SU71620A1 - The method of producing zinc phosphide and apparatus for performing this method - Google Patents
The method of producing zinc phosphide and apparatus for performing this methodInfo
- Publication number
- SU71620A1 SU71620A1 SU1087-47A SU352450A SU71620A1 SU 71620 A1 SU71620 A1 SU 71620A1 SU 352450 A SU352450 A SU 352450A SU 71620 A1 SU71620 A1 SU 71620A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- phosphorus
- zinc
- zinc phosphide
- producing zinc
- phosphide
- Prior art date
Links
Landscapes
- Lubricants (AREA)
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
Description
Прад.гагаетс способ гга.лучеии фосфида цинка B3anMo;j.eiicTBiieN{ желтого фосфора и цинка, отличающийс тем. что процесс взаимодействи между жидки фосфором и расплавлеипым ципком всдут в нагреваемом извне аппарате типа uiapoBofi ме.тыницы. снабженном хо ,1С|Дильником. расположенным )II аппарата, с це,тыо кондепсаппи непрореагировавших с цинком паров фосфора.The method is known as the method of radiation of zinc phosphide B3anMo; j.eiicTBiieN {yellow phosphorus and zinc, characterized in that. that the process of interaction between liquid phosphorus and molten zip is blown in an externally heated uiapoBofi type device, me. pages. equipped with ho, 1C | Dilnikom. located) of the II apparatus, on the whole, on the go of kodepsappi of the phosphorus vapors unreacted with zinc.
На чертеже схематически noKa:5aii предлагаемы ariiiapar.In the drawing, schematically, noKa: 5aii are proposed ariiiapar.
у ппарат представл ет собой помешенную в электропечь / шаровую мельницу 2, барабан которой опираетс цaпфa iи I 4 на подПинники 5.The appliance is an electric / ball mill 2 placed in an electric furnace, the drum of which rests the capstan I and I 4 on the pinboards 5.
загружаетс цинком через загрузочный ,1Юк о. Печь / закрьп ают и включают обогрев. После п,тав.тени цинка во Bininunoшуюс ..мельницу по нропушениой через трубе 7. снабженкой электрообогревательным устройством 8, осторожно подаетс отмеренное ко,1ичество жидкого же,ттого фосфора, которьн, пада на расплав ,1енный цинк, превращаетс в фосфид. Неуспевающие |)еагиро ;ать папы фосфора ковденсируютс на внутренней новерхностп встроенного вод ного конденсатора .9 и фосфор стекает обратно на поверхность цинка. Вода в конденсатор подаетс че)ез 10 н вытекает через полую папфу 4. Внешн поверхност, конденсатора 9 снабжена изол цией //. Дл очистки внутренней новерхности конденсатора 9 от с.тучайного образовани красного фосфора пре.тусмотрены 1нары 12. удерживаемые от скатывани буртиком 13. имеющим сверлени .тл стока фосфораОбразуюп1а с в мелынипе на поверхности цинка корочка фосфида непрерывно размалываетс шарами 14, что нар ду с полнотой реакции обеспечивает нужную тонину помола. Через Зи-НО миН. 1тэсле спуска всего фосфора иагрев выключаетс и мельница переноситс кранод па о.хлажцени-э, после чего готовый фосфид выгружаетс . loaded with zinc through the boot, 1 yuk o. The stove / stove and switch on heating. After p, thaw. Of zinc in a Bininusic mill, by means of a pipe through a pipe 7. A supply of an electrical heating device 8 is carefully applied to the measured amount of liquid, the same phosphorus phosphorus, the melt pad, 1% zinc is converted to phosphide. Poor phosphates of phosphorus are condensed on the inner surface of the integrated water condenser .9 and phosphorus flows back to the surface of zinc. Water to the condenser is fed through 10 n through the hollow duct 4. The external surface of the condenser 9 is insulated with //. In order to clean the internal surface of the condenser 9 from the mass formation of red phosphorus, 1 test 12 was held. Held from rolling down with a flange 13. Drilled with phosphorus runoff. Shaped in a shredder on the zinc surface, the crust of phosphide was continuously ground by balls 14, which is completely complete provides the necessary fineness of grinding. Through zi-but min. During the descent of all the phosphorus, the heater is turned off and the mill is transferred to the cranod oh hojadseni-e, after which the finished phosphide is discharged.
С 11ельк) :pcvu; iJai Crn-iH от мс;г 1Цого П1)01-1з;:йтн в рсзу;1ьтате i ypnoi реакции | 03;-;огс) ;1овышени дав.пеии , п;5едусл1огреи iii)e;i,oxpaните .чьнык , Bbiiio.iiieHHbiii в виде крышки /J, прижатой к полой цапфе пру киис;й /6. Пр .1 подьеме дав.чепи свыше pacieTiioro крышка 75, иружш;}, смвигаете по uairpaii.niroiUHM 17 и ;ij)i:oTK buu er Me;ibiiHuy.C 11elk): pcvu; iJai Crn-iH from ms; g 1Quogo P1) 01-1z;: yn to RSZ; 1yatte i ypnoi reactions | 03; -; ogs); 1 to increase the pressure of the lines, n; 5 deluxe conditions iii) e; i, optite.chyk, Bbiiio.iiieHHbiii in the form of a cover / J, pressed to the hollow pin of the sleeve; y / 6. Ex. 1, lifting the speed above pacieTiioro lid 75, andruzh;}, smuyvayu uairpaii.niroiUHM 17 and; ij) i: oTK buu er Me; ibiiHuy.
иособ получени фосфида luiiiKa взаимодействием же.иого п цинка. OT.;i и ч аю ;ц и не тем, что процесс взаи.моде| ;стду жидки tpoctpopoM и расплав.ленным цинком ведут в пагре1 звие аппарате типа шаровой ме/пдшцы, снабжемпом холом , руас::о,1о ке ппз1м внутри ainuipaTa, с цслвю копаенсаиии гирс:вавшнл с ш-птком па|к)в фосфо)а.and a method for producing luiiiKa phosphide by the interaction of the same zinc. OT.; I and chayu; c and not by the fact that the process is mutual. ; where the liquid tpoctpopoM and molten zinc are brought to the apparatus with a spherical ball / meteorology unit, provided with a cold, roacat :: o, 1 ke pptz1m inside ainuipaTa, with a copaensiai girs: a vannipacta with a pair of pts1m, inside ainuipaTa; )but.
тиарат дл выполнени способа но п. 1, о т л и ч а ю щ п и е Oil в;зп;о,1иеп в пиде niap-oBoii мельницы, внутри которой 5заи холсдилцник-кспденсатор, также выпо.тненный в ви:де .- с шарами, с целью очистки р/абочеИ поверхности хо.ПОдил депсатора от краено1о фосфора.tiarat for the implementation of the method of p. 1, of the oil in the oil; oh; o, 1iep in the niap-oBoii mill, inside which there is a 5-core horsdale-xpdensator, also available in the .- with balls, for the purpose of cleaning the p / abdomen; And the surface of the ho.Podil depsator from kraeno1o phosphorus.
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Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
SU1087-47A SU71620A1 (en) | 1947-03-01 | 1947-03-01 | The method of producing zinc phosphide and apparatus for performing this method |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
SU1087-47A SU71620A1 (en) | 1947-03-01 | 1947-03-01 | The method of producing zinc phosphide and apparatus for performing this method |
Publications (1)
Publication Number | Publication Date |
---|---|
SU71620A1 true SU71620A1 (en) | 1947-11-30 |
Family
ID=52630051
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
SU1087-47A SU71620A1 (en) | 1947-03-01 | 1947-03-01 | The method of producing zinc phosphide and apparatus for performing this method |
Country Status (1)
Country | Link |
---|---|
SU (1) | SU71620A1 (en) |
-
1947
- 1947-03-01 SU SU1087-47A patent/SU71620A1/en active
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