步驟中所使用之黏合劑液 體，亦與上述相同。 在本步驟及隨後之使糊精被覆之步驟中，所噴霧之上 述黏合劑液體之總量，以所噴霧之糊精是相當於所製造之 增黏劑造粒物之總量之1〜10質量％之液量為佳。以3〜8 質量％較佳。 在本實施形態中’所使用之黏合劑液體中之糊精以與 初級原料中之糊精相同種類之糊精為佳，其原因為：生產 時之混亂和操作錯誤較少。 此外’除了糊精以外’黏合劑液體亦可包含增黏多醣 類。可包含例如：三仙膠。 <使糊精被覆在初級造粒物上之步驟> 在使糊精被覆之步驟中’係使相對於初級原料中之增 黏多醣類100質量份為85質量份以上之糊精被覆在上述步 驟中所得之初級造粒物上。以使相對於增黏多醣類丨〇〇質 量份為90〜130質量份之糊精被覆為佳。以使95〜12〇質 量份之糊精被覆較佳。以11 〇〜115質量份更佳，以！ 〇〇〜 11〇質量份最佳。若在上述範圍内使糊精被覆在初級造粒 物上’則可獲得一種增黏劑造粒物，其不會產生結塊，而 容易分散。 使糊精被覆在初級造粒物上之步驟，具體而言以包括 將黏合劑液體喷霧在次級原料中而獲得次級造粒物之步 驟，該次級原料係於上述初級造粒物中添加糊精並混合而 得為佳。此外，亦可依需要而在次級造粒物中添加糊精並 201206562 混合再使黏合劑液體噴霧在其中而獲得三級造粒物，亦可 進一步同樣進行而獲得四級或四級以上的造粒物。換言 之，亦可分成數個階段來進行使糊精被覆在初級造粒物上 之步驟，從製造效率等之觀點來看，宜為一次，亦即以次 級造粒物作為目標之增黏劑造粒物。 <造粒方法> 本貫施形態之獲得初級造粒物之步驟及使糊精被覆之 步驟中，造粒方法可舉例如：流動層造粒法、授拌造粒法、 轉動式造粒法、及塗佈造粒法.，以流動層造粒法特佳。 流動層造粒法係藉由下述方式來獲得初級造粒物，例 如：將粉體（初級原料）置入流動層造粒法塗佈裝置中，並 從下方送入加熱至50〜i〇〇°c之暖風，來使粉體流動並混 合，從上方以喷嘴將上述黏合劑液體喷霧在該流動層，均 勻地以3〜5mL/min、氣壓〇.5〜15MPa將黏合劑液體喷霧 在粉體表面，來製造凝聚粒後，使其乾燥。其次，暫時停 止流動層造粒法塗佈裝置之運轉’在裝置中額外投入糊 精，並從裝置之下方吹入加熱至5〇〜1〇(rc之暖風，來使初 級造粒物及額外加入之糊精流動並混合，而獲得次級原 料，對於該次級料’可藉由以與上述相同的條件進行造 粒後使其乾燥，來製造增黏劑造粒物（次級造粒物 [本發明之實施形態之增黏劑造粒物] 本發明之實施形態之增黏劑造粒物係以上述製造方法 所製造者，可適於使用作為飲食品，特別是可適於使用作 為以㈣、吞❹難者為對象之飲食品。經由使用該增黏 201206562 劑造粒物’即可使料多醣類在水巾等之分散性提高。 果汁飲料、菜汁飲料 維他命補給飲料、營養 法式清湯、濃湯、奶油 清湯’可直接添加於該 添加本發明之實施形態之增黏劑造粒物之對象飲食品 無特別限定，可舉例如：水、牛乳、乳飲料、乳酸菌飲料、 摻有果汁之清涼飲料、碳酸飲料 茶飲料、運動飲料、機能性飲料 補給平衡飲料、葡萄酒等水果酒 濃湯、中式湯等各種湯、味噌湯 等中使液體增黏。 [本發明之實施形態之功效] 根據本&明之實施形_’可提供—種增黏劑造粒物及 -製造方法，該增黏劑造粒物分散性良好、不會產生結塊、 點度會快速上升，並且平衡黏度高，除此之外亦不會損害 飲食品之風味。因&，可提供—種增黏劑造粒物及其製造 方法’該增黏劑造粒物之較佳的用途係用於以n且嚼 困難者為對象之飲食品。 ”、 其次’藉由實施例來說明本發明，但本發明並不受此 寻貫施例所限定。 [實施例] [增黏劑造粒物之製造] 第1圖係表示實施例及比較例之掷 製 f彳]之増黏劑造粒物之概略 化·步驟之流程圖。 藉由流動層造粒法，按照表1〜2 述順皮A s己載之調配，並以下 來製造實施例1〜5及比較例1之增黏劑造粒物。 201206562 首先，秤量各原料後，分別準備初級原料及黏合劑液 體（10質量％糊精水溶液100g)，並將初級原料投入流動層 造粒塗佈裝置（商品名：SFC_LABO, FREUND產業（股）製） 中’並從該裝置之底部吹人加熱至75t之暖風，來使粉體 流動並現合。接著，從該裝置之上部之噴霧喷嘴以 5mL/min、氣壓〇』MPa將上述黏合劑液體喷霧在初級原料 中來進行造粒後，使其乾燥，藉此獲得初級造粒物。 其次，暫時停止流動層造粒法塗佈裝置之運轉，在裝 置中額外投入與初級原料中之糊精相同種類之糊精，並從 該裝置之底部吹入加熱至75。(：之暖風，來使初級造粒物及 額外加入之糊精流動並混合，而獲得次級原料，對於該次 級原料，藉由以與上述相同的條件進行造粒後使其乾燥， 而獲得增黏劑造粒物（次級造粒物）。 藉由流動層造粒法，按照表2記載之調配，並以下述 順序’來製造比較例2之增黏劑造粒物。 首先，秤量各原料後，分別準備初級原料及黏合劑液 體（10質量％糊精水溶液）’並將初級原料投入流動層造粒 塗佈裝置（商品名：SFC-LABO，FREUND產業（股）製）中， 並從該裝置之底部吹入加熱至75。(：之暖風，來使粉體流動 並混合。接著，從該裝置之上部之噴霧噴嘴以5mL/min、 氣壓0.8MPa將所準備之黏合劑水溶液噴霧後使其乾燥，藉 此獲得增黏劑造粒物（初級造粒物）。 12 201206562 [表l] 實施例1 實施例2 實施例3 實施例4 實施例5 增黏劑造粒物之調配 上列：調配量(g) (下列：質畺％) 三仙膠 76 (38.0) 76 (38.0) 76 (38.0) 76 (37.0) 76 (38.0) 瓜爾膠 3 (1.5) 3 (1.5) 4 (2.0) 2 (1.0) 3 (1.5) CMC-Na 4 (2.0) 4 (2.0) 4 (2.0) 4 (2.0) 4 (2-0) 糊精 117 (58.5) 117 (58.5) 116 (58.0) 120 (60.0) 117 (58.5) 合計 200 (100.0) 200 (100.0) 200 (100.0) 200 (100.0) 200 (100.0) 初級原料之調配 上列：調配量(g) (下列：質量％) 三仙膠 A 76 (66.1) 76 (75.2) 76 (74.5) 74 (82.2) 76 (91.3) 瓜爾膠 B 3 (2.6) 3 (3.0) 4 (3.9) 2 (2-2) 3 (3.6) CMC-Na C 4 (3.5) 4 (4.0) 4 (3.9) 4 (4.4) 4 (4.8) 糊精 D 32 (27.8) 18 (17.8) 18 (17.6) 10 (11.1) 0.2 (0.2) 合計 115 (100.0) 101 (100.0) 102 (100.0) 90 (100.0) 83.2 (100.0) 次級原料中之糊精之調配量E (R) 75 89 88 100 106.8 所喷霧之黏合劑液體中之糊精之 量 上列：調配量(g) (下列：質量％) 10 (10) 10 (10) 10 (10) 10 (10) 10 (10) 次級原料中之糊精相對於初級原 料中之增黏多酶類100質量份之 量(質量份） E/(A+B + C)xl00 90.4 107.2 104.8 125.0 128.7 初級原料中之糊精相對於初級原 料中之增黏多醣類100質量份之 量(質量份） D/(A+B + C)xl00 38.6 21.7 21.4 12.5 0.2 13 201206562 [表2] 比較例1 比較例2 增黏劑造粒物之調配 上列：調配量(g) (下列：質量％) 三仙膠 76 (38.0) 76 (38.0) 瓜爾膠 3 (1.5) 3 (1.5) CMC-Na 4 (2.0) 4 (2.0) 糊精 117 (58.5) 117 (58.5) 合計 200 (100.0) 200 (100.0) 初級原料之調配 上列：調配量(g) (下列：質量％) 三仙膠 A 76 (61.8) 76 (40.0) 瓜爾膠 B 3 (2.4) 3 (1.6) CMC-Na C 4 (3-3) 4 (2.1) 糊精 D 40 (32.5) 107 (56.3) 合計 123 (100.0) 190 (100.0) 次級原料中之糊精之調配量E (R) 67 — 所喷霧之黏合劑液體中之糊精之量 上列：調配量(g) (下列：質量％) 10 (10) 10 (10) 次級原料中之糊精相對於初級原料中之增黏多醣類 100質量份之量(質量份） E/(A+B + C)xl00 80.7 — 初級原料中之糊精相對於初級原料中之增黏多醣類 100質量份之量(質量份） D/(A+B + C)xl00 48.2 128.9 [增黏劑造粒物之評估1] 對於所得之增黏劑造粒物，分別進行下述評估。評估 結果如表3〜4所示。 (水中之分散性及抑制結塊產生之評估） 一面以藥匙來攪拌水（商品名：南阿爾卑斯之天然水， SUNTORY(股）製）100g，一面添加增黏劑造粒物1.5g，並藉 由目視確認後，以下述三階段來評估分散性及抑制結塊產 14 201206562 生。 〇：增黏劑造粒物立刻分散在整個 之狀態 尺中而未產生結塊 △:增黏劑造粒物雖立刻分散在整個水中 結塊之狀態 一二开 x:增黏劑造粒物難以分散而產；ψ *县从 苽阳座生大置結塊之狀態 (黏度之評估） 藉由下述方法來測定上升黏度及平衡黏度，並進行評 估。黏度係使用黏度計（T0KIMEC公司製，型號: visc〇meter(model:bm))之轉子 N〇 3，以心㈣之轉 數進行測定β 、上升黏度：以上述在水中之分散性及抑制結塊產生之 評估中添加增黏劑造粒物之30秒後之黏度之測定值作為 上升黏度，以下述三階段進行評估。 ◎:為1500mPa. s以上而黏度快速上升，顯著良好 Ο :為PGOmPa. s以上且小於丨則s而黏度快 速上升，良好 X :小於900mPa . s而黏度緩慢上升 平衡黏度：以上述在水中之分散性及抑制結塊產生之 评估中添加增黏劑造粒物之60分鐘後之黏度之測定值作 為平衡黏度，以下述兩階段進行評估。 〇：為3000mPa . s以上而平衡黏度高 X :小於3000mPa . s而平衡黏度低 15 201206562 [表3] 實施例2 n〇n ◎ 1700 實施例3_ ~------ 貫施例4 實施例5 〇 ~~〇 ~ 〇 ◎ 2000 〇~ 950 〇 1050 〇 Γ〇 3600 [〇 3〇〇〇 卜〇 3500 上升考…工 中之分散性、抑制結塊產生、 上升黏度及平衡黏度之任一 m m ^ ^ 者句良好，而可作為以咀嚼、 吞％困難者為對象之水來使用。 [表4]100 parts by mass of the mucopolysaccharide is a step of coating the above-mentioned primary granules with 85 d. <Step of obtaining primary granules> In the step of obtaining the primary granules of the present embodiment, the binder liquid is sprayed in the primary raw material containing the polysaccharide-promoting polysaccharide. (Primary material): The knife-grade raw material contains a polysaccharide-promoting polysaccharide. Preferably, the dextrin containing the polysaccharide of the viscosity-increasing polysaccharide and the paste is contained in an amount of more than 0.1 to 45 parts by mass relative to the multi-viscosity (10). It is preferred to include a dextrin having a content of 15 to about 10 parts by mass relative to the viscosity-increasing class (10) parts by mass. More preferably, the dextrin is contained in an amount of 18 to 29 parts by mass based on 10 parts by mass of the phase. U is preferably the best in terms of 2G to 24f parts by mass fraction of the multiparticulate (10). If the viscosity-increasing polysaccharides and dextrin are in the above range, the tackifier granules are added to water or the like and the mixture 1 is raised, and the 讦n is depleted to exhibit viscosity and excellent granulation efficiency. In the point of view of the rapid increase in viscosity, it is better than 2q~M^^, which is more than the weight-increasing multi-audio class. If the dextrin content is relative to the thickening and multi-brewing: The IT used will be reduced in the subsequent step of covering the dextrin, so that the disintegration of the tackifier granules in the water or the like is added. It will produce agglomeration. 201206562 The dextrin in the primary raw material is preferably the same kind of dextrin as the dextrin which is covered in the subsequent step of covering the dextrin, because the confusion and the operational error are small. (Tackified Polysaccharide) In the present embodiment, the polysaccharide-promoting polysaccharide is not particularly limited, and is excellent in viscosity increase after the completion of the solution, and is based on Sanxian gum, guar gum, and carrageenan. Preferably, one or more of the locust bean gum, sodium alginate, polytriglucose, and c salt are selected. In particular, it is preferable to use three kinds of guar gum, guar gum, locust bean gum, and CMC sodium salt / , .+ 乂 115; or two. It is best to use Sanxian gum, guar gum, and CMC sodium salt. The triterpene gum preferably contains, in the primary raw material, the content of the tri-skin in the tackifier granules in an amount of 30 to 45 mass%. The mass is 33 to 43: preferably, it is preferably 35 to 40% by mass. 〇 Guar gum is included in the primary raw material to make the content of the glue in the viscosifier granules 〇5~3 〇 〇 夕 夕 夕 夕 夕 夕 夕 夕 夕 夕 夕 夕 夕 夕 夕 夕 夕 夕 夕 夕 夕 夕 夕 夕 夕 。 It is preferably 1 to 3 mass%, more preferably U 1 to 2.5 mass%. The CMC sodium salt is preferably contained in the primary raw material in an amount such that the content of the CMC sodium salt in the granule granule is 4% by mass. Preferably, it is preferably in the range of μ and 5 %, and more preferably in the range of 1 > 5 to 2 5 f. (Binder liquid) The binder liquid sprayed in the primary raw material is preferably water or an aqueous solution containing 2% or less of dextrin. The aqueous solution containing dextrin 丄~汕% by mass is preferably an aqueous solution containing 5 to 2% by mass, more preferably 5 to 15% by mass. 201206562 The binder liquid used in the subsequent step of covering the dextrin is also the same as described above. In this step and the subsequent step of coating the dextrin, the total amount of the above-mentioned adhesive liquid sprayed is 1 to 10 of the total amount of the granulated granules produced by the dextrin sprayed. The mass % of the liquid is preferred. It is preferably 3 to 8 mass%. In the present embodiment, the dextrin in the binder liquid used is preferably the same type of dextrin as the dextrin in the primary raw material, because the production is disordered and the operation error is small. Further, the 'adhesive liquid other than dextrin may also contain a polysaccharide-promoting polysaccharide. It may include, for example, Sanxian gum. <Step of coating dextrin on primary granules> In the step of coating dextrin, 'the dextrin coating is 85 parts by mass or more with respect to 100 parts by mass of the thickening polysaccharide in the primary raw material On the primary granules obtained in the above steps. It is preferred that the dextrin coating is 90 to 130 parts by mass based on the weight of the polysaccharide of the polysaccharide. It is preferred to coat the dextrin in a mass ratio of 95 to 12 Å. It is better to use 11 〇 ~ 115 parts by mass! 〇〇 ~ 11 〇 the best quality. If the dextrin is coated on the primary granules within the above range, a tackifier granule can be obtained which does not cause agglomeration and is easily dispersed. a step of coating the dextrin on the primary granules, specifically comprising the step of obtaining a secondary granule by spraying a binder liquid in the secondary raw material, the secondary raw material being attached to the primary granulated material Adding dextrin and mixing it is better. In addition, dextrin may be added to the secondary granules as needed, and 201206562 may be mixed to spray the binder liquid therein to obtain the third-stage granules, and the quaternary granules may be further obtained in the same manner to obtain the quaternary or higher grading. Granulation. In other words, the step of coating the dextrin on the primary granules may be carried out in several stages, and from the viewpoint of production efficiency and the like, it is preferably one time, that is, a tackifier which is targeted by secondary granules. Granulation. <Pelletization method> In the step of obtaining the primary granules and the step of coating the dextrin in the present embodiment, the granulation method may be, for example, a fluidized bed granulation method, a granulation method, or a rotary granulation method. The granulation method and the coating granulation method are particularly preferred by the flow layer granulation method. The fluidized bed granulation method obtains primary granules by, for example, placing a powder (primary material) in a fluidized bed granulation coating apparatus and feeding it from below to heat up to 50 〜 〇暖°c warm air, so that the powder flows and mixes, spray the above binder liquid on the flowing layer from above with a nozzle, uniformly to 3~5mL/min, pressure 〇5~15MPa to bond the liquid Spray on the surface of the powder to make agglomerated grains and then dry them. Secondly, temporarily stop the operation of the flow layer granulation coating device. 'Adding dextrin to the device and blowing it to the bottom of the device to 5 〇 1 〇 (rc warm air to make the primary granules and The additional dextrin is flowed and mixed to obtain a secondary raw material, and the secondary material can be produced by granulating and drying it under the same conditions as above to produce a tackifier granule (secondary build Granules [Tackifier granules according to the embodiment of the present invention] The tackifier granules of the embodiment of the present invention are produced by the above-described production method, and can be suitably used as foods and drinks, and are particularly suitable for use. By using the foods and beverages for the purpose of (4) and swallowing, the dispersibility of the polysaccharides in water towels and the like can be improved by using the viscous material of the viscous 201206562 granules. Vitamin beverages, vegetable juice beverages, vitamin supplements The foods and beverages which can be directly added to the viscous granules of the embodiment of the present invention are not particularly limited, and examples thereof include water, cow's milk, milk beverage, and lactic acid bacteria. Beverage, blend The juice is thickened by a refreshing drink of a fruit juice, a carbonated beverage tea beverage, a sports drink, a functional beverage replenishment balanced drink, a fruit wine soup such as wine, a soup such as a Chinese soup, a miso soup, and the like. Efficacy] According to the present embodiment, it is possible to provide a tackifier granule and a manufacturing method which have good dispersibility, no agglomeration, rapid rise in point, and High balance viscosity, in addition to the taste of food and beverage, because of &, can provide a kind of tackifier granules and its manufacturing method 'The preferred use of the tackifier granules The present invention is described by the following examples, but the present invention is not limited by the above examples. [Examples] [Adhesive granulation] Manufacture of the material] Fig. 1 is a flow chart showing the outline and steps of the granule granules of the examples and the comparative examples. The flow layer granulation method is described in Tables 1 to 2 The production of the cis-A s has been carried out, and the following examples 1 to 5 are produced. The tackifier granules of Example 1. 201206562 First, after weighing each raw material, prepare a primary raw material and a binder liquid (100 g of a 10 mass % dextrin aqueous solution), and put the primary raw material into a fluidized bed granulation coating apparatus (product Name: SFC_LABO, FREUND Industry Co., Ltd.) and 'heated from the bottom of the device to 75t of warm air to make the powder flow and recombine. Then, from the spray nozzle on the top of the device to 5mL / Min, air pressure 〇 MPa The above-mentioned binder liquid is sprayed in the primary raw material to be granulated, and then dried to obtain primary granules. Next, the operation of the fluidized bed granulation coating device is temporarily stopped. The same type of dextrin as the dextrin in the primary material was additionally charged in the apparatus, and heated to 75 from the bottom of the apparatus. (: the warm air, the primary granules and the additionally added dextrin are flowed and mixed to obtain a secondary raw material, and the secondary raw material is granulated and dried by the same conditions as above, The tackifier granules (secondary granules) were obtained. The viscous granules of Comparative Example 2 were produced by the flow layer granulation method according to the formulation described in Table 2 in the following order. After weighing each raw material, prepare the primary raw material and the binder liquid (10% by mass aqueous solution of dextrin), and put the primary raw material into a fluidized layer granulation coating device (trade name: SFC-LABO, FREUND Industry Co., Ltd.) And, from the bottom of the device, heat is applied to 75. (: warm air to make the powder flow and mix. Then, prepare from the spray nozzle at the top of the device at 5 mL/min, pressure 0.8 MPa. The aqueous binder solution is sprayed and dried to obtain tackifier granules (primary granules). 12 201206562 [Table 1] Example 1 Example 2 Example 3 Example 4 Example 5 The distribution of the granules is listed above: the amount of blending (g) (the following:畺%) Sanxianjia 76 (38.0) 76 (38.0) 76 (38.0) 76 (37.0) 76 (38.0) Guar 3 (1.5) 3 (1.5) 4 (2.0) 2 (1.0) 3 (1.5) CMC -Na 4 (2.0) 4 (2.0) 4 (2.0) 4 (2.0) 4 (2-0) Dextrin 117 (58.5) 117 (58.5) 116 (58.0) 120 (60.0) 117 (58.5) Total 200 (100.0) 200 (100.0) 200 (100.0) 200 (100.0) 200 (100.0) Preparation of primary raw materials listed above: blending amount (g) (below: mass%) Sanxianjiao A 76 (66.1) 76 (75.2) 76 (74.5 74 (82.2) 76 (91.3) Guar B 3 (2.6) 3 (3.0) 4 (3.9) 2 (2-2) 3 (3.6) CMC-Na C 4 (3.5) 4 (4.0) 4 (3.9 4 (4.4) 4 (4.8) Dextrin D 32 (27.8) 18 (17.8) 18 (17.6) 10 (11.1) 0.2 (0.2) Total 115 (100.0) 101 (100.0) 102 (100.0) 90 (100.0) 83.2 (100.0) The amount of dextrin in the secondary raw material E (R) 75 89 88 100 106.8 The amount of dextrin in the sprayed liquid of the sprayed liquid is listed above: Formulation amount (g) (hereinafter: mass%) 10 (10) 10 (10) 10 (10) 10 (10) 10 (10) The amount of dextrin in the secondary raw material relative to 100 parts by mass of the multi-adhesive multi-enzyme in the primary raw material (parts by mass) E/(A) +B + C)xl00 90.4 107.2 104.8 125.0 128.7 The amount of the dextrin in the raw material relative to 100 parts by mass of the polysaccharide of the primary raw material (parts by mass) D / (A + B + C) x l00 38.6 21.7 21.4 12.5 0.2 13 201206562 [Table 2] Comparative Example 1 Comparative Example 2 Formulation of tackifier granules Top: Formulation amount (g) (below: mass%) Sanxianjia 76 (38.0) 76 (38.0) Guar gum 3 (1.5) 3 (1.5) CMC-Na 4 (2.0) 4 (2.0) Dextrin 117 (58.5) 117 (58.5) Total 200 (100.0) 200 (100.0) Preparation of primary raw materials listed above: Formulation amount (g) (The following: mass%) Sanxianjiao A 76 (61.8) 76 (40.0) Guar B 3 (2.4) 3 (1.6) CMC-Na C 4 (3-3) 4 (2.1) Dextrin D 40 (32.5) 107 (56.3) Total 123 (100.0) 190 (100.0) The amount of dextrin in the secondary raw material E (R) 67 - the amount of dextrin in the sprayed liquid of the sprayed above: the amount of blending (g) (below: mass%) 10 (10) 10 (10) The amount of dextrin in the secondary raw material relative to 100 parts by mass of the polysaccharide in the primary raw material (parts by mass) E/(A+B + C)xl00 80.7 — the relative dextrin in the primary raw material 100 parts by mass of the polysaccharide-promoting polysaccharide in the primary raw material (parts by mass) D/(A+B + C) xl00 48.2 128.9 [Evaluation of tackifier granules 1] For the obtained tackifier granules, the following evaluations were respectively carried out. The evaluation results are shown in Tables 3 to 4. (Evaluation of the dispersibility in the water and the inhibition of the formation of agglomerates) While stirring 100 g of water (trade name: natural water of Southern Alps, manufactured by SUNTORY Co., Ltd.) with a spatula, 1.5 g of a viscous granule was added thereto. After visual confirmation, the dispersibility and inhibition of agglomeration production were evaluated in the following three stages. 〇: The viscosifier of the tackifier is immediately dispersed in the whole state without causing agglomeration. △: The granules of the tackifier are immediately dispersed in the whole water and agglomerated. One open and two open x: tackifier granules It is difficult to disperse and produce; ψ * County from the Fuyang Block, the state of the agglomeration (viscosity evaluation) The rising viscosity and the equilibrium viscosity were measured by the following methods and evaluated. The viscosity is measured by the rotor N〇3 of a viscometer (manufactured by T0KIMEC, model: visc〇meter (model: bm)), and the number of revolutions of the heart (four) is measured. β, rising viscosity: the above dispersibility in water and suppression of knots The measured value of the viscosity after 30 seconds from the addition of the tackifier granule in the evaluation of the block generation was evaluated as the rising viscosity in the following three stages. ◎: 1500mPa·s or more and the viscosity rises rapidly, which is significantly good Ο: PGOmPa. s or more and less than 丨 s and the viscosity rises rapidly, good X: less than 900mPa. s and the viscosity slowly rises. Balance viscosity: in the above water The measurement of the viscosity after 60 minutes from the addition of the tackifier granules in the evaluation of dispersibility and suppression of agglomeration generation was evaluated as the equilibrium viscosity in the following two stages. 〇: 3,000 mPa·s or more and equilibrium viscosity is high X: less than 3000 mPa. s and equilibrium viscosity is low 15 201206562 [Table 3] Example 2 n〇n ◎ 1700 Example 3_~------ Example 4 Implementation Example 5 〇~~〇~ 〇◎ 2000 〇~ 950 〇1050 〇Γ〇3600 [〇3〇〇〇卜〇3500 Rising test...Dispersibility at work, inhibition of agglomeration generation, rising viscosity and equilibrium viscosity The mm ^ ^ sentence is good, but can be used as water for those who chew and swallow. [Table 4]
[增黏劑造粒物之評估2] 對於所得之增點劑造粒物（實施例2 進行分散性及抑制結塊卜這方法來 味之評估。 塊產生之㈣、黏度之評估、以及風 (健康飲料） ® Μ Μ授拌健康飲料（商品名·寶礦力水得，大 二樂品(股)製)10。卜面添加實施例2之增黏劑造粒物 g後L果立刻分散在整個液中而未產生結塊，且黏度 現亦良好述之評估基準進行評估後，上升黏度為 平衡黏度為〇）。此經賦予黏稠性之健康飲料的風味亦 而可作為以嚼、吞嚷困難者為對象之健康飲料來 201206562 (茶） 樂喊來攪拌茶(商品名：〇i茶，（股)伊 制、ιηΛ 〜.余，（股）伊藤園 製）、g，—面添加實施例2之增黏劑造粒物i5g後，結果 义d刀散在整個液中而未產生結塊，且黏度顯現亦良好（以 前述之評估基準進行評估後，上升黏度為◎，平衡黏度為 〇）。此經賦予黏稠性之茶的風味亦良好，而可作為以咀 嚼、吞藥困難者為對象之茶來使用。 【圖式簡單說明】 第1圖係表示實施例及比較例之增黏劑造粒物之概略 製造步驟之流程圖。 【主要元件符號說明】[Evaluation of tackifier granules 2] Evaluation of the obtained granules of granules (Example 2 for dispersibility and inhibition of agglomeration). Bulk generation (IV), viscosity evaluation, and wind (healthy drink) ® Μ Μ Μ 健康 健康 健康 健康 Μ Μ Μ Μ Μ Μ Μ Μ Μ Μ Μ Μ Μ Μ Μ Μ Μ Μ Μ Μ Μ Μ Μ Μ Μ Μ Μ Μ Μ Μ Μ Μ Μ 健康 健康 健康 健康 健康 健康 健康 健康Dispersed in the whole liquid without agglomeration, and the viscosity is also well evaluated as the evaluation criteria, the rising viscosity is the equilibrium viscosity 〇). The flavor of the viscous health drink can also be used as a healthy drink for those who have difficulty in chewing and swallowing. 201206562 (Tea) screaming to stir the tea (trade name: 〇i tea, (share), Ιη,~.余, (股) Itoyuan system), g, - surface added the adhesion promoter granule i5g of Example 2, the result d knife scattered in the whole liquid without agglomeration, and the viscosity appeared also good ( After evaluation based on the aforementioned evaluation criteria, the ascending viscosity was ◎ and the equilibrium viscosity was 〇). The viscous tea is also excellent in flavor, and can be used as a tea for those who have difficulty in chewing or swallowing. BRIEF DESCRIPTION OF THE DRAWINGS Fig. 1 is a flow chart showing the outline manufacturing steps of the tackifier granules of the examples and the comparative examples. [Main component symbol description]