SG189364A1 - A process for extracting antioxidants from oil palm biomass - Google Patents
A process for extracting antioxidants from oil palm biomass Download PDFInfo
- Publication number
- SG189364A1 SG189364A1 SG2013027313A SG2013027313A SG189364A1 SG 189364 A1 SG189364 A1 SG 189364A1 SG 2013027313 A SG2013027313 A SG 2013027313A SG 2013027313 A SG2013027313 A SG 2013027313A SG 189364 A1 SG189364 A1 SG 189364A1
- Authority
- SG
- Singapore
- Prior art keywords
- oil palm
- vessel
- biomass
- water soluble
- solvent
- Prior art date
Links
- 235000001950 Elaeis guineensis Nutrition 0.000 title claims abstract description 87
- 239000002028 Biomass Substances 0.000 title claims abstract description 76
- 238000000034 method Methods 0.000 title claims abstract description 40
- 239000003963 antioxidant agent Substances 0.000 title abstract description 7
- 240000003133 Elaeis guineensis Species 0.000 title 1
- 241000512897 Elaeis Species 0.000 claims abstract description 86
- 150000001875 compounds Chemical class 0.000 claims abstract description 49
- 239000002904 solvent Substances 0.000 claims abstract description 42
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims abstract description 40
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 39
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 39
- 239000003463 adsorbent Substances 0.000 claims abstract description 24
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 24
- 229910002092 carbon dioxide Inorganic materials 0.000 claims abstract description 20
- 239000001569 carbon dioxide Substances 0.000 claims abstract description 20
- 241001133760 Acoelorraphe Species 0.000 claims abstract description 12
- 239000000835 fiber Substances 0.000 claims abstract description 12
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical group O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000000741 silica gel Substances 0.000 claims abstract description 11
- 229910002027 silica gel Inorganic materials 0.000 claims abstract description 11
- 125000003158 alcohol group Chemical group 0.000 claims abstract description 8
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract description 48
- 238000000605 extraction Methods 0.000 abstract description 28
- 238000003809 water extraction Methods 0.000 abstract description 4
- 150000002989 phenols Chemical class 0.000 abstract description 2
- 238000003815 supercritical carbon dioxide extraction Methods 0.000 abstract description 2
- 230000002349 favourable effect Effects 0.000 abstract 1
- 239000003960 organic solvent Substances 0.000 abstract 1
- 230000001988 toxicity Effects 0.000 abstract 1
- 231100000419 toxicity Toxicity 0.000 abstract 1
- 239000002699 waste material Substances 0.000 abstract 1
- 239000000706 filtrate Substances 0.000 description 8
- 239000000843 powder Substances 0.000 description 8
- 239000000203 mixture Substances 0.000 description 4
- 239000012141 concentrate Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- JOHZPMXAZQZXHR-UHFFFAOYSA-N pipemidic acid Chemical compound N1=C2N(CC)C=C(C(O)=O)C(=O)C2=CN=C1N1CCNCC1 JOHZPMXAZQZXHR-UHFFFAOYSA-N 0.000 description 1
- 238000004094 preconcentration Methods 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/889—Arecaceae, Palmae or Palmaceae (Palm family), e.g. date or coconut palm or palmetto
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P39/00—General protective or antinoxious agents
- A61P39/06—Free radical scavengers or antioxidants
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/003—Refining fats or fatty oils by enzymes or microorganisms, living or dead
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/10—Refining fats or fatty oils by adsorption
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/15—Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/37—Extraction at elevated pressure or temperature, e.g. pressurized solvent extraction [PSE], supercritical carbon dioxide extraction or subcritical water extraction
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Microbiology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Medicinal Chemistry (AREA)
- Biochemistry (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- Pharmacology & Pharmacy (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Toxicology (AREA)
- General Chemical & Material Sciences (AREA)
- Alternative & Traditional Medicine (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Medical Informatics (AREA)
- Mycology (AREA)
- Epidemiology (AREA)
- Fats And Perfumes (AREA)
Abstract
This present invention relates to a process for extracting and recovering of water soluble compounds with anti-oxidative properties from oil palm biomass such as oil palm leaves, palm pressed fibre and empty fruit bunches. The process can be a sub critical water extraction, sub critical carbon dioxide extraction, supercritical water extraction or supercritical carbon dioxide extraction. Concentration of total phenolic compounds, a type of water soluble antioxidants in the oil palm leaves, pressed fibre and empty fruit bunches ranges from 5 to 20mg/g of biomass. These water soluble antioxidants can be extracted and recovered by way of solvent free process which is more favorable as the usage of organic solvents during extraction may pose problems of toxicity, waste disposal, storage as well as health issues. There are four different embodiments for extracting water soluble compounds with anti-oxidative properties. The four different embodiments are as follows: i) a process without solvent and without adsorbent; ii) a process without solvent but with adsorbent; iii) a process with solvent and with adsorbent; and iv) a process with solvent but without adsorbent. The adsorbent is silica gel and the solvent is alcohol such as methanol.
Description
A PROCESS FOR EXTRACTING ANTIOXIDANTS FROM OIL PALM
BIOMASS
The present invention relates to a process for extracting compounds with anti- oxidative properties from oil palm biomass such as oil palm leaves, palin pressed fibre and empty fruitbunches. :
The oil palm produces a vast variety of biomass, i.e. frond, empty fruit bunches, pressed fibre, etc. Each of these types of biomass has applications in different industries such as pulp and paper, wood and blo-ensrgy industries. Before being treated and used for these applications, the oil palm biomass is a potential source of water soluble antioxidants. Concentration of total phenolic compounds, a type of water soluble antioxidants in oil palm leaves, pressed fibre and empty fruit bunches ranges from 5 to 20mg/g of biomass. Therefore there is a need to extract the water soluble antioxidants from the oil palm biomass.
The present invention relates to a process for extracting and recovering of water soluble compounds with anti-oxidative properties from oil palm biomass such as oil palm leaves, palm pressed fibre and empty palm fruit bunches. There are four different embodiments for extracting water soluble compounds with anti-oxidative properties. 25: The first embodiment of the process for extracting water soluble compounds with anti-oxidative properties from oil palm biomass includes the steps of: i) reducing size of the oil palm biomass between 2-10mm length; i1) loading the oil palm biomass from step (i) into a vessel; iii) subjecting the oil palm biomass with a stream of carbon dioxide having pressure range of 30-70MPa; iv) collecting water soluble compounds released from an outlet of the vessel.
The second embodiment of the process for extracting water soluble compounds with anti-oxidative properties from oil palm biomass includes the steps of: i) reducing size of the oil palm biomass between 2-10mm length; ii) ~~ immersing the oil palm biomass in a solvent; iif) = loading the oil palm biomass from step (ii) into a vessel containing adsorbent; iv) subjecting the oil palm biomass with a stream of carbon dioxide having pressure range of 30-70MPa ;
Vv) collecting water soluble compounds released from an outlet of the vessel.
The third embodiment of the process for extracting water soluble compounds with anti-oxidative properties from oil palm biomass includes the steps of: 1) reducing size of the oil palm biomass between 2-10mm length; ii) immersing the oil palm biomass in a solvent; 1i1) loading the oil palm biomass from step (ii) into a vessel containing adsorbent; iv) subjecting the oil palm biomass with a stream of carbon dioxide having pressure range of 30-70MPa and a stream of solvent simultaneously; v) collecting water soluble compounds released from an outlet of the vessel.
The fourth embodiment of the process for extracting water soluble compounds with anti-oxidative properties from oil palm biomass includes the steps of: i) reducing size of the oil palm biomass between 2-10mm length; i1) loading the oil palm biomass from step (i) into a vessel; iit) subjecting the oil palm biomass with a stream of carbon dioxide having pressure range of 30-70MPa and a stream of solvent simultaneously; iv) collecting water soluble compounds released from an outlet of the vessel.
The process for extracting water soluble compounds with anti-oxidative properties from oil palm biomass can be a sub critical water extraction, sub critical carbon dioxide extraction, supercritical water extraction or supercritical carbon dioxide extraction. The vessel is heated at a temperature range of 30-75°C upon loading of the oil palm biomass in the vessel in all the four embodiments. The adsorbent is silica gel. The solvent is alcohol such as methanol.
The present invention relates to a process for extracting and recovering of water soluble compounds with anti-oxidative properties from oil palm biomass such as oil palm leaves, palm pressed fibre and empty palm fruit bunches. There are four different embodiments for extracting water soluble compounds with anti-oxidative properties. The four different embodiments are as follows: 1) a process without solvent and without adsorbent; i) a process without solvent but with adsorbent; iii) a process with solvent and with adsorbent; and iv) a process with solvent but without adsorbent.
The adsorbent is silica gel and the solvent is alcohol such as methanol.
Hereinafter, this specification will describe the present invention according to the preferred embodiments of the present invention. However, it is to be understood that . limiting the description to the preferred embodiments of the invention is merely to facilitate discussion of the present invention and it is envisioned that those skilled in the art may devise various modifications and equivalents without departing from the scope of the appended claims.
All the four embodiments require grinding of the palm biomass into smaller mass or sizes prior to the process for extracting and recovering of water soluble compounds.
This allows for higher extraction efficiency. Once the oil palm biomass is grinded into smaller sizes, they are ready for extraction. :
The first embodiment relates to a process for extracting water soluble compounds with anti-oxidative properties without solvent and without adsorbent. In this case, the oil palm biomass is loaded into an empty vessel. Then, the vessel is sealed. The vessel comprises a vent for gas to pass through at top of the vessel and another vent or outlet at the other end. Gas which is pressurized and heated to certain pressure and temperature (termed as super or sub critical state) is pumped into the vessel. The gas which is passing through the oil palm biomass, dissolves and carries the anti-oxidative compounds along as it is being released from the outlet of the vessel. The gas released from the outlet is then collected. Once the gas is released from the vessel, it depressurized spontaneously, leaving behind the anti-oxidative compounds.
The second embodiment is similar to the first embodiment with the exception that theoil palm biomass is first immersed in a solvent and the solvent is then concentrated to a minimal volume. The solvent is then loaded into a vessel pre-packed with an adsorbent.
Pressurized gas is then pumped into the vessel and the anti-oxidative compounds are ~ being carried through the adsorbent to an outlet of the vessel upon which, they are collected. This embodiment gives an advantage of being able to concentrate the anti- oxidative compounds in the oil palm biomass prior to extraction, thus is more efficient and gives higher throughput.
The third embodiment is similar to the second whereby prior to extraction, the oil palm biomass is pre concentrated in a solvent and the solvent is loaded into a vessel pre packed with adsorbent. In this embodiment however, a solvent is pumped and pre mixed with pressurized gas before they are pumped into the vessel. The pressurized gas, solvent and anti-oxidative compounds from the oil palm biomass are then collected at an outlet of the vessel. This embodiment involves a solvent and therefore yields higher extraction efficiency than the embodiment without the presence of a solvent.
The fourth embodiment is similar to the first embodiment whereby the oil palm biomass is loaded straight into an empty vessel without the need for pre concentration in a solvent. A solvent is pumped and pre mixed with pressurized gas before they are : pumped into the vessel. The pressurized gas, solvent and anti-oxidative compounds from the oil palm biomass are then collected at an outlet of the vessel. This embodiment involves a solvent and therefore yields higher efficiency than the embodiment without the presence of solvent.
In all the four embodiments, the pressurized gas is carbon dioxide having pressure range of 30-70MPa. The vessel is heated at a temperature range of 30-75°C upon loading of the oil palm biomass in the vessel in all the four embodiments. The adsorbent is silica gel. The solvent is alcohol such as methanol. : :
The invention will be further understood from the following non-limited examples. ~~ EXAMPLE 1
Empty fruit bunch that is obtained upon pressing of oil palm fruit bunches for its oil is ground into powder form of 2 — 10mm length. 30g of the grounded empty fruit bunch are loaded into an empty, 30mL extraction vessel. The extraction vessel is then heated to 40°C. Pressurized carbon dioxide (150 bars, - 4°C) is pumped into the vessel for 3 hours.
The extract containing the anti-oxidative compounds that come out from an outlet of the extraction vessel is collected.
EXAMPLE 2
Empty fruit bunch that is obtained upon pressing of oil palm fruit bunches for its oil is ground into powder form of 2 — 10mm length. 5g of the grounded empty fruit bunch is immersed in 30mL methanol and mixed vigorously. Thereafter, the mixture is filtered and the methanol in the filtrate is removed till only about SmL remained. 1mL of the filtrate is loaded into 250mm length x 200mm internal diameter vessel which is pre- packed with silica gel. The extraction vessel is then heated to 40°C. Pressurized carbon dioxide (150 bars, - 4°C) is pumped into the vessel for 1hour. The extract containing the anti-oxidative compounds that come out from an outlet of the extraction vessel is collected. :
EXAMPLE 3 oo
Empty fruit bunch that is obtained upon pressing of oil palm fruit bunches for its oil is ground into powder form of 2 — 10mm length. 5g of the grounded empty fruit bunch is immersed in 30mL methanol and mixed vigorously. Thereafter, the mixture is filtered and the methanol in the filtrate is removed till only about 5mL remained. ImL of the filtrate is loaded into 250mm length x 200mm internal diameter vessel which is pre- packed with silica gel. The extraction vessel is then heated to 40°C. Pressurized carbon dioxide (150 bars, - 4°C) and 0.5mL methanol are pumped into the vessel simultaneously for 1 hour. The extract containing the anti-oxidative compounds that come out from an . outlet of the extraction vessel is collected. :
EXAMPLE 4
Empty fruit bunch that is obtained upon pressing of oil palm fruit bunches for its oil is ground into powder form of 2 — 10mm length. 30g of the grounded empty fruit bunch was loaded into an empty, 30mL extraction vessel. The extraction vessel is then heated to 40°C. Pressurized carbon dioxide (150 bars, - 4°C) and 0.2mL methanol are pumped into the vessel simultaneously for 3 hours. The extract containing the anti-oxidative compounds that come out from an outlet of the extraction vessel is collected.
EXAMPLE 5
Fresh oil palm leaves are grounded into powder form of 2 — 7mm length. 30g of the grounded oil palm leaves is loaded into an empty, 30mL extraction vessel. The extraction vessel is then heated to 40°C. Pressurized carbon dioxide (150 bars, - 4°C) is pumped into the vessel for 3 hours. The extract containing the anti-oxidative compounds that come out from an outlet of the extraction vessel is collected.
EXAMPLE 6
Fresh oil palm leaves are grounded into powder form of 2 — 10mm length. 5g of the grounded oil palm leaves is- immersed in 30mL methanol and mixed vigorously.
Thereafter, the mixture is filtered and the methanol in the filtrate is removed till only about 5mL remained. ImL of the filtrate is loaded into 250mm length x 200mm internal diameter vessel which is pre-packed with silica gel. The extraction vessel is then heated to 40°C. Pressurized carbon dioxide (150 bars, - 4°C) is pumped into the vessel for lhour. The extract containing the anti-oxidative compounds that come out from an outlet of the extraction vessel is collected. : oo :
EXAMPLE 7
Fresh oil palm leaves are grounded into powder form of 2 — 10mm length. 5g of the grounded empty fruit bunch is immersed in 30mL methanol and mixed vigorously.
Thereafter, the mixture is filtered and the methanol in the filtrate is removed till only about SmL remained. 1mL of the filtrate is loaded into 250mm length x 200mm internal diameter vessel which is pre-packed with silica gel. The extraction vessel is then heated to 40°C. Pressurized carbon dioxide (150 bars, - 4°C) and 0.5mL methanol are pumped into the vessel simultaneously for 1 hour. The extract containing the anti-oxidative = compounds that come out from an outlet of the extraction vessel is collected.
EXAMPLE 8 Co
Fresh oil palm leaves are grounded into powder form of 2 — 10mm length. 30g of the | grounded oil palm leaves is loaded into an empty, 30mL extraction vessel. The extraction vessel is then heated to 40°C. Pressurized carbon dioxide (150 bars, - 4°C) and 0.2mL methanol are pumped into the vessel simultaneously for 3 hours. The extract containing the anti-oxidative compounds that come out from an outlet of the extraction vessel is collected.
Claims (12)
1." A process for extracting water soluble compounds with anti-oxidative properties from oil palm biomass, the process includes the steps of: - 1) reducing size of the oil palm biomass between 2-10mm length; i1) loading the oil palm biomass from step (i) into a vessel; : 1ii) subjecting the oil palm biomass with a stream of carbon dioxide having pressure range of 30-70MPa; = - iv) collecting the water soluble compounds released from an outlet of the vessel. wherein the vessel is heated at a temperature range of 30-75°C upon loading of the oil palm biomass in the vessel; and ~~ wherein the oil palm biomass is such-as palm leaves, pressed fibre and empty fruit bunches.
2. A process for extracting water soluble compounds with anti-oxidative properties from oil palm biomass, the process includes the steps of: 1) reducing size of the oil palm biomass between 2-10mm length; ii) immersing the oil palm biomass in a solvent; ii1) loading the oil palm biomass from step (ii) into a vessel containing adsorbent; iv) subjecting the oil palm biomass with a stream of carbon dioxide having pressure range of 30-70MPa ; : Vv) collecting the water soluble compounds released from an outlet of the vessel. wherein the vessel is heated at a temperature range of 30-75°C upon loading of the oil palm biomass in the vessel; and | : wherein the oil palm biomass is such as palm leaves, pressed fibre and empty fruit bunches. :
3. The process for extracting water soluble compounds with anti-oxidative properties as claimed in claim 2 wherein the adsorbent is silica gel.
4. The process for extracting water soluble compounds with antioxidative properties as claimed in claim 2 wherein the solvent is alcohol.
5. A process for extracting water soluble compounds with anti-oxidative properties from oil palm biomass, the process includes the steps of: i) reducing size of the oil palm biomass between 2-10mm length; ii) immersing the oil palm biomass in a solvent; oo 1ii) loading the oil palm biomass from step (ii) into a vessel containing adsorbent; iv) subjecting the oil palm biomass with a stream of carbon dioxide having pressure range of 30-70MPa and a stream of solvent simultaneously; Vv) collecting the water soluble compounds released from an outlet of the vessel. wherein the vessel is heated at a temperature range of 30-75°C upon loading of the oil palm biomass in the vessel; and oo wherein the oil palm biomass is such as palm leaves, pressed fibre and empty fruit bunches.
6. The process for extracting water soluble compounds with anti-oxidative properties as claimed in claim 5 wherein the adsorbent is silica gel.
7. ~~ The process for extracting water soluble compounds with anti-oxidative properties as claimed in claim 5 wherein the solvent is alcohol.
8. A process for extracting water soluble compounds with anti-oxidative properties from oil palm biomass, the process includes the steps of: 1) reducing size of the oil palm biomass between 2-10mm length; ii) immersing the oil palm biomass in a solvent; 1i1) loading the oil palm biomass from step (ii) into a vessel containing adsorbent; iv) subjecting the oil palm biomass with a stream of carbon dioxide having pressure range of 30-70MPa and a stream of solvent simultaneously; Vv) collecting the water soluble compounds released from an outlet of the vessel. wherein the vessel is heated at a temperature range of 30-75°C upon loading of the oil palm biomass in the vessel; and = wherein the oil palm biomass is such as palm leaves, pressed fibre and empty fruit bunches.
9. The process for extracting water soluble compounds with anti-oxidative properties as claimed in claim 8 wherein the adsorbent is silica gel.
10. The process for extracting water soluble compounds with anti-oxidative properties as claimed in claim 8 wherein the solvent is alcohol.
11. A process for extracting water soluble compounds with anti-oxidative properties from oil palm biomass, the process includes the steps of: 1) | reducing size of the oil palm biomass between 2-10mm length; ii) loading the oil palm biomass from step (1) into a vessel; iii) subjecting the oil palm biomass with a stream of carbon dioxide having pressure range of 30-70MPa and a stream of solvent simultaneously; iv) collecting the water soluble compounds released from an outlet of the vessel. wherein the vessel is heated at a temperature range of 30-75°C upon loading of the oil palm biomass in the vessel; and wherein the oil palm biomass is such as palm leaves, pressed fibre and empty fruit bunches.
12. The process for extracting water soluble compounds with anti-oxidative properties as claimed in claim 11 wherein the solvent is alcohol.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| MYPI2010004801 | 2010-10-12 | ||
| PCT/MY2011/000217 WO2012050425A2 (en) | 2010-10-12 | 2011-10-12 | A process for extracting antioxidants from oil palm biomass |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SG189364A1 true SG189364A1 (en) | 2013-05-31 |
Family
ID=45938834
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SG2013027313A SG189364A1 (en) | 2010-10-12 | 2011-10-12 | A process for extracting antioxidants from oil palm biomass |
Country Status (3)
| Country | Link |
|---|---|
| MY (1) | MY177259A (en) |
| SG (1) | SG189364A1 (en) |
| WO (1) | WO2012050425A2 (en) |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| MY130618A (en) * | 2002-11-27 | 2007-07-31 | Malaysian Palm Oil Board | A method of extracting and isolating minor components from vegetable oil |
-
2011
- 2011-10-12 SG SG2013027313A patent/SG189364A1/en unknown
- 2011-10-12 WO PCT/MY2011/000217 patent/WO2012050425A2/en active Application Filing
- 2011-10-12 MY MYPI2013001268A patent/MY177259A/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| MY177259A (en) | 2020-09-10 |
| WO2012050425A3 (en) | 2012-06-07 |
| WO2012050425A2 (en) | 2012-04-19 |
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