SU356849A1 - - Google Patents
Info
- Publication number
- SU356849A1 SU356849A1 SU1615596A SU1615596A SU356849A1 SU 356849 A1 SU356849 A1 SU 356849A1 SU 1615596 A SU1615596 A SU 1615596A SU 1615596 A SU1615596 A SU 1615596A SU 356849 A1 SU356849 A1 SU 356849A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- trichlorethylene
- reaction
- chlorosilane
- hours
- mixture
- Prior art date
Links
- XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical group ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 10
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 5
- 229910052725 zinc Inorganic materials 0.000 claims description 5
- 239000011701 zinc Substances 0.000 claims description 5
- 239000005046 Chlorosilane Substances 0.000 claims description 4
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 4
- KOPOQZFJUQMUML-UHFFFAOYSA-N chlorosilane Chemical compound Cl[SiH3] KOPOQZFJUQMUML-UHFFFAOYSA-N 0.000 claims description 4
- 239000011777 magnesium Substances 0.000 claims description 4
- 229910052749 magnesium Inorganic materials 0.000 claims description 4
- 229910019142 PO4 Inorganic materials 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 229910052751 metal Inorganic materials 0.000 claims description 3
- 239000002184 metal Substances 0.000 claims description 3
- 239000003960 organic solvent Substances 0.000 claims description 3
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 3
- 239000010452 phosphate Substances 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims 1
- IJOOHPMOJXWVHK-UHFFFAOYSA-N chlorotrimethylsilane Chemical compound C[Si](C)(C)Cl IJOOHPMOJXWVHK-UHFFFAOYSA-N 0.000 description 12
- 239000005051 trimethylchlorosilane Substances 0.000 description 6
- CWMFRHBXRUITQE-UHFFFAOYSA-N trimethylsilylacetylene Chemical group C[Si](C)(C)C#C CWMFRHBXRUITQE-UHFFFAOYSA-N 0.000 description 6
- 238000004821 distillation Methods 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- 239000011541 reaction mixture Substances 0.000 description 3
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 2
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- KWYZNESIGBQHJK-UHFFFAOYSA-N chloro-dimethyl-phenylsilane Chemical compound C[Si](C)(Cl)C1=CC=CC=C1 KWYZNESIGBQHJK-UHFFFAOYSA-N 0.000 description 2
- 229910052744 lithium Inorganic materials 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 description 1
- 125000003710 aryl alkyl group Chemical group 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- MEUXNEGJODESOX-UHFFFAOYSA-N chloro-cyclohexyl-dimethylsilane Chemical compound C[Si](C)(Cl)C1CCCCC1 MEUXNEGJODESOX-UHFFFAOYSA-N 0.000 description 1
- XSDCTSITJJJDPY-UHFFFAOYSA-N chloro-ethenyl-dimethylsilane Chemical compound C[Si](C)(Cl)C=C XSDCTSITJJJDPY-UHFFFAOYSA-N 0.000 description 1
- XJIDVLVCFQUUMH-UHFFFAOYSA-N chloro-methyl-bis(2-methylphenyl)silane Chemical compound CC1=CC=CC=C1[Si](C)(Cl)C1=CC=CC=C1C XJIDVLVCFQUUMH-UHFFFAOYSA-N 0.000 description 1
- OJZNZOXALZKPEA-UHFFFAOYSA-N chloro-methyl-diphenylsilane Chemical compound C=1C=CC=CC=1[Si](Cl)(C)C1=CC=CC=C1 OJZNZOXALZKPEA-UHFFFAOYSA-N 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- -1 dimethylphenylethylene silane Chemical compound 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 150000001367 organochlorosilanes Chemical class 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000012429 reaction media Substances 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU356849A1 true SU356849A1 (enExample) |
Family
ID=
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| EP3390410B1 (en) | Methods of making high purity trisilylamine | |
| Hatanaka et al. | On the regioselectivity of palladium catalyzed cross-coupling reactions of alkenylsilanes: Participation of β-cationic organosilicate-palladium species during the transmetallation | |
| US4801719A (en) | Silanes, process for their preparation, and their use | |
| SU356849A1 (enExample) | ||
| JPH0547552B2 (enExample) | ||
| US4837339A (en) | 4-Substituted-1,2,3,6-tetrahydrophthalic acid anhydride | |
| Labrecque et al. | Synthesis of (aminomethyl) silanes with the use of an easily cleavable carbon-silicon bond | |
| US4469881A (en) | [2-(p-t-Butylphenyl)ethyl]silanes and method of making the same | |
| Yuan et al. | A new and efficient asymmetric synthesis of 1‐amino‐1‐alkylphosphonic acids | |
| JPS6320834B2 (enExample) | ||
| Bochatay et al. | 4-Amino-1-allenylsilanes from 4-Aminopropargylic Acetates through a Silylzincation/Elimination Sequence | |
| US4748262A (en) | (Phenyl dimethyl carbinyl) silane compound and a method for the preparation thereof | |
| US4661608A (en) | Process for the manufacture of silylmetallocene compounds | |
| Baum et al. | Synthesis of organosilanes and polysiloxanes with nitro and fluoro substituents | |
| SU677665A3 (ru) | Способ получени дихлорсилана | |
| JP3279620B2 (ja) | 光学活性シリル化合物の製造法 | |
| US5136072A (en) | Thexyl C1 -C4 alkyl dialkoxy silane | |
| JPS6212770B2 (enExample) | ||
| JP2001187795A (ja) | ハロゲン化１，２−ジシラエタンの製法 | |
| Sukata | Efficient synthesis of silyl azides using sodium azide impregnated on amberlite XAD resin | |
| JPH10218883A (ja) | Ｎ，ｎ−ビス（トリメチルシリル）アリルアミンの製造方法 | |
| US4824980A (en) | Process to produce O-silyl O,N-ketene acetals | |
| CN102482301B (zh) | 乙烯基-炔基取代的锗化合物和获得乙烯基-炔基取代的锗化合物的方法 | |
| JP4345118B2 (ja) | エチニルシクロプロパンの製造方法 | |
| RU2299213C1 (ru) | Способ получения алкоксисиланов |