SU199908A1 - - Google Patents
Info
- Publication number
- SU199908A1 SU199908A1 SU1085380A SU1085380A SU199908A1 SU 199908 A1 SU199908 A1 SU 199908A1 SU 1085380 A SU1085380 A SU 1085380A SU 1085380 A SU1085380 A SU 1085380A SU 199908 A1 SU199908 A1 SU 199908A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- chloromethyl
- bis
- solution
- thiophene
- derivative
- Prior art date
Links
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 9
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 9
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 7
- -1 5-ethyl mercapto-4 chloromethyl-2-methyl-thiophene Chemical compound 0.000 description 5
- 150000003568 thioethers Chemical class 0.000 description 4
- 229960000583 acetic acid Drugs 0.000 description 3
- HRQGCQVOJVTVLU-UHFFFAOYSA-N bis(chloromethyl) ether Chemical compound ClCOCCl HRQGCQVOJVTVLU-UHFFFAOYSA-N 0.000 description 3
- 239000000155 melt Substances 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- NNRCAZIHWSMGBR-UHFFFAOYSA-N 3,4-bis(chloromethyl)-2,5-bis(methylsulfanyl)thiophene Chemical compound CSC=1SC(SC)=C(CCl)C=1CCl NNRCAZIHWSMGBR-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 125000000217 alkyl group Chemical group 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 125000004772 dichloromethyl group Chemical group [H]C(Cl)(Cl)* 0.000 description 2
- 239000012362 glacial acetic acid Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- XKJCHHZQLQNZHY-UHFFFAOYSA-N phthalimide Chemical class C1=CC=C2C(=O)NC(=O)C2=C1 XKJCHHZQLQNZHY-UHFFFAOYSA-N 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- MRQAWFUGTGBTKD-UHFFFAOYSA-N 2,5-diethylthiophene-3-thiol Chemical compound CCc1cc(S)c(CC)s1 MRQAWFUGTGBTKD-UHFFFAOYSA-N 0.000 description 1
- ZLSMPEVZXWDWEK-UHFFFAOYSA-N 2-methylsulfanylthiophene Chemical compound CSC1=CC=CS1 ZLSMPEVZXWDWEK-UHFFFAOYSA-N 0.000 description 1
- CAMMXFZPWQSNTJ-UHFFFAOYSA-N 3-(chloromethyl)-2,5-bis(methylsulfanyl)thiophene Chemical compound CSC1=CC(CCl)=C(SC)S1 CAMMXFZPWQSNTJ-UHFFFAOYSA-N 0.000 description 1
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- 235000011148 calcium chloride Nutrition 0.000 description 1
- 239000003610 charcoal Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 125000004218 chloromethyl group Chemical group [H]C([H])(Cl)* 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 239000012044 organic layer Substances 0.000 description 1
- 239000013618 particulate matter Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 125000001544 thienyl group Chemical group 0.000 description 1
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU199908A1 true SU199908A1 (cg-RX-API-DMAC10.html) |
Family
ID=
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