TH9592B - Methods for producing solid porous carbon material products and solid porous carbon products - Google Patents

Abstract

DC60 (03/12/40) Until now, the use of bran was less than it should have. And not in the used stage Is an industrial object source This invention is a method for manufacturing porous carbon products and solid porous carbon material products. Obtained from the above rice bran Let's burn and do Steady carbonization These materials were used in a wide variety of applications. It consists of different steps of kneading rice bran with thermosetting resin. And a sufficient amount of a solution containing wet flour and water. Bran is rice bran or wheat bran. The grain size Making the kneaded bran in metal mold, pressure and gas evacuation. Will be printed out Do burn and Carbonization That came out of the metal mold By heating the desired final combustion temperature at a predetermined rate Under an inactive gas atmosphere or under vacuum and cooling from the desired final combustion temperature. Reaching normal temperature too The rate was set until now, the use of bran was less than it should have. And not in the used stage Is an industrial object source This invention is a method for manufacturing porous carbon products and solid porous carbon material products. Obtained from the said dance Let's burn and do Steady carbonization The resulting materials are widely used in various applications. It consists of different steps of kneading rice bran with thermosetting resin. And a sufficient amount of a solution containing wet flour and water. Bran is rice bran or wheat bran. The grain size Making the kneaded bran in metal mold, pressure and gas evacuation. Will be printed out Do burn and Carbonization That came out of the metal mold By heating the desired final combustion temperature at a predetermined rate Under an inactive gas atmosphere or under vacuum and cooling from the desired final combustion temperature. Reaching normal temperature too Predetermined rate

Claims (1)

1.Method for producing carbon-inorganic composites Porouscarbon-inorganic composite material consists of various processes of fat-degreased rice bran with a thermoseting resin with sufficient amounts of Slurry with wet talc or water Making a fat-degreased side dance that is massaged into tablets. To get the grain size As already defined, forming of granulated fat-eliminated rice bran. In a metal mold by applying pressure And expel the gas To prepare the molded products Sintering and carbonization Products that are formed to prepare products that have been carbonized. Nice removed from the used metal die by heating it to the desired final combustion temperature at a predetermined rate under an inactive gas atmosphere. Or under vacuum and to cool the carbonized product to normal temperature with the predetermined rate 2. Methods consistent with claim 1, where the molded product Was heated from Room temperature to 250 ํ at 1.2 ํ / min, from 250 ํ to 350 ํ at a rate of 1 ํ / minute, from 350 ํ to 500 ํ at the rate of 1.2 ํ / min, maintain your position at 500 Is the final combustion temperature of 3 cm in the process of combustion. Or carbonization under an inactive gas atmosphere or under vacuum It was then cooled to normal temperature at a rate of 1.5 ํ / min in the cooling process. 3. Method corresponding to claim 1, where the 12 mesh grain size was the specified grain size. The temperature of 500 ํ is the desired final combustion temperature. 4. Method corresponding to claim 3, where the pelletizing process is performed by heating up to 80 ํ. Porous carbon-inorganic composite material It consists of a different process of kneading the degreased rice bran sifted through a 20 mesh sieve with thermosetting resin and a sufficient amount of slurry containing wet talc or water. Making rice bran that has been eliminated fat that has been massaged into granules. By heating 60 ํ to 80 ํ C and eliminating volatile substances. Forming the pellets that are then sifted into a sieve. With the grain size as obtained Already set in the desired metal mold By applying pressure And repeating the gas out To prepare the molded products Sintering and carbonization Products that have been formed to prepare carbonized products. Nice removed from the metal mold, too, heated to the desired final burning temperature. The predetermined rate under inactive gas pressure. Or under vacuum and cooling of the product that has been carbonized from the last combustion temperature to the normal temperature at a predetermined rate. 6. Methods consistent with claim 5, where the product That was molded to be heated from Room temperature to 250 ํ at 1.2 ํ / min, from 250 ํ to 350 ํ at a rate of 1 ํ / min, from 350 ํ to 500 ํ at the rate of 1.2 ํ / min, keep it at 500 ํ. For 3cm in the process of combustion and carbonization under a gas-tight atmosphere Or under vacuum and cooled to normal temperature at a rate of 1.5 ํ / min in the cooling process. 7. Production method of carbon composites. - Inorganic porous solid It consists of different steps of massaged fat-degreased rice bran with adjusted grains. With thermosetting resin and sufficient amount of solution containing wet talc or water Making rice bran that has been kneaded into granules To have a parallel grain as has been defined Forming the pellets that are then sifted into a sieve. With the grain size as obtained Already retracted into the desired metal mold By applying pressure And repeating the gas out To prepare the molded products Sintering and carbonization Products that are formed to prepare products that have been carbonized. The nice was removed from the metal mold by heating the final combustion temperature of approximately 700 ํ C or more with a rate of As predetermined under inactive gas pressure Or under vacuum and cooling of the carbonized product that has been cooled from the last combustion temperature to the normal temperature at a predetermined rate. 8. Approach corresponding to claim 7, where The molded product is heated from Room temperature up to 250 ํ at 1.2 ํ / minute, from 250 ํ to 350 ํ at a rate of 1 ํ / minute, from 350 ํ to 500 ํ at 1.2 ํ / minute. To maintain at 500 ํ for 2 cm in the combustion or carbonization process under an inactive gas atmosphere. Or under vacuum and cooled to normal temperature at 1.5 ํ / min in the cooling process 9. Method consistent with claim 7, where bran is bran with The massaging process was performed by adding 24% phenolic resin by weight to the degreased rice bran. 1 0. Manufacturing Methods Carbon products. - Inorganic porous solid It consists of various methods of kneading the degreased rice bran sifted through a 20 mesh sieve with thermosetting resin. And a sufficient amount of the solution that contains wet talc or water. Making rice bran that has been kneaded into granules By heating 60 ํ to 80 ํ C and eliminating volatile substances. Forming the pellets that are then sifted into a sieve. With the grain size as obtained Already retracted into the desired metal mold By applying pressure And repeating the gas out To prepare the molded products Sintering and carbonization Products that are molded to prepare the products that are The carbonization was removed from the metal mold by heating it to the final combustion temperature of approximately 700 ํ or more at a rate of As predetermined under inactive gas pressure or under vacuum and the product The carbonization was cooled from the last burning temperature to the normal temperature at a predetermined rate. Electrolysis of carbonized products obtained in acid solution 1 1. Method consistent with claim 10, where the molded product is heated from Room temperature to 250 ํ at 1.2 ํ / min, from 250 ํ to 350 ํ at a rate of 1 ํ / min, from 350 ํ to 500 ํ at the rate of 1.2 ํ / min, maintain your current at 500 ํ. For 2 cm in the process of combustion or carbonization under an inactive gas atmosphere Or under vacuum and allowed to cool to normal temperature at 1.5 ํ / min in the cooling process.