SU332092A1 - - Google Patents
Info
- Publication number
- SU332092A1 SU332092A1 SU1258284A SU1258284A SU332092A1 SU 332092 A1 SU332092 A1 SU 332092A1 SU 1258284 A SU1258284 A SU 1258284A SU 1258284 A SU1258284 A SU 1258284A SU 332092 A1 SU332092 A1 SU 332092A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- mol
- temperature
- water
- stirring
- sodium
- Prior art date
Links
- 238000000034 method Methods 0.000 claims description 13
- -1 halide halides Chemical class 0.000 claims description 6
- 239000012736 aqueous medium Substances 0.000 claims description 4
- 150000001991 dicarboxylic acids Chemical class 0.000 claims description 4
- 150000002763 monocarboxylic acids Chemical class 0.000 claims description 4
- 229910052783 alkali metal Inorganic materials 0.000 claims description 3
- 239000013543 active substance Substances 0.000 claims description 2
- 125000003710 aryl alkyl group Chemical group 0.000 claims description 2
- 125000004432 carbon atom Chemical group C* 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 20
- 238000003756 stirring Methods 0.000 description 13
- 239000000047 product Substances 0.000 description 10
- 239000011541 reaction mixture Substances 0.000 description 9
- 239000007864 aqueous solution Substances 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 5
- 238000001035 drying Methods 0.000 description 5
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 4
- 239000007900 aqueous suspension Substances 0.000 description 4
- MKANCOHERYHKAT-UHFFFAOYSA-L dibenzyltin(2+);dichloride Chemical compound C=1C=CC=CC=1C[Sn](Cl)(Cl)CC1=CC=CC=C1 MKANCOHERYHKAT-UHFFFAOYSA-L 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 239000002244 precipitate Substances 0.000 description 3
- 239000000725 suspension Substances 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 2
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 2
- 239000000460 chlorine Substances 0.000 description 2
- 229910052801 chlorine Inorganic materials 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 150000004820 halides Chemical class 0.000 description 2
- 239000002674 ointment Substances 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- KYKFCSHPTAVNJD-UHFFFAOYSA-L sodium adipate Chemical compound [Na+].[Na+].[O-]C(=O)CCCCC([O-])=O KYKFCSHPTAVNJD-UHFFFAOYSA-L 0.000 description 2
- 239000001601 sodium adipate Substances 0.000 description 2
- 235000011049 sodium adipate Nutrition 0.000 description 2
- 239000011780 sodium chloride Substances 0.000 description 2
- UDWXLZLRRVQONG-UHFFFAOYSA-M sodium hexanoate Chemical compound [Na+].CCCCCC([O-])=O UDWXLZLRRVQONG-UHFFFAOYSA-M 0.000 description 2
- RYYKJJJTJZKILX-UHFFFAOYSA-M sodium octadecanoate Chemical compound [Na+].CCCCCCCCCCCCCCCCCC([O-])=O RYYKJJJTJZKILX-UHFFFAOYSA-M 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000004094 surface-active agent Substances 0.000 description 2
- 239000005711 Benzoic acid Substances 0.000 description 1
- OBLHJVIUIHMHOM-UHFFFAOYSA-L C(C1=CC=CC=C1)(=O)[O-].C(C1=CC=CC=C1)(=O)[O-].C(C1=CC=CC=C1)[Sn+2]CC1=CC=CC=C1 Chemical compound C(C1=CC=CC=C1)(=O)[O-].C(C1=CC=CC=C1)(=O)[O-].C(C1=CC=CC=C1)[Sn+2]CC1=CC=CC=C1 OBLHJVIUIHMHOM-UHFFFAOYSA-L 0.000 description 1
- QMBQNHGAJUNECS-UHFFFAOYSA-L C(CCCCCCCCC(=O)[O-])(=O)[O-].C(C1=CC=CC=C1)[Sn+2]CC1=CC=CC=C1 Chemical compound C(CCCCCCCCC(=O)[O-])(=O)[O-].C(C1=CC=CC=C1)[Sn+2]CC1=CC=CC=C1 QMBQNHGAJUNECS-UHFFFAOYSA-L 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 229920012485 Plasticized Polyvinyl chloride Polymers 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 1
- UFYYBMYIZKRDCG-UHFFFAOYSA-L [benzoyloxy(dioctyl)stannyl] benzoate Chemical compound [O-]C(=O)C1=CC=CC=C1.[O-]C(=O)C1=CC=CC=C1.CCCCCCCC[Sn+2]CCCCCCCC UFYYBMYIZKRDCG-UHFFFAOYSA-L 0.000 description 1
- LVIAVDPYLHRLNQ-UHFFFAOYSA-L [dibenzyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound C=1C=CC=CC=1C[Sn](OC(=O)CCCCCCCCCCC)(OC(=O)CCCCCCCCCCC)CC1=CC=CC=C1 LVIAVDPYLHRLNQ-UHFFFAOYSA-L 0.000 description 1
- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 description 1
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 235000010233 benzoic acid Nutrition 0.000 description 1
- 239000003139 biocide Substances 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- SVSRQMUJHHQAAX-UHFFFAOYSA-N dibenzyltin Chemical compound C=1C=CC=CC=1C[Sn]CC1=CC=CC=C1 SVSRQMUJHHQAAX-UHFFFAOYSA-N 0.000 description 1
- URUAAUSPFAHCOA-UHFFFAOYSA-L dibenzyltin(2+) hexanoate Chemical compound C(CCCCC)(=O)[O-].C(CCCCC)(=O)[O-].C(C1=CC=CC=C1)[Sn+2]CC1=CC=CC=C1 URUAAUSPFAHCOA-UHFFFAOYSA-L 0.000 description 1
- BNADHZBWFBSFQB-UHFFFAOYSA-L dibenzyltin(2+);hexanedioate Chemical compound [O-]C(=O)CCCCC([O-])=O.C=1C=CC=CC=1C[Sn+2]CC1=CC=CC=C1 BNADHZBWFBSFQB-UHFFFAOYSA-L 0.000 description 1
- NTEABVBMFIONGY-UHFFFAOYSA-L dibenzyltin(2+);octadecanoate Chemical compound C=1C=CC=CC=1C[Sn+2]CC1=CC=CC=C1.CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O NTEABVBMFIONGY-UHFFFAOYSA-L 0.000 description 1
- RJGHQTVXGKYATR-UHFFFAOYSA-L dibutyl(dichloro)stannane Chemical compound CCCC[Sn](Cl)(Cl)CCCC RJGHQTVXGKYATR-UHFFFAOYSA-L 0.000 description 1
- AYOHIQLKSOJJQH-UHFFFAOYSA-N dibutyltin Chemical compound CCCC[Sn]CCCC AYOHIQLKSOJJQH-UHFFFAOYSA-N 0.000 description 1
- 239000012975 dibutyltin dilaurate Substances 0.000 description 1
- SBOSGIJGEHWBKV-UHFFFAOYSA-L dioctyltin(2+);dichloride Chemical compound CCCCCCCC[Sn](Cl)(Cl)CCCCCCCC SBOSGIJGEHWBKV-UHFFFAOYSA-L 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- POULHZVOKOAJMA-UHFFFAOYSA-M dodecanoate Chemical compound CCCCCCCCCCCC([O-])=O POULHZVOKOAJMA-UHFFFAOYSA-M 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000013467 fragmentation Methods 0.000 description 1
- 238000006062 fragmentation reaction Methods 0.000 description 1
- 239000012760 heat stabilizer Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229940070765 laurate Drugs 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- KZKQGUVWZYKJBN-UHFFFAOYSA-N methyl 5-methylsulfonylpyridine-3-carboxylate Chemical compound COC(=O)C1=CN=CC(S(C)(=O)=O)=C1 KZKQGUVWZYKJBN-UHFFFAOYSA-N 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 229920002379 silicone rubber Polymers 0.000 description 1
- 239000004945 silicone rubber Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000001632 sodium acetate Substances 0.000 description 1
- 235000017281 sodium acetate Nutrition 0.000 description 1
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 description 1
- 239000004299 sodium benzoate Substances 0.000 description 1
- 235000010234 sodium benzoate Nutrition 0.000 description 1
- 229960005480 sodium caprylate Drugs 0.000 description 1
- BTURAGWYSMTVOW-UHFFFAOYSA-M sodium dodecanoate Chemical compound [Na+].CCCCCCCCCCCC([O-])=O BTURAGWYSMTVOW-UHFFFAOYSA-M 0.000 description 1
- BYKRNSHANADUFY-UHFFFAOYSA-M sodium octanoate Chemical compound [Na+].CCCCCCCC([O-])=O BYKRNSHANADUFY-UHFFFAOYSA-M 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- LNANSYMQXPWAEI-UHFFFAOYSA-M tribenzylstannyl acetate Chemical compound C=1C=CC=CC=1C[Sn](CC=1C=CC=CC=1)(OC(=O)C)CC1=CC=CC=C1 LNANSYMQXPWAEI-UHFFFAOYSA-M 0.000 description 1
- 238000004073 vulcanization Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU332092A1 true SU332092A1 (en:Method) |
Family
ID=
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JPH08277291A (ja) | スルホン酸のジルコニウム化合物 | |
| US4001266A (en) | Process for the manufacture of 2-(2-hydroxyphenyl)benztriazoles | |
| SU332092A1 (en:Method) | ||
| JPH08253463A (ja) | Ｎ，ｎ−ジアルキル、−ジシクロアルキル、−ジアリール又は−ジアラルキルベンズチアゾリルスルフエンアミド類の製造法 | |
| US2904586A (en) | alpha-hydroxy-1, 2, 5, 6-tetrahydrobenzylphosphinous acid and preparation thereof | |
| EP0700379B1 (en) | Process to prepare p-alkyl- and p-arylsulphonylbenzoic acid derivatives | |
| KR100297624B1 (ko) | 유기인 화합물의 제조방법 | |
| JPS63258442A (ja) | テトラフルオロフタル酸の製造方法 | |
| RU1801112C (ru) | Способ получени О,О-диалкил-О-(2-трет-бутил-5-пиримидинил)тиофосфатов | |
| US4374778A (en) | Monoalkylfluorotin compounds | |
| US4877901A (en) | Process for synthesizing N,N'-dithiobis(sulfonamides) | |
| US7291741B2 (en) | Process of production of n-alkyl-2-benzthiazolysulfeneimides, device for their production and method of their purification | |
| US2764608A (en) | Dihalocyanovinyl benzoates | |
| KR900006556B1 (ko) | 2-구아니디노티아졸 유도체의 제조방법 | |
| JP2943944B2 (ja) | ３−置換−２，４，５−トリフルオロ安息香酸及びその 製造方法 | |
| JP2667201B2 (ja) | Ｌ−アスコルビン酸の製造法 | |
| WO2023156905A1 (en) | A process for the preparation of triclopyr-butotyl | |
| US2721208A (en) | Quaternary-ammonium-salt of n-beta-aminoethyl carbamates | |
| JPH0651660B2 (ja) | ニトロベンズアルデヒドの精製方法 | |
| SU400582A1 (ru) | Способ получения 4-карбоксиметилтиополихлор- пиридинов (или -алкилпиридинов) | |
| SU924044A1 (ru) | Способ получения триалкилизоциануратов 1 | |
| DE1768568B2 (de) | Verfahren zur herstellung von organozinnverbindungen | |
| SU328702A1 (ru) | Способ получени -тиазолил- или -пиримидиниламидов 2,3-дигидро-6метил-1,4-оксатиин карбоновой -5 кислоты | |
| RU2032691C1 (ru) | Способ получения окисей третичных фосфинов | |
| US3321500A (en) | Process for the preparation of alpha-monochlorohydrin monoesters of carboxylic acids |