SU182134A1 - - Google Patents

Info

Publication number

SU182134A1

SU182134A1 SU1005666A SU1005666A SU182134A1 SU 182134 A1 SU182134 A1 SU 182134A1 SU 1005666 A SU1005666 A SU 1005666A SU 1005666 A SU1005666 A SU 1005666A SU 182134 A1 SU182134 A1 SU 182134A1

Authority

SU

USSR - Soviet Union

Prior art keywords

phosgene

solution

ate

temperature

mol

Prior art date

Links

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• YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 12
• YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 description 6
• JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 4
• MWFMGBPGAXYFAR-UHFFFAOYSA-N 2-hydroxy-2-methylpropanenitrile Chemical compound CC(C)(O)C#N MWFMGBPGAXYFAR-UHFFFAOYSA-N 0.000 description 3
• UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
• 238000000034 method Methods 0.000 description 3
• RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
• VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
• 238000006243 chemical reaction Methods 0.000 description 2
• AOGYCOYQMAVAFD-UHFFFAOYSA-N chlorocarbonic acid Chemical compound OC(Cl)=O AOGYCOYQMAVAFD-UHFFFAOYSA-N 0.000 description 2
• IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 2
• 229910000041 hydrogen chloride Inorganic materials 0.000 description 2
• 239000000203 mixture Substances 0.000 description 2
• 239000003960 organic solvent Substances 0.000 description 2
• UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 2
• 239000002994 raw material Substances 0.000 description 2
• 238000003786 synthesis reaction Methods 0.000 description 2
• VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 2
• XCAFUVXBLCWDMX-UHFFFAOYSA-N 2-cyanopropan-2-yl carbonochloridate Chemical compound N#CC(C)(C)OC(Cl)=O XCAFUVXBLCWDMX-UHFFFAOYSA-N 0.000 description 1
• FZFAMSAMCHXGEF-UHFFFAOYSA-N chloro formate Chemical compound ClOC=O FZFAMSAMCHXGEF-UHFFFAOYSA-N 0.000 description 1
• -1 chloroformate ester Chemical class 0.000 description 1
• 238000001816 cooling Methods 0.000 description 1
• 238000000354 decomposition reaction Methods 0.000 description 1
• 150000002148 esters Chemical class 0.000 description 1
• 238000002329 infrared spectrum Methods 0.000 description 1
• 239000003208 petroleum Substances 0.000 description 1
• 238000002360 preparation method Methods 0.000 description 1
• AOJFQRQNPXYVLM-UHFFFAOYSA-N pyridin-1-ium;chloride Chemical compound [Cl-].C1=CC=[NH+]C=C1 AOJFQRQNPXYVLM-UHFFFAOYSA-N 0.000 description 1
• 238000001953 recrystallisation Methods 0.000 description 1
• 238000010992 reflux Methods 0.000 description 1
• 238000003756 stirring Methods 0.000 description 1