SU1630611A3 - Способ получени производных 2-оксиндол-1-карбоксамида - Google Patents
Способ получени производных 2-оксиндол-1-карбоксамида Download PDFInfo
- Publication number
- SU1630611A3 SU1630611A3 SU853869756A SU3869756A SU1630611A3 SU 1630611 A3 SU1630611 A3 SU 1630611A3 SU 853869756 A SU853869756 A SU 853869756A SU 3869756 A SU3869756 A SU 3869756A SU 1630611 A3 SU1630611 A3 SU 1630611A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- oxindole
- group
- solvent
- fifteen
- alkyl
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract 4
- 238000002360 preparation method Methods 0.000 title claims abstract 4
- UYINJAQCJCYCGO-UHFFFAOYSA-N 2-oxo-3h-indole-1-carboxamide Chemical class C1=CC=C2N(C(=O)N)C(=O)CC2=C1 UYINJAQCJCYCGO-UHFFFAOYSA-N 0.000 title abstract 2
- 239000002904 solvent Substances 0.000 claims abstract description 8
- JYGFTBXVXVMTGB-UHFFFAOYSA-N indolin-2-one Chemical compound C1=CC=C2NC(=O)CC2=C1 JYGFTBXVXVMTGB-UHFFFAOYSA-N 0.000 claims abstract 5
- 125000000217 alkyl group Chemical group 0.000 claims abstract 4
- 229910052731 fluorine Inorganic materials 0.000 claims abstract 4
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract 4
- WRJWRGBVPUUDLA-UHFFFAOYSA-N chlorosulfonyl isocyanate Chemical compound ClS(=O)(=O)N=C=O WRJWRGBVPUUDLA-UHFFFAOYSA-N 0.000 claims abstract 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract 3
- 239000002253 acid Substances 0.000 claims abstract 2
- 125000003545 alkoxy group Chemical group 0.000 claims abstract 2
- 239000007864 aqueous solution Substances 0.000 claims abstract 2
- 238000009835 boiling Methods 0.000 claims abstract 2
- 230000007062 hydrolysis Effects 0.000 claims abstract 2
- 238000006460 hydrolysis reaction Methods 0.000 claims abstract 2
- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract 2
- 239000011707 mineral Substances 0.000 claims abstract 2
- 150000007522 mineralic acids Chemical class 0.000 claims abstract 2
- 125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 claims abstract 2
- 150000007524 organic acids Chemical class 0.000 claims abstract 2
- 239000003960 organic solvent Substances 0.000 claims abstract 2
- 125000001544 thienyl group Chemical group 0.000 claims abstract 2
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims description 12
- 238000001704 evaporation Methods 0.000 claims description 2
- 230000008020 evaporation Effects 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- SYSQUGFVNFXIIT-UHFFFAOYSA-N n-[4-(1,3-benzoxazol-2-yl)phenyl]-4-nitrobenzenesulfonamide Chemical class C1=CC([N+](=O)[O-])=CC=C1S(=O)(=O)NC1=CC=C(C=2OC3=CC=CC=C3N=2)C=C1 SYSQUGFVNFXIIT-UHFFFAOYSA-N 0.000 claims description 2
- 238000000655 nuclear magnetic resonance spectrum Methods 0.000 claims description 2
- 239000007858 starting material Substances 0.000 claims description 2
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 claims 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims 3
- 239000000460 chlorine Substances 0.000 claims 3
- 239000001257 hydrogen Substances 0.000 claims 3
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims 2
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims 2
- 229910052801 chlorine Inorganic materials 0.000 claims 2
- 239000011737 fluorine Substances 0.000 claims 2
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 claims 1
- 101100339482 Colletotrichum orbiculare (strain 104-T / ATCC 96160 / CBS 514.97 / LARS 414 / MAFF 240422) HOG1 gene Proteins 0.000 claims 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 claims 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 claims 1
- 229910052794 bromium Inorganic materials 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 claims 1
- 150000002431 hydrogen Chemical group 0.000 claims 1
- 230000003993 interaction Effects 0.000 claims 1
- JNCFYJHIPGISLS-UHFFFAOYSA-N n-(2-oxo-3h-indole-1-carbonyl)sulfamoyl chloride Chemical class C1=CC=C2N(C(=O)NS(=O)(=O)Cl)C(=O)CC2=C1 JNCFYJHIPGISLS-UHFFFAOYSA-N 0.000 claims 1
- 239000000243 solution Substances 0.000 claims 1
- 230000000202 analgesic effect Effects 0.000 abstract 1
- 230000003110 anti-inflammatory effect Effects 0.000 abstract 1
- 239000000571 coke Substances 0.000 abstract 1
- 150000002391 heterocyclic compounds Chemical class 0.000 abstract 1
- 125000004149 thio group Chemical group *S* 0.000 abstract 1
- 125000002023 trifluoromethyl group Chemical group FC(F)(F)* 0.000 abstract 1
- 150000003949 imides Chemical class 0.000 description 1
Landscapes
- Indole Compounds (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
- Plural Heterocyclic Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US59066784A | 1984-03-19 | 1984-03-19 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU1630611A3 true SU1630611A3 (ru) | 1991-02-23 |
Family
ID=24363181
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU853869756A SU1630611A3 (ru) | 1984-03-19 | 1985-03-18 | Способ получени производных 2-оксиндол-1-карбоксамида |
Country Status (7)
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP6570301B2 (ja) * | 2015-04-23 | 2019-09-04 | キヤノン株式会社 | ４−フルオロイサチン誘導体の製造方法 |
-
1985
- 1985-02-26 IN IN155/DEL/85A patent/IN162626B/en unknown
- 1985-03-18 SU SU853869756A patent/SU1630611A3/ru active
- 1985-03-18 DD DD85274213A patent/DD232265A5/de not_active IP Right Cessation
- 1985-03-18 MW MW585A patent/MW585A1/xx unknown
- 1985-03-18 ZA ZA851994A patent/ZA851994B/xx unknown
- 1985-03-19 JP JP5562885A patent/JPS60209565A/ja active Granted
- 1985-03-19 ZM ZM1085A patent/ZM1085A1/xx unknown
Non-Patent Citations (1)
| Title |
|---|
| El-Enany M.M., Ghoneim К.П., Khalifa M. Attempted Preparation of Certain Benzodiazepines. - Bull Fac. Pharm. Cairo Univ, 1975, 14, p.29- 37. Патент US № 4556672, кл.514-414, 1984. * |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0342270B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1991-06-26 |
| IN162626B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1988-06-18 |
| DD232265A5 (de) | 1986-01-22 |
| ZM1085A1 (en) | 1985-09-20 |
| MW585A1 (en) | 1986-04-09 |
| ZA851994B (en) | 1986-11-26 |
| JPS60209565A (ja) | 1985-10-22 |
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