SU515437A3 - Способ получени алкандикарбоновых кислот - Google Patents
Способ получени алкандикарбоновых кислотInfo
- Publication number
- SU515437A3 SU515437A3 SU1959291A SU1959291A SU515437A3 SU 515437 A3 SU515437 A3 SU 515437A3 SU 1959291 A SU1959291 A SU 1959291A SU 1959291 A SU1959291 A SU 1959291A SU 515437 A3 SU515437 A3 SU 515437A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- acid
- solution
- peroxide
- minutes
- ferrous
- Prior art date
Links
- 239000002253 acid Substances 0.000 title claims description 13
- 150000007513 acids Chemical class 0.000 title claims description 6
- 238000004519 manufacturing process Methods 0.000 title description 3
- 238000000034 method Methods 0.000 claims description 11
- 150000002978 peroxides Chemical class 0.000 claims description 10
- 125000004432 carbon atom Chemical group C* 0.000 claims description 9
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 claims description 7
- 239000002904 solvent Substances 0.000 claims description 7
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 6
- 150000003839 salts Chemical class 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 4
- 238000006243 chemical reaction Methods 0.000 claims description 3
- 230000003647 oxidation Effects 0.000 claims description 2
- 238000007254 oxidation reaction Methods 0.000 claims description 2
- 238000000926 separation method Methods 0.000 claims description 2
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 claims 9
- WMRCTEPOPAZMMN-UHFFFAOYSA-N 2-undecylpropanedioic acid Chemical compound CCCCCCCCCCCC(C(O)=O)C(O)=O WMRCTEPOPAZMMN-UHFFFAOYSA-N 0.000 claims 6
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 claims 6
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims 2
- 238000004821 distillation Methods 0.000 claims 2
- 229910052742 iron Inorganic materials 0.000 claims 2
- 238000010521 absorption reaction Methods 0.000 claims 1
- 125000001931 aliphatic group Chemical class 0.000 claims 1
- 239000008346 aqueous phase Substances 0.000 claims 1
- 125000004429 atom Chemical group 0.000 claims 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 claims 1
- 238000001816 cooling Methods 0.000 claims 1
- FYLJKQFMQFOLSZ-UHFFFAOYSA-N cyclohexylperoxycyclohexane Chemical compound C1CCCCC1OOC1CCCCC1 FYLJKQFMQFOLSZ-UHFFFAOYSA-N 0.000 claims 1
- 239000003085 diluting agent Substances 0.000 claims 1
- 239000011790 ferrous sulphate Substances 0.000 claims 1
- 235000003891 ferrous sulphate Nutrition 0.000 claims 1
- 239000011521 glass Substances 0.000 claims 1
- 239000011261 inert gas Substances 0.000 claims 1
- JFKVLQMLKGZJOK-UHFFFAOYSA-L iron(2+);pentanoate Chemical compound [Fe+2].CCCCC([O-])=O.CCCCC([O-])=O JFKVLQMLKGZJOK-UHFFFAOYSA-L 0.000 claims 1
- 238000004811 liquid chromatography Methods 0.000 claims 1
- 229910052757 nitrogen Inorganic materials 0.000 claims 1
- 239000012044 organic layer Substances 0.000 claims 1
- 239000003960 organic solvent Substances 0.000 claims 1
- 239000011541 reaction mixture Substances 0.000 claims 1
- 239000007787 solid Substances 0.000 claims 1
- 238000003756 stirring Methods 0.000 claims 1
- 239000000126 substance Substances 0.000 claims 1
- 238000005292 vacuum distillation Methods 0.000 claims 1
- NQPDZGIKBAWPEJ-UHFFFAOYSA-N valeric acid Chemical compound CCCCC(O)=O NQPDZGIKBAWPEJ-UHFFFAOYSA-N 0.000 claims 1
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- VTLYFUHAOXGGBS-UHFFFAOYSA-N Fe3+ Chemical compound [Fe+3] VTLYFUHAOXGGBS-UHFFFAOYSA-N 0.000 description 1
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 1
- JYWWHUGVBALUCU-UHFFFAOYSA-J [Fe+2](Cl)Cl.S(=O)(=O)([O-])[O-] Chemical compound [Fe+2](Cl)Cl.S(=O)(=O)([O-])[O-] JYWWHUGVBALUCU-UHFFFAOYSA-J 0.000 description 1
- 150000007933 aliphatic carboxylic acids Chemical class 0.000 description 1
- 150000001735 carboxylic acids Chemical class 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/41—Preparation of salts of carboxylic acids
- C07C51/412—Preparation of salts of carboxylic acids by conversion of the acids, their salts, esters or anhydrides with the same carboxylic acid part
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7232963A FR2199531B1 (enExample) | 1972-09-18 | 1972-09-18 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU515437A3 true SU515437A3 (ru) | 1976-05-25 |
Family
ID=9104391
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1959291A SU515437A3 (ru) | 1972-09-18 | 1973-09-17 | Способ получени алкандикарбоновых кислот |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US3917687A (enExample) |
| JP (1) | JPS4969610A (enExample) |
| BR (1) | BR7307132D0 (enExample) |
| CH (1) | CH590813A5 (enExample) |
| CS (1) | CS178434B2 (enExample) |
| DD (1) | DD107256A5 (enExample) |
| DE (1) | DE2346998A1 (enExample) |
| ES (1) | ES418873A1 (enExample) |
| FR (1) | FR2199531B1 (enExample) |
| GB (1) | GB1407783A (enExample) |
| IT (1) | IT995435B (enExample) |
| NL (1) | NL7312461A (enExample) |
| SU (1) | SU515437A3 (enExample) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| IT1122203B (it) * | 1979-07-17 | 1986-04-23 | Brichima Spa | Processo per la produzione di composti organici alifatici,difunzionali |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2601224A (en) * | 1951-01-05 | 1952-06-24 | Du Pont | Preparation of difunctional compounds |
| US2601223A (en) * | 1951-01-05 | 1952-06-24 | Du Pont | Preparation of dibasic carboxylic acids |
-
1972
- 1972-09-18 FR FR7232963A patent/FR2199531B1/fr not_active Expired
-
1973
- 1973-07-19 DD DD172371A patent/DD107256A5/xx unknown
- 1973-09-10 NL NL7312461A patent/NL7312461A/xx not_active Application Discontinuation
- 1973-09-14 BR BR7132/73A patent/BR7307132D0/pt unknown
- 1973-09-17 SU SU1959291A patent/SU515437A3/ru active
- 1973-09-17 JP JP48103959A patent/JPS4969610A/ja active Pending
- 1973-09-17 CH CH1330873A patent/CH590813A5/xx not_active IP Right Cessation
- 1973-09-17 GB GB4357873A patent/GB1407783A/en not_active Expired
- 1973-09-17 US US397977A patent/US3917687A/en not_active Expired - Lifetime
- 1973-09-18 ES ES418873A patent/ES418873A1/es not_active Expired
- 1973-09-18 DE DE19732346998 patent/DE2346998A1/de active Pending
- 1973-09-18 IT IT29080/73A patent/IT995435B/it active
- 1973-09-18 CS CS6423A patent/CS178434B2/cs unknown
Also Published As
| Publication number | Publication date |
|---|---|
| GB1407783A (en) | 1975-09-24 |
| DD107256A5 (enExample) | 1974-07-20 |
| US3917687A (en) | 1975-11-04 |
| CS178434B2 (enExample) | 1977-09-15 |
| IT995435B (it) | 1975-11-10 |
| ES418873A1 (es) | 1976-06-16 |
| DE2346998A1 (de) | 1974-04-04 |
| NL7312461A (enExample) | 1974-03-20 |
| JPS4969610A (enExample) | 1974-07-05 |
| FR2199531A1 (enExample) | 1974-04-12 |
| CH590813A5 (enExample) | 1977-08-31 |
| FR2199531B1 (enExample) | 1975-03-14 |
| BR7307132D0 (pt) | 1974-07-18 |
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