SU154544A1 - - Google Patents

Info

Publication number

SU154544A1

SU154544A1 SU782241A SU782241A SU154544A1 SU 154544 A1 SU154544 A1 SU 154544A1 SU 782241 A SU782241 A SU 782241A SU 782241 A SU782241 A SU 782241A SU 154544 A1 SU154544 A1 SU 154544A1

Authority

SU

USSR - Soviet Union

Prior art keywords

acid

autoclave

mol

preparation

distillation

Prior art date

Links

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• 239000002253 acid Substances 0.000 description 5
• ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 3
• 238000002360 preparation method Methods 0.000 description 3
• IKHGUXGNUITLKF-UHFFFAOYSA-N Acetaldehyde Chemical compound CC=O IKHGUXGNUITLKF-UHFFFAOYSA-N 0.000 description 2
• 150000007513 acids Chemical class 0.000 description 2
• 150000001805 chlorine compounds Chemical class 0.000 description 2
• 150000001875 compounds Chemical class 0.000 description 2
• 238000004821 distillation Methods 0.000 description 2
• 238000000034 method Methods 0.000 description 2
• NGNBDVOYPDDBFK-UHFFFAOYSA-N 2-[2,4-di(pentan-2-yl)phenoxy]acetyl chloride Chemical compound CCCC(C)C1=CC=C(OCC(Cl)=O)C(C(C)CCC)=C1 NGNBDVOYPDDBFK-UHFFFAOYSA-N 0.000 description 1
• OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
• 238000001816 cooling Methods 0.000 description 1
• 239000000706 filtrate Substances 0.000 description 1
• 125000002485 formyl group Chemical class [H]C(*)=O 0.000 description 1
• 238000010438 heat treatment Methods 0.000 description 1
• 239000002917 insecticide Substances 0.000 description 1
• 230000003993 interaction Effects 0.000 description 1
• SAWKFRBJGLMMES-UHFFFAOYSA-N methylphosphine Chemical compound PC SAWKFRBJGLMMES-UHFFFAOYSA-N 0.000 description 1
• -1 methylphosphinic acid vinyl ester chloride Chemical compound 0.000 description 1
• SCLFRABIDYGTAZ-UHFFFAOYSA-N methylphosphonic acid dichloride Chemical compound CP(Cl)(Cl)=O SCLFRABIDYGTAZ-UHFFFAOYSA-N 0.000 description 1
• 239000003960 organic solvent Substances 0.000 description 1
• 229910052698 phosphorus Inorganic materials 0.000 description 1
• 239000011574 phosphorus Substances 0.000 description 1
• 229920000642 polymer Polymers 0.000 description 1
• 239000011541 reaction mixture Substances 0.000 description 1
• 239000007858 starting material Substances 0.000 description 1
• 150000003512 tertiary amines Chemical class 0.000 description 1
• ILWRPSCZWQJDMK-UHFFFAOYSA-N triethylazanium;chloride Chemical compound Cl.CCN(CC)CC ILWRPSCZWQJDMK-UHFFFAOYSA-N 0.000 description 1
• 229920001567 vinyl ester resin Polymers 0.000 description 1