TW201129574A - Novel thermal radical generating agent, method for producing same, liquid crystal sealing agent and liquid crystal display cell - Google Patents
Novel thermal radical generating agent, method for producing same, liquid crystal sealing agent and liquid crystal display cellInfo
- Publication number
- TW201129574A TW201129574A TW099139293A TW99139293A TW201129574A TW 201129574 A TW201129574 A TW 201129574A TW 099139293 A TW099139293 A TW 099139293A TW 99139293 A TW99139293 A TW 99139293A TW 201129574 A TW201129574 A TW 201129574A
- Authority
- TW
- Taiwan
- Prior art keywords
- liquid crystal
- group
- radical generating
- hydrogen atom
- agent
- Prior art date
Links
- 239000003795 chemical substances by application Substances 0.000 title abstract 6
- 239000004973 liquid crystal related substance Substances 0.000 title abstract 6
- 238000007789 sealing Methods 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 125000004435 hydrogen atom Chemical group [H]* 0.000 abstract 5
- KGSFMPRFQVLGTJ-UHFFFAOYSA-N 1,1,2-triphenylethylbenzene Chemical class C=1C=CC=CC=1C(C=1C=CC=CC=1)(C=1C=CC=CC=1)CC1=CC=CC=C1 KGSFMPRFQVLGTJ-UHFFFAOYSA-N 0.000 abstract 3
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical group [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 abstract 1
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- 238000011109 contamination Methods 0.000 abstract 1
- 125000001301 ethoxy group Chemical group [H]C([H])([H])C([H])([H])O* 0.000 abstract 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 abstract 1
- 238000005187 foaming Methods 0.000 abstract 1
- 125000005843 halogen group Chemical group 0.000 abstract 1
- 230000001939 inductive effect Effects 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 125000000956 methoxy group Chemical group [H]C([H])([H])O* 0.000 abstract 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 abstract 1
- 125000000951 phenoxy group Chemical group [H]C1=C([H])C([H])=C(O*)C([H])=C1[H] 0.000 abstract 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 abstract 1
- 229910052710 silicon Inorganic materials 0.000 abstract 1
- 229920001187 thermosetting polymer Polymers 0.000 abstract 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L63/00—Compositions of epoxy resins; Compositions of derivatives of epoxy resins
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
- C07F7/1804—Compounds having Si-O-C linkages
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/14—Polycondensates modified by chemical after-treatment
- C08G59/1433—Polycondensates modified by chemical after-treatment with organic low-molecular-weight compounds
- C08G59/1438—Polycondensates modified by chemical after-treatment with organic low-molecular-weight compounds containing oxygen
- C08G59/1455—Monocarboxylic acids, anhydrides, halides, or low-molecular-weight esters thereof
- C08G59/1461—Unsaturated monoacids
- C08G59/1466—Acrylic or methacrylic acids
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/40—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
- C08G59/4007—Curing agents not provided for by the groups C08G59/42 - C08G59/66
- C08G59/4014—Nitrogen containing compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Emergency Medicine (AREA)
- General Chemical & Material Sciences (AREA)
- Sealing Material Composition (AREA)
- Polymerisation Methods In General (AREA)
- Polymerization Catalysts (AREA)
- Epoxy Resins (AREA)
- Macromonomer-Based Addition Polymer (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Provided are a tetraphenyl ethane derivative represented by the following formula (1), a method for producing the same, a use of the tetraphenyl ethane derivative as a radical generating agent, a thermosetting liquid crystal sealing agent comprising the tetraphenyl ethane derivative and especially useful for liquid crystal dripping process, the radical generating agent having an excellent radical generating ability without inducing foaming, and when used in the liquid crystal sealing agent, thus having a long pot life, and excellent seal forming ability and gap forming ability, without any liquid crystal contamination. (wherein, Y1 and Y2 each independently represents a hydrogen atom, a phenyl group or a silicon atom, R1 to R6 each independently represents a hydrogen atom or a linear or branched C1 to 4 alkyl group, X1 to X4 each independently represents a hydrogen atom, a methyl group, a ethyl group, a methoxy group, an ethoxy group, a phenoxy group, or a halogen group. Provided that, when Y1 or Y2 is hydrogen atom, the R1 to R3 or R4 to R6 bonding toY1 or Y2 does not exist, and Y1 and Y2 are not both hydrogen atoms at the same time.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2009261421 | 2009-11-17 | ||
| JP2009269727 | 2009-11-27 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| TW201129574A true TW201129574A (en) | 2011-09-01 |
| TWI482777B TWI482777B (en) | 2015-05-01 |
Family
ID=44059397
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| TW099139293A TWI482777B (en) | 2009-11-17 | 2010-11-16 | Thermally curable liquid crystal sealing agent for drop fill process and liquid crystal display cell |
| TW103121871A TWI511974B (en) | 2009-11-17 | 2010-11-16 | Novel tetraphenyl ethane derivative, radical generating agent containing the same, cured article of the same and method for producing same |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| TW103121871A TWI511974B (en) | 2009-11-17 | 2010-11-16 | Novel tetraphenyl ethane derivative, radical generating agent containing the same, cured article of the same and method for producing same |
Country Status (5)
| Country | Link |
|---|---|
| JP (1) | JP5783606B2 (en) |
| KR (1) | KR101806152B1 (en) |
| CN (2) | CN102612521B (en) |
| TW (2) | TWI482777B (en) |
| WO (1) | WO2011061910A1 (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TWI466914B (en) * | 2013-03-07 | 2015-01-01 | Nippon Kayaku Kk | A liquid crystal display unit, and a liquid crystal display unit obtained by the method |
| TWI576360B (en) * | 2012-08-27 | 2017-04-01 | Nippon Kayaku Kk | A liquid crystal sealant and a liquid crystal display cell using the liquid crystal sealant |
Families Citing this family (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102011050035A1 (en) * | 2011-05-02 | 2012-11-08 | Byk-Chemie Gmbh | Low-emission, by free-radical polymerization thermally curable fiber-matrix semifinished product |
| KR101885944B1 (en) * | 2011-07-13 | 2018-08-06 | 닛뽄 가야쿠 가부시키가이샤 | Liquid crystal sealant and liquid crystal display cell using same |
| TW201420736A (en) * | 2012-07-17 | 2014-06-01 | Nippon Kayaku Kk | Liquid-crystal sealant and LCD cell using same |
| JP5531166B1 (en) * | 2013-03-07 | 2014-06-25 | 日本化薬株式会社 | Manufacturing method of liquid crystal display cell and liquid crystal display cell obtained by the method |
| JP6144961B2 (en) * | 2013-05-09 | 2017-06-07 | 積水化学工業株式会社 | Liquid crystal dropping method sealing agent, vertical conduction material, and liquid crystal display element |
| JP6182999B2 (en) * | 2013-06-25 | 2017-08-23 | 日油株式会社 | Thermosetting resin composition for color filter protective film, and color filter provided with the cured film |
| JP6288756B2 (en) * | 2013-07-16 | 2018-03-07 | 日本化薬株式会社 | Manufacturing method of liquid crystal display cell and liquid crystal display cell obtained by the method |
| JP6235297B2 (en) * | 2013-10-16 | 2017-11-22 | 日本化薬株式会社 | Liquid crystal sealant and liquid crystal display cell using the same |
| JP6238761B2 (en) * | 2014-01-20 | 2017-11-29 | 日本化薬株式会社 | Liquid crystal sealant and liquid crystal display cell using the same |
| JP2015215514A (en) * | 2014-05-12 | 2015-12-03 | 協立化学産業株式会社 | Sealant for liquid crystal display |
| CN106662781B (en) * | 2014-07-24 | 2020-05-15 | 三井化学株式会社 | Liquid crystal sealing agent and method for manufacturing liquid crystal display panel |
| JP2016038507A (en) | 2014-08-08 | 2016-03-22 | 日本化薬株式会社 | Liquid crystal sealing agent and liquid crystal display cell having the same |
| JP6465741B2 (en) * | 2015-05-11 | 2019-02-06 | 日本化薬株式会社 | Liquid crystal sealant and liquid crystal display cell using the same |
| JP6482371B2 (en) * | 2015-05-11 | 2019-03-13 | 日本化薬株式会社 | Method for producing resin composition |
| JP6465740B2 (en) * | 2015-05-11 | 2019-02-06 | 日本化薬株式会社 | Liquid crystal sealant and liquid crystal display cell using the same |
| EP3712192B1 (en) | 2017-11-16 | 2024-08-21 | Mitsubishi Chemical Corporation | Thermosetting resin composition, prepreg, and fiber-reinforced composite material and production method therefor |
| WO2019221027A1 (en) * | 2018-05-17 | 2019-11-21 | 積水化学工業株式会社 | Liquid crystal display element sealing agent, vertical conduction material, and liquid crystal display element |
| JP7432492B2 (en) | 2020-12-11 | 2024-02-16 | 日本化薬株式会社 | Liquid crystal sealant for liquid crystal dripping method |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2164482C3 (en) * | 1971-12-24 | 1980-07-31 | Bayer Ag, 5090 Leverkusen | Initiators for radical polymerization reactions |
| US3931355A (en) * | 1971-12-24 | 1976-01-06 | Bayer Aktiengesellschaft | Radical-initiated polymerization reactions and mixture |
| JPS57142990A (en) * | 1981-02-27 | 1982-09-03 | Yuki Gosei Yakuhin Kogyo Kk | Silylating reagent |
| US4393185A (en) * | 1981-06-02 | 1983-07-12 | Ciba-Geigy Corporation | Thermally polymerizable mixtures and processes for the thermally-initiated polymerization of cationically polymerizable compounds |
| JPH0311083A (en) * | 1989-06-08 | 1991-01-18 | Toray Dow Corning Silicone Co Ltd | Silylating agent |
| MXPA97008152A (en) * | 1997-10-23 | 2003-12-11 | Ct De Investigacion En Quimica | Method for the preparation of nanocomposites composed of dienic and thermoplastic elastomers. |
| JP3874073B2 (en) * | 2001-04-06 | 2007-01-31 | 信越化学工業株式会社 | Method for producing chlorosilane compound having texyl group |
| JP4405325B2 (en) * | 2004-06-23 | 2010-01-27 | 積水化学工業株式会社 | Sealant for liquid crystal display element, vertical conduction material, and liquid crystal display element |
-
2010
- 2010-11-12 KR KR1020127013344A patent/KR101806152B1/en active IP Right Grant
- 2010-11-12 CN CN201080051849.1A patent/CN102612521B/en active Active
- 2010-11-12 JP JP2011541804A patent/JP5783606B2/en active Active
- 2010-11-12 CN CN201410239409.9A patent/CN104031082A/en active Pending
- 2010-11-12 WO PCT/JP2010/006651 patent/WO2011061910A1/en active Application Filing
- 2010-11-16 TW TW099139293A patent/TWI482777B/en active
- 2010-11-16 TW TW103121871A patent/TWI511974B/en active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TWI576360B (en) * | 2012-08-27 | 2017-04-01 | Nippon Kayaku Kk | A liquid crystal sealant and a liquid crystal display cell using the liquid crystal sealant |
| TWI466914B (en) * | 2013-03-07 | 2015-01-01 | Nippon Kayaku Kk | A liquid crystal display unit, and a liquid crystal display unit obtained by the method |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102612521B (en) | 2015-10-07 |
| TW201437220A (en) | 2014-10-01 |
| JPWO2011061910A1 (en) | 2013-04-04 |
| KR101806152B1 (en) | 2017-12-07 |
| KR20120085855A (en) | 2012-08-01 |
| TWI511974B (en) | 2015-12-11 |
| WO2011061910A1 (en) | 2011-05-26 |
| CN102612521A (en) | 2012-07-25 |
| JP5783606B2 (en) | 2015-09-24 |
| CN104031082A (en) | 2014-09-10 |
| TWI482777B (en) | 2015-05-01 |
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