SU150493A1 - - Google Patents
Info
- Publication number
- SU150493A1 SU150493A1 SU747282A SU747282A SU150493A1 SU 150493 A1 SU150493 A1 SU 150493A1 SU 747282 A SU747282 A SU 747282A SU 747282 A SU747282 A SU 747282A SU 150493 A1 SU150493 A1 SU 150493A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- nitrocyclohexane
- methanol
- cyclohexanone oxime
- electrodes
- diaphragm
- Prior art date
Links
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 19
- VEZUQRBDRNJBJY-UHFFFAOYSA-N cyclohexanone oxime Chemical compound ON=C1CCCCC1 VEZUQRBDRNJBJY-UHFFFAOYSA-N 0.000 description 14
- NJNQUTDUIPVROZ-UHFFFAOYSA-N nitrocyclohexane Chemical compound [O-][N+](=O)C1CCCCC1 NJNQUTDUIPVROZ-UHFFFAOYSA-N 0.000 description 8
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 6
- 238000000034 method Methods 0.000 description 6
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 6
- 229910021529 ammonia Inorganic materials 0.000 description 3
- 238000005868 electrolysis reaction Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- GUQRKZPMVLRXLT-UHFFFAOYSA-N n-cyclohexylhydroxylamine Chemical compound ONC1CCCCC1 GUQRKZPMVLRXLT-UHFFFAOYSA-N 0.000 description 3
- 229910052697 platinum Inorganic materials 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 2
- PAFZNILMFXTMIY-UHFFFAOYSA-N cyclohexylamine Chemical compound NC1CCCCC1 PAFZNILMFXTMIY-UHFFFAOYSA-N 0.000 description 2
- VLKZOEOYAKHREP-UHFFFAOYSA-N methyl pentane Natural products CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 2
- -1 nitrocyclohexane ammonium salt Chemical compound 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 229920006395 saturated elastomer Polymers 0.000 description 2
- 239000002253 acid Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- GBMDVOWEEQVZKZ-UHFFFAOYSA-N methanol;hydrate Chemical compound O.OC GBMDVOWEEQVZKZ-UHFFFAOYSA-N 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
- 239000010937 tungsten Substances 0.000 description 1
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU150493A1 true SU150493A1 (enrdf_load_stackoverflow) |
Family
ID=
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US4714530A (en) | Method for producing high purity quaternary ammonium hydroxides | |
| DE10244633B3 (de) | Verfahren zur Herstellung von Alkincarbonsäuren durch Oxidation von Alkinalkoholen | |
| SU150493A1 (enrdf_load_stackoverflow) | ||
| US3193479A (en) | Electrolytic coupling of an olefinic compound with a ketone | |
| US2485982A (en) | Electrolytic production of aminoalcohols | |
| Shono et al. | Electro-organic chemistry. Part 93. Electro-organic transformation of aldehydes and ketones to α-hydroxylated acetals utilizing mediators and some synthetic uses of the products | |
| Lee et al. | Paired electro-oxidation Part II: Production of anthraquinone in an undivided cell | |
| US2793991A (en) | Production of cyanogen | |
| US3630860A (en) | Electrochemical treatment of material produced by reaction in electrochemical cell | |
| JPH04341593A (ja) | 水酸化第四アンモニウム水溶液の製造方法 | |
| JP2023521638A (ja) | レドックスフローセルにおける電解質としての使用のためのｔｅｍｐｏ誘導体溶液 | |
| Baizer et al. | Electrolytic Reductive Coupling: XX. Mixed Reductive Couplings with Acrylonitrile Reductions at the Cathode Voltage Required for the More Difficultly Reduced Partner | |
| Becker et al. | Electrochemical reduction of unsaturated nitriles in acetonitrile and nitromethane | |
| CN118726997B (zh) | 一种香兰素及其类似物的电氧化制备方法 | |
| Miralles-Roch et al. | Electrochemical conversion of α-nitrobenzylic compounds into the corresponding oximes—Part 2. Macroscale electrolyses | |
| EP4193004B1 (en) | Method for preparing 3-hydroxy-3-methylbutyric acid (hmb) or salts thereof | |
| Fichter | Electrochemical experiments with various organic acids | |
| SU619484A1 (ru) | Способ получени -метил -2пирролидона | |
| Joy et al. | A Novel Biphasic Electrolysis Method for the Oxidation of Benzaldoximes Using Potassium Perchlorate as the Mediator | |
| US4842700A (en) | Preparation of ω-hydroxyaldehydes or cyclic hemiacetals thereof | |
| US3658667A (en) | Electrolyte reduction of ozonolysis products | |
| US2916426A (en) | Electrolytic production of unsymmetrical dimethylhydrazine | |
| SU292887A1 (ru) | Способ получения гидроксилал^ина | |
| JP2599746B2 (ja) | エポキシケトンの開裂法 | |
| Ye et al. | Selective anodic oxidation of camphor |