SU416349A1 - - Google Patents

Info

Publication number

SU416349A1

SU416349A1 SU1746572A SU1746572A SU416349A1 SU 416349 A1 SU416349 A1 SU 416349A1 SU 1746572 A SU1746572 A SU 1746572A SU 1746572 A SU1746572 A SU 1746572A SU 416349 A1 SU416349 A1 SU 416349A1

Authority

SU

USSR - Soviet Union

Prior art keywords

hexafluoro

hexane

methanol

dimethylaminophenyl

boiling

Prior art date

1972-02-07

Links

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• OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 18
• VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 6
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
• 238000009835 boiling Methods 0.000 description 4
• 239000000203 mixture Substances 0.000 description 4
• HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
• 238000001816 cooling Methods 0.000 description 3
• 238000000034 method Methods 0.000 description 3
• 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 3
• 239000000047 product Substances 0.000 description 3
• UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 2
• UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 description 2
• 239000003795 chemical substances by application Substances 0.000 description 2
• 150000001875 compounds Chemical class 0.000 description 2
• 150000008050 dialkyl sulfates Chemical class 0.000 description 2
• VAYGXNSJCAHWJZ-UHFFFAOYSA-N dimethyl sulfate Chemical compound COS(=O)(=O)OC VAYGXNSJCAHWJZ-UHFFFAOYSA-N 0.000 description 2
• 239000000706 filtrate Substances 0.000 description 2
• 238000002955 isolation Methods 0.000 description 2
• 238000002360 preparation method Methods 0.000 description 2
• 150000003512 tertiary amines Chemical class 0.000 description 2
• OVEMTTZEBOCJDV-UHFFFAOYSA-N 4-hexylaniline Chemical compound CCCCCCC1=CC=C(N)C=C1 OVEMTTZEBOCJDV-UHFFFAOYSA-N 0.000 description 1
• 230000010933 acylation Effects 0.000 description 1
• 238000005917 acylation reaction Methods 0.000 description 1
• 239000003513 alkali Substances 0.000 description 1
• 230000029936 alkylation Effects 0.000 description 1
• 238000005804 alkylation reaction Methods 0.000 description 1
• 230000015572 biosynthetic process Effects 0.000 description 1
• 238000006243 chemical reaction Methods 0.000 description 1
• 238000009833 condensation Methods 0.000 description 1
• 230000005494 condensation Effects 0.000 description 1
• 238000006193 diazotization reaction Methods 0.000 description 1
• 238000010438 heat treatment Methods 0.000 description 1
• 238000004519 manufacturing process Methods 0.000 description 1
• 238000006396 nitration reaction Methods 0.000 description 1
• 230000001766 physiological effect Effects 0.000 description 1
• 239000000843 powder Substances 0.000 description 1
• 239000002244 precipitate Substances 0.000 description 1
• 238000006722 reduction reaction Methods 0.000 description 1
• 238000010992 reflux Methods 0.000 description 1
• 150000003839 salts Chemical class 0.000 description 1
• 238000007127 saponification reaction Methods 0.000 description 1
• 239000013049 sediment Substances 0.000 description 1
• 238000000926 separation method Methods 0.000 description 1
• 229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
• 235000017557 sodium bicarbonate Nutrition 0.000 description 1
• 238000003786 synthesis reaction Methods 0.000 description 1